scholarly journals Influence of surface treatment on shear bond strength of orthodontic brackets

2013 ◽  
Vol 18 (3) ◽  
pp. 54-62 ◽  
Author(s):  
Ione Helena Vieira Portella Brunharo ◽  
Daniel Jogaib Fernandes ◽  
Mauro Sayão de Miranda ◽  
Flavia Artese
Keyword(s):  
Bond Strength ◽  
Aluminum Oxide ◽  
Sodium Bicarbonate ◽  
Surface Treatment ◽  
Hydrofluoric Acid ◽  
Shear Bond Strength ◽  
Resin Composite ◽  
Orthodontic Brackets ◽  
Treatment Methods ◽  
Hybrid Resin

INTRODUCTION: The shear bond strength of orthodontic brackets bonded to micro-hybrid and micro-particulate resins under different surface treatment methods was assessed. METHODS: Two hundred and eighty test samples were divided into 28 groups (n = 10), where 140 specimens were filled with Durafill micro-particulate resin and 140 with Charisma composite. In 140 samples, a coupling agent (silane) was applied. The surface treatment methods were: Phosphoric and hydrofluoric acid etching, sodium bicarbonate and aluminum oxide blasting, stone and burs. A Universal Instron Machine was used to apply an occlusal shear force directly to the resin composite bracket surface at a speed of 0.5 mm/min. The means were compared using analysis of variance and multivariate regression to assess the interaction between composites and surface treatment methods. RESULTS: Means and standard deviations for the groups were: Sodium bicarbonate jet 11.27±2.78; burs 9.26±3.01; stone 7.95±3.67; aluminum oxide blasting 7.04±3.21; phosphoric acid 5.82±1.90; hydrofluoric acid 4.54±2.87, and without treatment 2.75±1.49. An increase of 1.94 MPa in shear bond strength was seen in Charisma groups. Silane agent application reduced the Charisma shear bond strength by 0.68 Mpa, but increased Durafill means for bicarbonate blasting (0.83), burs (0.98) and stone drilling (0.46). CONCLUSION: The sodium bicarbonate blasting, burs and stone drilling methods produced adequate shear bond strength and may be suitable for clinical use. The Charisma micro hybrid resin composite showed higher shear bond means than Durafill micro particle composite.

scholarly journals Bond strength of orthodontic brackets to polymethylmethacrylate: effect of the surface treatment and adhesive system

2021 ◽  
Vol 62 (1) ◽  
Author(s):  
Rita Cardoso ◽  
◽  
Joana Godinho ◽  
Luís Jardim ◽  
◽  
...  
Keyword(s):  
Bond Strength ◽  
Aluminum Oxide ◽  
Surface Treatment ◽  
Failure Mode ◽  
Shear Bond Strength ◽  
Adhesive System ◽  
Orthodontic Brackets ◽  
Control Group ◽  
Universal Adhesive ◽  
Machine Failure

Objectives: To evaluate the influence of the surface treatment and adhesive system on the shear bond strength and the failure mode of orthodontic brackets bonded to polymethylmethacrylate surfaces. Methods: Ninety metal brackets (n=15) were bonded to aged discs of polymethylmethacrylate SR Ivocron subjected to three surface conditions (no treatment; sandblasting with 50-μm aluminum oxide; roughening with a tungsten bur), using two combinations of adhesives (methylmethacrylate monomer + Transbond XT Primer; Scotchbond Universal Adhesive) followed by the composite Transbond XT. In the control group, metal brackets were bonded with Transbond XT to 15 human mandibular incisors. The specimens were thermocycled, stored in distilled water (37ºC, 7 days), and tested in shear, using an Instron universal machine. Failure mode was classified according to the adhesive remnant index using a stereomicroscope. The data were analyzed with an analysis of variance and posthoc tests (p<0.05). Results: Significant differences were found between the bracket bond strength to polymethylmethacrylate with different surface treatments (p<0.001). Sandblasting with aluminum oxide was superior to tungsten bur roughening. The adhesive system did not significantly influence the shear bond strength nor the failure mode (p=0.8415). All experimental groups showed lower bond strengths than the control group (p=0.1566). Conclusions: Mechanical surface treatment significantly influenced the bracket’s bond strength to polymethylmethacrylate. Sandblasting with aluminum oxide was the most effective mechanical treatment. The weakest adhesive link was found at the acrylic-adhesive interface. Orthodontic bonding to polymethylmethacrylate was weaker than bonding to enamel, regardless of the surface treatment and the adhesive used.

