scholarly journals Quantitative evaluation of microleakage in class V cavities using one-bottle and self-etching adhesive systems

2004 ◽  
Vol 18 (3) ◽  
pp. 253-259 ◽  
Author(s):  
Fabiana Mantovani Gomes França ◽  
Flávio Henrique Baggio Aguiar ◽  
Alex José Souza dos Santos ◽  
José Roberto Lovadino
Keyword(s):  
Methylene Blue ◽  
In Vitro Study ◽  
Adhesive System ◽  
Acid Etching ◽  
Single Bond ◽  
Adhesive Systems ◽  
Class V ◽  
Bonding System ◽  
Root Dentin

The aim of this in vitro study was to evaluate quantitatively the microleakage in class V cavities restored with one-bottle and self-etching adhesive systems with and without previous acid etching. Two one-bottle adhesive systems (Single Bond and Prime & Bond 2.1) and one self-etching adhesive system (Clearfil Mega Bond) were used in this study. One hundred and twenty sound human premolar teeth were randomly divided into 6 groups, and 20 class V restorations were prepared in the root dentin to test each bonding system. Each bonding system was used with and without acid etching. Specimens were prepared, dyed with 2% methylene blue, sectioned, triturated, and evaluated with an absorbance spectrophotometer test in order to quantify the infiltrated dye. Results were statistically evaluated by ANOVA and Tukey-Kramer test. No statistically significant differences were found among the adhesive systems when no etching agent was used. However, the Single Bond adhesive system showed statistically significant lower microleakage means than Clearfil Mega Bond and Prime & Bond 2.1 when 37% phosphoric acid was used. Single Bond and Clearfil Mega Bond adhesive systems presented similar behavior when the manufacturers' instructions were followed.

scholarly journals Microleakage study of three adhesive systems

2004 ◽  
Vol 15 (3) ◽  
pp. 194-198 ◽  
Author(s):  
Vanessa Gallego Arias ◽  
Inger Teixeira Campos ◽  
Luiz André Freire Pimenta
Keyword(s):  
Methylene Blue ◽  
Dwell Time ◽  
Composite Resin ◽  
In Vitro Study ◽  
Adhesive System ◽  
Class Ii ◽  
The Self ◽  
Adhesive Systems ◽  
Molar Teeth

The purpose of this in vitro study was to evaluate the efficacy of three hydrophilic dentin adhesive systems to reduce class II restoration microleakage. A total of 60 human molar teeth were used in which two box cavities were made on the distal and mesial surfaces, with a cervical margin in dentin. These cavities were randomly divided into 3 groups (n = 40 each), according to adhesive system tested: G1: OptiBond SOLO®; G2: Amalgambond Plus®; G3: Etch & Prime 3.0®. The cavities were restored with the composite resin Z-100®. The groups were thermocycled 2000 times (5 ± 1ºC and 55 ± 1ºC) with a dwell time of 1 min. The teeth were then immersed in 2% methylene blue, pH 7.0, for 4 h, sectioned and observed with a stereomicroscope MEIJI 2000 (35X). The evaluation was made using scores (0-4) and the results were expressed through the sum of the ranks. G1 = 1994.00; G2 = 2294.00; G3 = 2972.00. The three groups were significantly different. The self-etching adhesive system Etch & Prime 3.0 was less effective in preventing microleakage. The OptiBond SOLO adhesive was the most effective in reducing microleakage in dentin margins when compared with Amalgambond Plus and Etch & Prime 3.0.

An In-Vitro Study of Microleakage Around Class V Cavities Bonded with a Self-Etching Material Versus a Conventional Two-Bottle System

2006 ◽  
Vol os13 (3) ◽  
pp. 107-111 ◽  
Author(s):  
Sinan Salim ◽  
Ario Santini ◽  
Alyaa Husham
Keyword(s):  
Flow Line ◽  
Adhesive System ◽  
The Self ◽  
Fisher Exact Test ◽  
Adhesive Systems ◽  
Class V ◽  
Bonding System ◽  
Significant Difference ◽  
Bonding Technique

