Effects of temperature and load during hot impression behavior of Cr-Ni stainless steel

Austenitic Stainless steels are majorly used because of their high resistance to aqueous corrosion and high temperature properties. Some major applications of stainless steels at high temperatures include engine and exhaust components in aircrafts, recuperators in steel mills, and pulverized coal injection lances for blast furnaces. In all the above said applications, the components are constantly subjected to loads and high temperatures. This makes the study of their creep behavior very important to decide the life of the component. Cr-Ni stainless steel was used as a starting material, and hot impression creep test was performed on cylindrical samples of 10 mm height and 15 mm diameter for a dwell time of 150 min at two different loads of 84 and 98 MPa and at two different temperatures 450 and 500 °C. The time vs. indentation depth was plotted, and creep rate was calculated in each case. It was observed that with an increase in time, creep rate increased in the primary creep region and remained almost constant in the secondary creep region irrespective of temperature and load. The indentation depth and creep rate increased with an increase in load and temperature.

A case study on severe damage at a tunnel in serpentinite rock mass

Face squeezing, floor heave, and buckling of invert were found after a 10-day holiday in 2014 around the serpentinite face of a tunnel in Hokkaido, Japan. The damage continued for over 2 months, extending 400 m toward the entrance causing a massive roof fall. The tunnel was excavated again with a circular section and extra-thick shotcrete, and the face had crossed the damaged part 6 years after the damage occurred. Uniaxial and triaxial compression tests were carried out to obtain the mechanical properties of the serpentinite to clarify the severe damage mechanism at the tunnel. The main experimental findings are as follows. The uniaxial compressive strength of the serpentinite samples was very low, and the ratio of the strength to the estimated overburden pressure was extremely low. The parameter n indicated that the time-dependent deformation of the serpentinite was not large but the same as ordinary rocks. All specimens showed strain-hardening in the triaxial compression test, and the friction angle was very low by the brucite content. Only primary creep was observed in the multistage triaxial creep test. The pressure on the shotcrete from rock mass for the damaged tunnel was enough to cause creep deformation and failure of shotcrete. From the above findings, designing the concrete lining that can support the earth and water pressure is recommended for tunnel excavation in such a weak serpentinite rock mass, particularly with a very low friction angle by brucite. Highlights Face squeezing, floor heave, and buckling of invert were found after a 10-day holiday around the serpentinite face in Hokkaido, Japan. The time-dependent deformation of the serpentinite was not large but the same as ordinary rocks. All specimens showed strain-hardening in the triaxial compression test, and the friction angle was very low by the brucite content. Only primary creep was observed in the multistage triaxial creep test. The severe damage to the tunnel was not a brittle creep failure of the serpentinite rock mass itself but the shotcrete lining.

A Numerical and Experimental Assessment of the Small Punch Creep Test for 316L(N) Stainless Steels

This paper presents a finite element analysis of the small punch creep test for 316L(N), which is compared with experimental data for 650 and 700 °C. Special emphasis is placed on (i) assessing the influence of friction and (ii) comparing two different creep models: the simple Norton creep and the more general creep model. The computed normalized deflection rate versus time is almost identical for all cases, which allows for scaling of the results. The computed time to rupture increases linearly with the friction coefficient due to a reduction in the mean stress. There is a good overall agreement between the experimental values and the computed deflection rate for a friction coefficient of around 0.3. It is shown that the initial reduction in deflection rate is due to stress relaxation and homogenization, and is only marginally affected by primary creep hardening. The computed results are compared with the equivalent stress and strain rates in the recently published small punch standard (EN 10371). The computed von Mises stresses at minimum deflection decrease linearly with the friction coefficient but are consistently slightly higher than the equivalent stress in the standard. For the strain rates, the computed values are significantly higher than the equivalent values in the standard. The presented simulations give a deeper insight of the small punch creep and impact of key parameters such the friction coefficient and in general as a guidance to refinement and improvement of the empirically based formulae in the standard.

