Effect of Peel Side on Optimum Condition for Measuring Flexible Film Peel Strength in T-Peel Adhesion Test

2013 ◽  
Vol 42 (1) ◽  
pp. 20120342 ◽  
Author(s):  
Rozzeta Dolah ◽  
Zenichi Miyagi
2014 ◽  
Vol 68 (4) ◽  
Author(s):  
Rozzeta Dolah ◽  
Zenichi Miyagi ◽  
Bo Bergman

As many researches focused on application of robust design engineering in practical case study, very less concerned on the criticality to data measurement system in parameter design. This paper will emphasize on the importance to be critical to data obtained during experiment. The existence of outliers is often ignored and the impact overlooked, thus endanger the results by producing false alarm and giving completely wrong parameter setting. The optimum condition from the data that contains outliers is compared with the corrected data measurement. The finding presents the indication procedure on how to confirm whether the data is reliable or not for evaluation. The data is unreliable when two main indicators are detected. Firstly, the measurement data plot detects outlier through linear regression analysis as it does not belong on the linear line. Secondly, poor reproducibility presented by estimation and confirmation of signal-to-noise ratio. This failure affects the experimental design and lead to wrong optimum condition. T-peel adhesion test using orthogonal array L9 is done as a case study to elucidate the detection of outlier and outlier effect on optimum condition. 


1994 ◽  
Vol 3 (4) ◽  
pp. 404-411 ◽  
Author(s):  
M. Sexsmith ◽  
T. Troczynski

2021 ◽  
Vol 9 (1) ◽  
Author(s):  
M. P. Carbonell-Blasco ◽  
M. A. Pérez-Limiñana ◽  
C. Ruzafa-Silvestre ◽  
F. Arán-Ais ◽  
E. Orgilés-Calpena

AbstractPolyurethanes, one of the most used polymers worldwide, are strongly dependent of non-renewable fossil resources. Thus, boosting the production of new polyurethanes based on more sustainable raw materials is crucial to move towards the footwear industry decarbonisation. The aim of this study is to synthesise and characterise reactive hotmelt polyurethanes from biomass and CO2-based polyols as bioadhesives for the footwear industry. The influence of biobased polyols on the polyurethane structure, and therefore, on their final properties was analysed by different experimental techniques such us Fourier transform infrared spectroscopy (FTIR), Differential scanning calorimetry (DSC), Thermogravimetric analysis (TGA), Melting viscosity, Softening temperature and T-peel strength test, in order to assess their viability for the upper to sole bonding process. The results obtained indicated that the incorporation of different amounts of the biobased polyols produces changes in the structure and final performance of the polyurethanes. Therefore, adhesion test carried out by the T-peel test 72 h after the upper -to- sole bonding of the sustainable adhesives show high final adhesion values. These sustainable raw materials provide polyurethane adhesives with additional beneficial non-toxicity and sustainable characteristics, without harming their properties during their useful life.


1989 ◽  
Vol 62 (2) ◽  
pp. 367-385 ◽  
Author(s):  
M. H. Chung ◽  
G. R. Hamed

Abstract We summarize and conclude the following: 1. The T-peel adhesion between uncrosslinked layers of IIR and NBR is rate and temperature dependent. Failure is interfacial at low rates; bulk cohesive tearing of the rubber occurs at intermediate rates, while interfacial failure returns at high rates. 2. Adhesion data could be reduced to mastercurves with experimentally determined shift factors which were in reasonable agreement with those calculated from the universal WLF equation with a Tg=−69°C. 3. At the lowest test rates, peel specimens containing in situ-formed copolymer had lower strength than those without the copolymer. This is probably due to the easy slippage of the segments of the low-molecular-weight copolymer in this regime. 4. At intermediate rates, in situ copolymer had no effect on peel strength; specimens failed by bulk cohesive tearing of rubber, whether or not the copolymer was present. 5. At high rates, peel specimens containing the copolymer exhibited improved strengths. The behavior is consistent with previous results on the autohesion of elastomers. Interdiffused chains of relatively low molecular weight are only capable of providing strong adhesion when the test speed is sufficiently rapid.


2017 ◽  
Vol 13 (4) ◽  
pp. 812-816
Author(s):  
Farah Syuhada Abdul Halim ◽  
Sheela Chandren ◽  
Madzlan Aziz ◽  
Leaw Wai Loon ◽  
Hadi Nur

High voltage powder spray coating (HVPSC) is one of the methods used for coating substrate with polymer powder in industries. This study utilizes HVPSC as a new deposition method of carbon-based powdered materials on stainless steel. Carbon-titania (C/TiO2) coated stainless steel was successfully prepared from the mixture of epoxide and titania powder, sprayed onto stainless steel plate using HVPSC, followed by pyrolysis at 300 °C under nitrogen atmosphere. The functional group of C/TiO2 was confirmed by Fourier transform infrared (FTIR) spectroscopy, where the FTIR spectrum showed the presence of C─H sp3, C═O, C─O, and Ti─O peaks. The morphology of the C/TiO2 sample studied using field emission scanning electron microscopy (FESEM) clearly shows that the particles of TiO2 were coated with carbon on their surface.  The coating performance was evaluated through the abrasion test and showed no weight loss. Adhesion of C/TiO2 coating was also tested in the peel adhesion test and the result showed that the attachment of C/TiO2 on the stainless steel is very strong. It has been proven that the HVPSC method is not only a simple technique to coat materials but also a very durable one


1989 ◽  
Vol 3 (1) ◽  
pp. 175-187 ◽  
Author(s):  
J. Kim ◽  
K.S. Kim ◽  
Y.H. Kim

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