Objective To evaluate the microleakage around class V restorations restored with either a self-etching adhesive system or a conventional two-bottle adhesive system used with ‘total etch’ technique, and their recommended resin-based composites (RBC). Methods Two types of adhesive systems were used. A self-etching adhesive, Etch and Prime 3.0 (Degussa AG, Hanau, Germany), and a conventional two-bottle adhesive, Gluma Solid Bond (Heraeus Kulzer, Dormagen, Germany). The bonding systems were used in strict accordance with the manufacturers’ instructions, except that, with the two-bottle adhesive system, the cavities were filled with either a ‘wet’ or a ‘dry’ bonding technique, subsequent to acid-etching with 20% phosphoric acid. Etch & Prime 3.0 was used in conjunction with Degufill Mineral (Degussa, Hanau, Germany) RBC and Gluma Solid Bond with Flow Line RBC (Heraeus Kulzer, Dormagen, Germany). Standardised bucco-cervical cavities were prepared on the buccal and lingual surfaces of 15 extracted maxillary first premolar teeth; all cavity margins were in enamel. Ten of the resulting cavities (Group A) were restored using Etch & Prime 3.0 and Degufill Mineral, ten (Group B) using Gluma Solid Bond (Wet Bond), and ten (Group C) using Gluma Solid Bond (Dry Bond). Leakage scores at occlusal and gingival margins were calculated after thermocycling 500 times between baths, held at 5°C and 55°C, respectively, with 30 seconds dwell time in both. Data were analysed by the Fisher Exact Test. Results There was no statistically significant difference between the self-etching adhesive and conventional two-bottle adhesive systems at either the occlusal or the gingival margins. With the self-etching adhesive, there was no statistically significant difference in leakage scores between occlusal and gingival margins. There was a statistically significant difference between the occlusal and the gingival margins when a ‘wet’ or ‘dry’ bonding technique was used with the conventional two-bottle adhesive system. Conclusions The results suggest that the application of a conventional two-bottle bonding system used with a ‘total etch’ technique is better than that of a self-etching adhesive system. With the former, the use of a ‘wet’ bonding does not give better results than a ‘dry’ bonding technique.

scholarly journals Effects of different antibacterial disinfectants on microleakage of bulk-fill composite bonded to different tooth structures

2021 ◽  
Vol 21 (1) ◽  
Author(s):  
Mohammed Bin-Shuwaish ◽  
Alhanouf AlHussaini ◽  
Lina AlHudaithy ◽  
Shamma AlDukhiel ◽  
Abdullah AlJamhan ◽  
...  
Keyword(s):  
In Vitro Study ◽  
Adhesive System ◽  
Control Group ◽  
Single Bond ◽  
Cavity Preparation ◽  
Universal Adhesive ◽  
Class V ◽  
Dye Penetration ◽  
Composite Samples

Abstract Background This in-vitro study aimed to investigate the effect of two different antibacterial disinfectants on the microleakage performance of newly developed bulk-fill composite, bonded to different tooth structures. Methods Class V cavities were prepared in 30 sound premolar teeth, with enamel occlusal margins (OM) and dentin cervical margins (CM). Two disinfectants, 2% chlorhexidine gluconate (CHX) and Listerine Miswak (ListM), were used. Teeth were divided into three groups (n = 10): G1, Control; G2, CHX; and G3, ListM. Disinfectants were applied to the cavity preparation walls after they were etched with 35% phosphoric acid. The Single Bond Universal adhesive system was then used, and teeth were restored with Filtek One Bulk Fill composite. Samples were examined, after thermocycling aging, by stereomicroscopy for the evaluation of marginal dye penetration. Results The highest mean microleakage score was reported in the CM of G1 (2.60 ± 1.174), which was significant compared with that of G2 only (p = 0.02). OM in G1 showed no microleakage, with no significant differences found among groups (χ2 = 1.39, p = 0.50). No significant differences were reported between G2 and G3 (p = 0.45 OM; p = 0.17 CM). Conclusions Cavity pretreatment with CHX is not significantly different to pretreatment with CHX. In contrast, CHX improved the cervical marginal seal as compare to the control group (G1).

scholarly journals Microleakage at enamel and dentin margins with a bulk fills flowable resin

