scholarly journals Effect of water storage on microshear bond strength of four dental adhesive systems to dentin

2015 ◽  
Vol 3 (2) ◽  
pp. 626
Author(s):  
Robinson Viegas Montenegro ◽  
Hugo Lemes Carlo ◽  
André Ulisses Dantas Batista ◽  
Sheyla Christinne Lira Montenegro ◽  
Ohana Rodrigues Farias

AIM: To evaluate the microshear bond strength of 4 dental adhesive systems after 1 year-water storage. MATERIAL AND METHODS: The sample consisted of 120 cylinders of composite, obtained from 24 bovine incisors, which were divided into four experimental groups: G1-Scotchbond Multi-Purpose, G2-Single Bond 2, G3-Clearfil SE Bond, G4-Adper Easy One and two storage times in distilled water: T0 - 24h and T1 - 1 year. A bivariate analysis was performed using the ANOVA and Tukey test (α=0.05). Results were evaluated inter-and intra-group in both times. RESULTS: After 24 hours, G1T0 (39.68A ± 11.55) showed higher bond strength (MPa) followed by G2T0 (22.71B ± 4.07), G3T0 (18.94BC ± 7.29) and G4T0 (13.30C ± 3.94). After 1 year of storage only G1T1 (33.95A ± 6.35) and G3T1 (13.59BC ± 2.63) maintained the bond strength values (p ≥ 0.05), while G2T1 (10.62C ± 4.32) and G4T1 (4.49D ± 2.49) presented a decrease in this values. CONCLUSION: The hydrophobic two-step adhesive systems maintained the bond strength after 1-year water storage.

Author(s):  
Sara Valizadeh ◽  
Aida Moradi ◽  
Mansooreh Mirazei ◽  
Hooman Amiri ◽  
Mohammad Javad Kharazifard

Objectives: The aim of this study was to compare the microshear bond strength (µSBS) of various adhesive systems to dentin. Materials and Methods: In this in vitro experimental study, 60 sound human third molars were divided into four groups. Dentin discs were prepared of middle-third dentin measuring 4 mm in diameter and 2 mm in thickness. Dentin surfaces were bonded with one of the four types of adhesives: (A) Single Bond (3M ESPE), Scotchbond Universal (3M ESPE) in etch and rinse (B) and self-etch (C) modes and (D) Clearfil SE Bond (Kuraray Noritake Dental). After the application of adhesive systems according to the manufacturers’ instructions, composite cylinders (Vit-l-escence) were bonded to dentin surfaces. The μSBS test was performed using a universal testing machine at a crosshead speed of 1 mm/min. Data were analyzed with one-way ANOVA and Tukey’s test (α=0.05). Results: The µSBS was the highest in self-etch Scotchbond Universal (15.8±6.08 MPa) followed by Clearfil SE Bond (15.24±4.6 MPa), etch and rinse Scotchbond Universal (11.68±4.07MPa) and Single Bond (11.24±3.74 MPa). A significant difference was only found between Single Bond and etch and rinse Scotchbond Universal groups (P=0.04). Conclusion: Based on the results of this study, application of Scotchbond Universal in self-etch mode provides a reliable bond to dentin.


Author(s):  
Sara Valizadeh ◽  
Aida Moradi ◽  
Mansooreh Mirazei ◽  
Hooman Amiri ◽  
Mohammad Javad Kharazifard

Objectives: The aim of this study was to compare the microshear bond strength (µSBS) of various adhesive systems to dentin. Materials and Methods: In this in vitro experimental study, 60 sound human third molars were divided into four groups. Dentin discs were prepared of middle-third dentin measuring 4 mm in diameter and 2 mm in thickness. Dentin surfaces were bonded with one of the four types of adhesives: (A) Single Bond (3M ESPE), Scotchbond Universal (3M ESPE) in etch and rinse (B) and self-etch (C) modes and (D) Clearfil SE Bond (Kuraray Noritake Dental). After the application of adhesive systems according to the manufacturers’ instructions, composite cylinders (Vit-l-escence) were bonded to dentin surfaces. The μSBS test was performed using a universal testing machine at a crosshead speed of 1 mm/min. Data were analyzed with one-way ANOVA and Tukey’s test (α=0.05). Results: The µSBS was the highest in self-etch Scotchbond Universal (15.8±6.08 MPa) followed by Clearfil SE Bond (15.24±4.6 MPa), etch and rinse Scotchbond Universal (11.68±4.07MPa) and Single Bond (11.24±3.74 MPa). A significant difference was only found between Single Bond and etch and rinse Scotchbond Universal groups (P=0.04). Conclusion: Based on the results of this study, application of Scotchbond Universal in self-etch mode provides a reliable bond to dentin.