Observations of the creep of polar firn

Constant-load creep tests were performed at −10°C at various compressive stresses from 0.05 to 0.75 MPa on specimens taken every 10 m along a firn core extracted at Summit, Greenland in June 2017. The microstructures before and after creep testing were examined using both X-ray microtomography (micro-CT) and optical images from thin sections. An Andrade-like equation was used to describe the primary creep behavior and yielded the time exponent k of 0.17–0.76. The onset of secondary creep occurred at strains of ~0.5–3% but was sometimes not observed at all in shallow firn specimens and at stresses ⩽0.43 MPa even for strain up to 32%. For the 50–80 m firn crept at stresses ⩾0.55 MPa, secondary creep occurred at strains of 2.6 ± 0.28%, and the stress exponent, n, in Glen's law, was found to range from 4.1 to 4.6, similar to those observed for fully dense ice. Micro-CT observations of crept specimens showed that in most cases, the specific surface area, the total porosity and the structure model index decreased, while the structure thickness increased with increasing density. These microstructural characteristics are consistent with the densification of the firn. Optical images from thin sections showed that recrystallization occurred in some specimens that had undergone secondary creep.

The Effect of Specimen Size and Test Procedure on the Creep Behavior of ME21 Magnesium Alloy

Lightweight constructions and materials offer the opportunity to reduce CO2 emissions in the transport sector. As components in vehicles are often exposed to higher temperatures above 40% of the melting temperature, there is a risk of creep. The creep behavior usually is investigated based on standard procedures. However, lightweight constructions frequently have dimensions not adequately represented by standardized specimen geometries. Therefore, comparative creep experiments on non-standardized miniature and standardized specimens are performed. Due to a modified test procedure specified by a miniature creep device, only the very first primary creep stage shows a minor influence, but subsequently, no effect on the creep process is detected. The creep behavior of hot extruded and heat treated ME21 magnesium alloy is investigated. It is observed that the creep parameters determined by the miniature and standard creep tests are different. As the deviations are systematic, qualitatively, evidence of the creep behavior is achieved. The creep parameters obtained, and particularly the creep strain and the strain rate, show a higher creep resistance of the miniature specimen. An initial higher number of twinned grains and possible multiaxiality in the gauge volume of the miniature specimen can be responsible.

An analytic description of the creep deformation of metals in the ultrasonic field

The effect of superimposed ultrasonic vibration on the primary creep of metals is modeled in terms of the synthetic theory of irrecoverable deformation. We consider two sonication modes: (i) the ultrasound acts continuously during the deformation, and (ii) the ultrasound is periodically on and off. Whereas both cases show a significant increase in primary creep, the periodical sonication leads to higher deformation values. To catch the phenomenon of ultrasound-assisted creep, we extend the flow rule equation by a term that accounts for the process occurring on the microlevel of material induced by ultrasound.

Creep Damage Repair of a Nickel-Based Single Crystal Superalloy Based on Heat Treatment

Taking nickel-based single crystal superalloy DD6 as the research object, different degrees of creep damage were prefabricated by creep interruption tests, and then the creep damage was repaired by the restoration heat treatment system of solid solution heat treatment and two-stage aging heat treatment. The results show that with the creep time increasing, the alloy underwent microstructure evolution including γ′ phase coarsening, N-type rafting and de-rafting. After the restoration heat treatment, the coarse rafted γ′ phase of creep damaged specimens dissolved, precipitated, grew up, and became cubic again. Except for the specimens with creep interruption of 100 h, the γ′ phase can basically achieve the same arrangement as the γ′ phase of the original sample. The comparison of the secondary creep test shows that the steady-state creep stage of the test piece after the restoration heat treatment is relatively increased, and the total creep life can reach the same level as the primary creep life. The high temperature creep properties of the tested alloy are basically recovered, and the restoration heat treatment effect is good.