2014 ◽  
Vol 08 (01) ◽  
pp. 001-008 ◽  
Author(s):  
Nicola Scotti ◽  
Allegra Comba ◽  
Alberto Gambino ◽  
Davide Salvatore Paolino ◽  
Mario Alovisi ◽  
...  
Keyword(s):  
Methylene Blue ◽  
Resin Composite ◽  
In Vitro Study ◽  
Artificial Ageing ◽  
Resin Composites ◽  
Class V ◽  
Dye Penetration ◽  
Before And After ◽  
Blue Solution

ABSTRACT Objective: The aim of this in vitro study was to evaluate the marginal sealing ability of a bulk fill flowable resin composite on both enamel and dentin substrates. Materials and Methods: 48 non-carious molars were selected and four Class-V cavities were prepared at the CEJ of each sample. Cavities were filled with Venus Diamond (Heraeus Kulzer); Venus Diamond Flow (Heraeus Kulzer) and Surefil SDR (Dentsply). Samples were divided into two groups: First group samples were immersed in a methylene blue solution for 30 min at 25°C. Second group samples were artificially aged and then treated with methylene blue. Samples were sectioned in the center of the restoration and observed with a 40x stereomicroscope, and the percentage of cavity infiltration was calculated. Results: Results were analyzed statistically by ANOVA (P < 0.05). The amount of infiltration was significantly lower for the enamel substrate compared with dentin (P = 0.0001) and in samples immediately immersed in methylene blue compared with those that were artificially aged (P = 0.011). The interaction between the composite material and the marginal substrate significantly affected dye penetration (P = 0.006). Conclusions: Bulk fill flowable resins provided significantly better marginal seal in dentin, both before and after artificial ageing. Nanohybrid resin composites and bulk fill flowable resins showed similar microleakage values at enamel margins. Bulk fills flowable resins provided significantly better marginal seal in dentin, both before and after artificial ageing. Nanohybrid resin composites and bulk fill flowable resins showed similar microleakage values at enamel margins.

scholarly journals A comparison of microleakage in self-etch fissure sealants and conventional fissure sealants with total-etch or self-etch adhesive systems

2018 ◽  
Vol 12 (02) ◽  
pp. 242-246 ◽  
Author(s):  
Azam Nahvi ◽  
Alireza Razavian ◽  
Hoorieh Abedi ◽  
Jamshid Yazdani Charati
Keyword(s):  
In Vitro Study ◽  
Conventional Technique ◽  
Single Bond ◽  
Adhesive Systems ◽  
Fissure Sealants ◽  
Fissure Sealant ◽  
Acid Etch ◽  
Self Etch ◽  
Group 1

ABSTRACT Objective: The present study was conducted to compare microleakage in self-etching fissure sealants and conventional fissure sealants with total-etch or self-etch adhesive systems. Settings and Design: This experimental in vitro study was conducted on 60 healthy third molars extracted from humans. The first group received Acid etch + Clinpro sealant, the second group received Acid etch + Single bond 2 + Clinpro sealant, the third group received Single bond universal (self-etching bonding) + Clinpro sealant, and the fourth group received prevent seal self-etching sealant. Materials and Methods: An incision was made on the teeth after they were immersed in methylene blue 5%. The samples were then examined under a stereomicroscope and the dye penetration rate was measured based on the Williams and Winter criteria. Statistical Analysis Used: The Kruskal–Wallis and Mann–Whitney tests were used for data analysis in SPSS-18 (P < 0.05). Results: Group 1 which was treated with the conventional technique (acid + fissure sealant) had the highest rate of microleakage compared to Groups 2 and 3 (P < 0.001). Conclusion: The results showed that the use of bonding results in a significant reduction in the microleakage of fissure sealants. The microleakage caused when using self-etch fissure sealant was not different from that caused by the use of the conventional method.

scholarly journals Influence of pH of different adhesive systems on the polymerization of a chemically cured composite resin