Effect of Er,Cr:YSGG Laser, Air Abrasion, and Silane Application on Repaired Shear Bond Strength of Composites

2013 ◽  
Vol 38 (3) ◽  
pp. E58-E66 ◽  
Author(s):  
SD Cho ◽  
P Rajitrangson ◽  
BA Matis ◽  
JA Platt
Keyword(s):  
Bond Strength ◽  
Aluminum Oxide ◽  
Surface Treatment ◽  
Shear Bond Strength ◽  
Resin Composite ◽  
Silica Coating ◽  
Surface Treatments ◽  
Control Group ◽  
Resin Composites ◽  
Air Abrasion

SUMMARY Aged resin composites have a limited number of carbon-carbon double bonds to adhere to a new layer of resin. Study objectives were to 1) evaluate various surface treatments on repaired shear bond strength between aged and new resin composites and 2) to assess the influence of a silane coupling agent after surface treatments. Methods Eighty disk-shape resin composite specimens were fabricated and thermocycled 5000 times prior to surface treatment. Specimens were randomly assigned to one of the three surface treatment groups (n=20): 1) air abrasion with 50-μm aluminum oxide, 2) tribochemical silica coating (CoJet), or 3) Er,Cr:YSGG (erbium, chromium: yttrium-scandium-gallium-garnet) laser or to a no-treatment control group (n=20). Specimens were etched with 35% phosphoric acid, rinsed, and dried. Each group was divided into two subgroups (n=10): A) no silanization and B) with silanization. The adhesive agent was applied and new resin composite was bonded to each conditioned surface. Shear bond strength was evaluated and data analyzed using two-way analysis of variance (ANOVA). Results Air abrasion with 50-μm aluminum oxide showed significantly higher repair bond strength than the Er,Cr:YSGG laser and control groups. Air abrasion with 50-μm aluminum oxide was not significantly different from tribochemical silica coating. Tribochemical silica coating had significantly higher repair bond strength than Er,Cr:YSGG laser and the control. Er,Cr:YSGG laser and the control did not have significantly different repair bond strengths. Silanization had no influence on repair bond strength for any of the surface treatment methods. Conclusion Air abrasion with 50-μm aluminum oxide and tribochemical silica followed by the application of bonding agent provided the highest repair shear bond strength values, suggesting that they might be adequate methods to improve the quality of repairs of resin composites.

scholarly journals Effect of surface treatment on the shear bond strength of a resin-based cement to porcelain

2006 ◽  
Vol 17 (4) ◽  
pp. 290-295 ◽  
Author(s):  
Marcos Paulo Nagayassu ◽  
Luciana Keiko Shintome ◽  
Eduardo Shigueyuki Uemura ◽  
José Eduardo Junho de Araújo
Keyword(s):  
Bond Strength ◽  
Surface Treatment ◽  
Hydrofluoric Acid ◽  
Shear Bond Strength ◽  
In Vitro Study ◽  
Resin Cement ◽  
Vitro Study ◽  
Acid Etching ◽  
And Control

The purpose of this in vitro study was to evaluate the effect of different surface treatments on the shear bond strength of a resin-based cement to porcelain. Sixty pairs of 50% aluminous porcelain discs were fabricated. In each pair, one disc measured 6 mm in diameter X 3 mm thickness (A) and the other measured 3 mm in diameter X 3mm thickness (B). The specimens were randomly assigned to 6 groups (n=10 pairs of discs), according to the surface treatment: etching with 10% hydrofluoric acid for 2 or 4min (G1 and G2); 50-µm particle aluminum oxide sandblasting for 5 s (G3); sandblasting followed by etching for 2 or 4min (G4 and G5) and control - no treatment (G6). A silane agent was applied to the treated surface of both discs of each pair. Bistite II DC dual-cure resin cement was applied and the B discs were bonded to their respective A discs. Specimens were stored in distilled water at 37ºC for 24 h and were tested in shear strength at a crosshead speed of 2 mm/min. Means in MPa were: G1: 14.21 ± 4.68; G2: 8.92 ± 3.02; G3: 10.04 ± 2.37; G4: 12.74 ± 5.15; G5: 10.99 ± 3.35; G6: 6.09 ± 1.84. Data were compared by one-way ANOVA and Tukey's test at 5% significance level. Bond strength recorded after 2-min acid etching was significantly higher than 4-min etching (p<0.05) and control (p<0.05), but did not differ significantlyfrom sandblasting alone (p>0.05) or followed by etching for 2 or 4 min (p>0.05). Within the limitations of an in vitro study, it may be concluded that 2-min hydrofluoric acid etching produced a favorable micromechanical retention that enhanced resin cement bond strength to porcelain.

scholarly journals Evaluation of shear bond strength of composite to porcelain according to surface treatment

2003 ◽  
Vol 14 (2) ◽  
pp. 132-135 ◽  
Author(s):  
Claudia Minami Kussano ◽  
Gerson Bonfante ◽  
José Gilmar Batista ◽  
João Henrique Nogueira Pinto
Keyword(s):  
Bond Strength ◽  
Surface Treatment ◽  
Hydrofluoric Acid ◽  
Shear Bond Strength ◽  
Room Temperature ◽  
Force Load ◽  
Group 4 ◽  
Group 3 ◽  
Group 2 ◽  
Group 1

