Microwave Processing Techniques for Electron Microscopy: A Four-Hour Protocol

Author(s):  
Rick T. Giberson ◽  
Richard S. Demaree
Author(s):  
S. Hasegawa ◽  
T. Kawasaki ◽  
J. Endo ◽  
M. Futamoto ◽  
A. Tonomura

Interference electron microscopy enables us to record the phase distribution of an electron wave on a hologram. The distribution is visualized as a fringe pattern in a micrograph by optical reconstruction. The phase is affected by electromagnetic potentials; scalar and vector potentials. Therefore, the electric and magnetic field can be reduced from the recorded phase. This study analyzes a leakage magnetic field from CoCr perpendicular magnetic recording media. Since one contour fringe interval corresponds to a magnetic flux of Φo(=h/e=4x10-15Wb), we can quantitatively measure the field by counting the number of finges. Moreover, by using phase-difference amplification techniques, the sensitivity for magnetic field detection can be improved by a factor of 30, which allows the drawing of a Φo/30 fringe. This sensitivity, however, is insufficient for quantitative analysis of very weak magnetic fields such as high-density magnetic recordings. For this reason we have adopted “fringe scanning interferometry” using digital image processing techniques at the optical reconstruction stage. This method enables us to obtain subfringe information recorded in the interference pattern.


2019 ◽  
Vol 29 (1) ◽  
pp. 1226-1234
Author(s):  
Safa Jida ◽  
Hassan Ouallal ◽  
Brahim Aksasse ◽  
Mohammed Ouanan ◽  
Mohamed El Amraoui ◽  
...  

Abstract This work intends to apprehend and emphasize the contribution of image-processing techniques and computer vision in the treatment of clay-based material known in Meknes region. One of the various characteristics used to describe clay in a qualitative manner is porosity, as it is considered one of the properties that with “kill or cure” effectiveness. For this purpose, we use scanning electron microscopy images, as they are considered the most powerful tool for characterising the quality of the microscopic pore structure of porous materials. We present various existing methods of segmentation, as we are interested only in pore regions. The results show good matching between physical estimation and Voronoi diagram-based porosity estimation.


2002 ◽  
Vol 8 (S02) ◽  
pp. 160-161 ◽  
Author(s):  
JoAnn Buchanan ◽  
Kristina D. Micheva ◽  
Stephen J Smith

2002 ◽  
Vol 8 (S02) ◽  
pp. 152-153 ◽  
Author(s):  
Ross G. Gerrity ◽  
George W. Forbes

1996 ◽  
Vol 452 ◽  
Author(s):  
Russell F. Pinizzotto ◽  
Young G. Rho ◽  
Yandong Chen ◽  
Robert M. Pirtle ◽  
Irma L. Pirtle ◽  
...  

AbstractThis paper describes the fabrication method and initial characterization of self-assembled mesoscale arrays of quantum-confined CdS nanoparticles using DNA as a template for the overall shape. Three DNAs were used: the circular and linear forms of the plasmid pUCLeu4, and circular φ×174 RF II. In all three cases, the mesoscale lengths are consistent with the A-form of DNA. The structural signatures and crystallography were confirmed using conventional and high resolution transmission electron microscopy, and electron diffraction. Optical spectroscopy demonstrated that the particles display quantum-confinement effects. This research is a fundamental demonstration of the power of combining biochemical and solid-state processing techniques.


1980 ◽  
Vol 2 ◽  
Author(s):  
A. G. CULLIS

ABSTRACTThe pulse processing techniques that have assumed prominence over the past few years offer various important advantages for device fabrication technology. However, the usefulness of each individual method depends substantially upon the specific annealing mechanism involved. This article demonstrates the role of electron microscopy in elucidating such mechanisms and in analysing annealed semiconductor structures of importance to both research workers and semiconductor technologists. The range of laser and electron beam pulse annealing methods is covered and defect structure transitions observed are related to the solid and liquid phase processes occurring. Characteristic impurity trapping and segregation phenomena are described.


2015 ◽  
Vol 4 (3) ◽  
pp. 1-15
Author(s):  
Tobias Choji ◽  
Samuel Ogenyi ◽  
Anthony Ngokere ◽  
Solomon Chollom ◽  
Kizito Jugu ◽  
...  

1994 ◽  
Vol 347 ◽  
Author(s):  
D. E. Clark ◽  
D. C. Folz ◽  
R. L. Schulz ◽  
Z. Fathi ◽  
A. D. Cozzi ◽  
...  

ABSTRACTMicrowave energy for processing materials is emerging as a vital manufacturing technology for the nineties and beyond. Research to date has shown significant advantages in several areas, including drying and sintering, joining, surface modification and waste remediation. Increased processing rates, improved physical and mechanical properties and, in some cases, reduced hazardous emissions have sparked the interest of many manufacturers in the ability to integrate microwave processing techniques into existing and future manufacturing operations. This presentation will provide an overview of the microwave processing research and development work in progress at the University of Florida.


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