2005 ◽  
Vol 16 (2) ◽  
pp. 107-111 ◽  
Author(s):  
Eduardo Batista Franco ◽  
Lawrence Gonzaga Lopes ◽  
Paulo Henrique Perlatti D'Alpino ◽  
José Carlos Pereira
Keyword(s):  
Bond Strength ◽  
Composite Resin ◽  
Testing Machine ◽  
In Vitro Study ◽  
Adhesive Layer ◽  
Adhesive System ◽  
Steel Matrix ◽  
Adhesive Systems ◽  
Influence Of Ph

The purpose of this study was to investigate the effect of pH of different adhesive systems on the polymerization of a chemically cured composite resin (Adaptic - AD), by means of tensile bond strength testing. The adhesive systems tested were: ARM, Prime & Bond 2.1 (PB), Scotchbond Multi Purpose (SMP) and Single Bond (SB). Bond strength at the resin/adhesive system/resin interface was assessed. Five groups (n=5) were formed, according to following configuration: G1: AD/ARM/AD; G2: AD/PB/AD; G3: AD/SMP/AD; G4: AD/SB/AD; G5: AD/AD (no adhesive). A two-mold stainless steel matrix with a cone-shaped opening (1-mm-thick; 4 mm in diameter) was used to obtain resin discs. AD resin was inserted into the first mold, left-self curing and an adhesive layer was applied onto resin surface and light-cured. The second mold was assembled over the first and was filled with the resin. After 10 min, this setting was loaded in tension in a universal testing machine running at a crosshead speed of 0.5 mm/min. Data were submitted to one-way ANOVA and Tukey's test (p<0.05). Bond strength means (kgf) were: G1: 15.23 ± 4.1; G2: 0.00 ± 0.0; G3: 16.96 ± 2.4; G4: 10.08 ± 2.7; G5: 15.44 ± 0.9. There were statistically significant differences (p<0.05) between G2-G1; G2-G3; G2-G4; G4-G1; G4-G3. The systems with the lowest pHs (PB and SB) yielded the lowest bond strength. The findings of this in vitro study demostrates that the pH of adhesive systems influences the polymerization and bond strength of chemically cured resin materials. The low pH simplified adhesive systems showed distinct degrees of incompatibility with the chemically cured resin, when compared to the conventional adhesive systems.

scholarly journals Influence of chlorhexidine on longitudinal bond strength to dentin: in vitro study

2017 ◽  
Vol 20 (1) ◽  
pp. 17 ◽  
Author(s):  
Beatriz Maria Fonseca ◽  
Daphne Camara Barcellos ◽  
César Rogério Pucci ◽  
Eduardo Bresciani ◽  
Maria Amélia Máximo de Araújo
Keyword(s):  
Phosphoric Acid ◽  
Bond Strength ◽  
Water Storage ◽  
In Vitro Study ◽  
Chlorhexidine Gluconate ◽  
Acid Etching ◽  
Single Bond ◽  
Etch And Rinse

<p><strong>Objective</strong>: This study evaluated the effect of 0.2% chlorhexidine gluconate solution used as an therapeutic primer on the long-term bond strength of etch-and-rinse adhesive to dentin. <strong>Material</strong> <strong>and</strong> <strong>Methods</strong>: Bovine incisors were worn to expose an area of dentin and were divided into 2 groups: Group C (Control) - acid etching with 37% phosphoric acid + Single Bond; Group CHX (0.2% CHX) - acid etching with 37% phosphoric acid + 0.2% CHX for 30 s + Single Bond. Blocks of composite were fabricated and stored for 24 h or 6 months, sectioned into beams and submitted to microtensile tests. Results were analyzed by two-way ANOVA and Tukey tests. <strong>Results</strong>: Mean (±SD) values (in MPa) were as follow: Group CHX/24h - 41.8(±2.62)A; Group C/24h - 40.8(±3.35)AB; Group CHX/6 months – 36.4(±3.52)B; Group CHX/6 months - 26.1(±1.54)C. <strong>Conclusion</strong>: CHX improve the imediatte bond strength of resin-dentin and significantly lowered the loss of bond strength after 6 months water storage as seen in the control bonds.</p><p><strong>Keywords</strong></p><p>Tensile bond strength; Dentin; Total-etch adhesives; Chlorhexidine gluconate.</p>

scholarly journals Evaluation of Caries-Free Restorations Bonded with Various Adhesive Systems: In Vitro Study