This study evaluated the shear bond strength of porcelain/composite using 40 metal + porcelain + composite cylindrical specimens divided into 4 groups, according to porcelain surface treatment: 1) no treatment, 2) mechanical retentions performed with diamond burs, 3) etching with phosphoric acid+silane, and 4) etching with hydrofluoric acid+silane. After being stored in distilled water at room temperature for one week, the specimens were submitted to a shear force (load) and the data were analyzed statistically (ANOVA). The means (in Mpa) of the groups were: 4.71 (group 1); 4.81 (group 2); 11.76 (group 3); 11.07 (group 4). There were no statistically significant differences between groups 1 and 2 and between groups 3 and 4.

scholarly journals Effect of Acid Etching, Silane and Thermal Cycling on the Bond Strength of Metallic Brackets to Ceramic

2016 ◽  
Vol 27 (6) ◽  
pp. 734-738 ◽  
Author(s):  
Natália Regina Santos de Matos ◽  
Ana Rosa Costa ◽  
Heloísa Cristina Valdrighi ◽  
Américo Bortolazzo Correr ◽  
Silvia Amélia Vedovello ◽  
...  
Keyword(s):  
Bond Strength ◽  
Thermal Cycling ◽  
Surface Treatment ◽  
Hydrofluoric Acid ◽  
Shear Bond Strength ◽  
Deionized Water ◽  
Acid Etching ◽  
Ceramic Surface ◽  
Adhesive Remnant Index ◽  
Post Hoc

Abstract The aim of this study was to evaluate the effect of silanes, thermal cycling and acid etching on the shear bond strength (SBS) of metallic brackets to feldspathic ceramic. Feldspathic ceramic cylinders (Groups 1, 2, 5 and 6) were etched for 60 s with 10% hydrofluoric acid and Groups 3, 4, 7 and 8, without acid etching. Two layers of silane Clearfil Ceramic Primer (CCP, Groups 1 to 4) and two layers of RelyX Ceramic Primer (RCP, groups 5 to 8) were applied and dried for 60 s. Brackets were bonded to the cylinders with Transbond XT and light-activated for 40 s with Bluephase G2. All specimens were stored in deionized water at 37 °C for 24 h, and the specimens of groups 1, 3, 5 and 7 were submitted to 7,000 thermal cycles (5 °C/55 °C). After storage, the SBS test was performed at a crosshead speed of 1 mm/min. Data were subjected to three-way ANOVA and Tukey's post hoc test (α=0.05). The adhesive remnant index (ARI) was evaluated at 8x magnification. The SBS of CCP was significantly greater than of RCP (p<0.05), with or without thermal cycling. Thermal cycling significantly reduced the SBS (p<0.05). The groups submitted to acid etching showed significantly higher SBS than those without acid etching (p<0.05). In conclusion, thermal cycling reduced SBS for all groups. The best ceramic surface treatment for bracket bonding was achieved by acid etching and CCP silane. The ARI results showed predominance of score 0 for all groups.

scholarly journals Assessment the Bond Strength of Ceramic Brackets to CAD/CAM Nanoceramic Composite and Interpenetrating Network Composite after Different Surface Treatments

2018 ◽  
Vol 2018 ◽  
pp. 1-6 ◽  
Author(s):  
Mustafa Mehmet Özarslan ◽  
Özlem Üstün ◽  
Ulviye Sebnem Buyukkaplan ◽  
Çağatay Barutcigil ◽  
Nurullah Türker ◽  
...  
Keyword(s):  
Bond Strength ◽  
Surface Treatment ◽  
Hydrofluoric Acid ◽  
Shear Bond Strength ◽  
Surface Treatments ◽  
Interpenetrating Network ◽  
Bonding Performance ◽  
Cad Cam ◽  
Ceramic Brackets ◽  
New Generation

Adult orthodontics may confront problems related to the bonding performance of orthodontic brackets to new generation restorative materials used for crown or laminate restorations. The aim of the present study was to investigate the shear bond strength of ceramic brackets to two new generation CAD/CAM interpenetrating network composite and nanoceramic composite after different surface treatments. Er,Cr:YSGG Laser, hydrofluoric acid (9%), sandblasting (50 μm Al2O3), and silane were applied to the surfaces of 120 CAD/CAM specimens with 2 mm thickness and then ceramic brackets were bonded to the treated surfaces of the specimens. Bond strength was evaluated using the shear bond strength test. According to the results, CAD/CAM block types and surface treatment methods have significant effects on shear bond strength. The lowest bond strength values were found in the specimens treated with silane (3.35 ± 2.09 MPa) and highest values were found in the specimens treated with sandblast (8.92 ± 2.77 MPa). Sandblasting and hydrofluoric acid surface treatment led to the most durable bonds for the two types of CAD/CAM blocks in the present study. In conclusion, different surface treatments affect the shear bond strength of ceramic brackets to CAD/CAM interpenetrating network composite and nanoceramic composite. Among the evaluated treatments, sandblasting and hydrofluoric acid application resulted in sufficient bonding strength to ceramic brackets for both of the CAD/CAM materials.

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