2020 ◽  
Vol 2020 ◽  
pp. 1-7
Author(s):  
Morakot Piemjai ◽  
Pareewan Chantarawej ◽  
Nobuo Nakabayashi
Keyword(s):  
Resin Composite ◽  
Artificial Saliva ◽  
In Vitro Study ◽  
Negative Control ◽  
Adhesive Systems ◽  
Hybrid Layer ◽  
Class V ◽  
Secondary Caries ◽  
Dye Penetration

Purpose. Secondary caries originate from a leakage pathway where oral acids can penetrate faster and demineralize the tooth substrate deeper which can be visualized by dye penetration. The ability to prevent secondary caries by contemporary adhesive systems was evaluated in this study. Dye penetration distance through leakage and into the tooth substrate adjacent to Class V restorations after artificial caries exposure was compared. Materials and Methods. Previously frozen extracted human molars were used to prepare the Class V cavities at the CEJ on axial surfaces. All cavities were restored with either the resin-composite or amalgam with or without resin adhesives: dry bonding: Super-Bond D-Liner II Plus; moist bonding: All-Bond 2; and self-etch bonding: AQ Bond and Clearfil Protect Bond. Two subgroups of Super-Bond D-Liner II Plus were immersed for 14 days at 37°C either in artificial saliva (negative control) or the artificial caries solution. The other groups were soaked in the artificial caries solution. The distance of dye penetration into the adjacent enamel, cementum/dentin, and tooth-resin interfaces was measured after immersion in 0.5% basic fuchsin dye for 24 h. The tooth-resin interfacial layer was investigated using SEM. Results. No dye penetration into the tooth-resin interface was found in Super-Bond D-Liner II Plus and AQ Bond groups which demonstrated a constant hybrid layer after a chemical challenge. The leakage distance at the cementum/dentin-resin interface of All-Bond 2, Clearfil Protect Bond, and non-adhesive amalgam (positive control) groups was significantly higher than the distance of dye penetration into the adjacent demineralized root surface (p<0.05). Conclusion. Caries associated with either amalgam or resin-composite restorations can be prevented using resin adhesives which can penetrate into the intact tooth substrate to form a stable hybrid layer. With caries-free restorations, tooth vitality may be conserved lifelong.

scholarly journals In vitro Study of the Structure and Adhesive Interface in Direct Restorations with Experimental Nanocomposite Materials and Adhesive Systems

2018 ◽  
Vol 55 (4) ◽  
pp. 620-625
Author(s):  
Anca Porumb ◽  
Adrian Almasi ◽  
Liana Todor ◽  
Cristian Adrian Ratiu ◽  
Gabriela Ciavoi ◽  
...  
Keyword(s):  
Clinical Importance ◽  
In Vitro Study ◽  
Adhesive System ◽  
Nanocomposite Materials ◽  
Variable Number ◽  
Adhesive Systems ◽  
Adhesive Interface ◽  
Chemistry Research ◽  
Self Etch

Using nanotechnology to produce composite materials it has been possible to obtain materials with similar or better mechanical properties than previous generation of microhybrids, and with exceptional aesthetics and chandelier due to the particularities of nanomaterials. At the same time, the improvement of adhesive techniques to enamel and dentin allowed the expansion of the area of direct composite restorations with a better prognostic over time.Eight carie-free molars were used and each of them was prepared with two class II cavities, which were filled using the C13 and C20 nanocomposites and the A1 and A2 experimental adhesive systems prepared at the Raluca Ripan Chemistry Research Institute. The teeth were divided into four groups of two teeth each, depending on the adhesive system and the composite material used. Scanning electron microscopy images (SEM) have described the adhesive interface and structure characteristics for the two nanocomposite materials and for the two studied adhesive systems.The studied nanocomposites have a variable number of porosities and air bubbles, with a clinical importance which is yet hard to establish.The experimental adhesives used produce a good interface and infiltration of the smear-layer but have not been visualized inside the dentinal canals.In vitro studies are necessary to evaluate the durability of adhesion in the case of self-etch adhesives in one or two steps.

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