2015 ◽  
Vol 26 (6) ◽  
pp. 642-647 ◽  
Author(s):  
Enio Marcos da Silva ◽  
Daniel Hatschbach Glir ◽  
Allana Walesca Martins Castanho Gill ◽  
Allan Fernando Giovanini ◽  
Adilson Yoshio Furuse ◽  
...  

The aim of this study was to evaluate the effect of 2% chlorhexidine (CHX) application during the bonding protocol on microshear bond strength of two adhesive systems, after storage in different media. Seventy-two human molars had their crowns cut in half and embedded in PVC cylinders with acrylic resin. The specimens were randomly divided into experimental groups (n=12) according to the adhesive system (Ambar and Single Bond 2), use of CHX in the bonding protocol, and time interval (24 h and 15 days) in the storage media (distilled water, mineral oil and 1% sodium hypochlorite - NaOCl). Adhesive systems were applied in accordance to manufacturers' recommendations, with or without the use of CHX, and resin composite (Z350 XT) cylinders were placed on the hybridized dentin. After photoactivation, the specimens were stored in distilled water, mineral oil and 1% NaOCl for 24 h and 15 days. Microshear bond strength was determined at a crosshead speed of 0.5 mm/min until fracture. The bond strength data were analyzed statistically by 4-way ANOVA and Tukey's test (α=5%). Use of CHX in the bonding protocol did not cause loss of bond strength in any of the evaluated situations, irrespective of time and storage medium. The storage medium had no influence on bond strength values after 15 days when the bond protocol without CHX application was used. However, the use of CHX in the protocol influenced negatively the bond strength values for Single Bond 2 after 15 days storage in distilled water and 1% NaOCl.


2016 ◽  
Vol 41 (3) ◽  
pp. E57-E63 ◽  
Author(s):  
JD Theobaldo ◽  
A Catelan ◽  
U Rodrigues-Filho ◽  
GM Marchi ◽  
DANL Lima ◽  
...  

SUMMARY Objective: To evaluate the microshear bond strength of composite resin restorations in dental blocks with or without exposure to cigarette smoke. Method: Eighty bovine dental blocks were divided into eight groups (n=10) according to the type of adhesive (Scotchbond Multi-Purpose, 3M ESPE, St Paul, MN, USA [SBMP]; Single Bond 2, 3M ESPE [SB]; Clearfil SE Bond, Kuraray Medical Inc, Okayama, Japan [CSEB]; Single Bond Universal, 3M ESPE [SBU]) and exposure to smoke (no exposure; exposure for five days/20 cigarettes per day). The adhesive systems were applied to the tooth structure, and the blocks received a composite restoration made using a matrix of perforated pasta. Data were statistically analyzed using analysis of variance and Tukey test (α<0.05). Results: For enamel, there was no difference between the presence or absence of cigarette smoke (p=0.1397); however, there were differences among the adhesive systems (p<0.001). CSEB showed higher values and did not differ from SBU, but both were statistically different from SB. The SBMP showed intermediate values, while SB demonstrated lower values. For dentin, specimens subjected to cigarette smoke presented bond strength values that were lower when compared with those not exposed to smoke (p<0.001). For the groups without exposure to cigarette smoke, CSEB showed higher values, differing from SBMP. SB and SBU showed intermediary values. For the groups with exposure to cigarette smoke, SBU showed values that were higher and statistically different from SB and CSEB, which presented lower values of bond strength. SBMP demonstrated an intermediate value of bond strength. Conclusion: The exposure of dentin to cigarette smoke influenced the bonding strength of adhesives, but no differences were noted in enamel.


2016 ◽  
Vol 17 (5) ◽  
pp. 399-407
Author(s):  
Girish Kulkarni ◽  
Vinay K Mishra

ABSTRACT Aims The purpose of this study was to compare the effect of enamel wetness on microshear bond strength using different adhesive systems. Objectives To evaluate microshear bond strength of three bonding agents on dry enamel; to evaluate microshear bond strength of three bonding agents on wet enamel; and to compare microshear bond strength of three different bonding agents on dry and wet enamel. Materials and methods Sixty extracted noncarious human premolars were selected for this study. Flat enamel surfaces of approximately 3 mm were obtained by grinding the buccal surfaces of premolars with water-cooled diamond disks. This study evaluated one etch-and-rinse adhesive system (Single Bond 2) and two self-etching adhesive systems (Clearfil SE Bond and Xeno-V). The specimens were divided into two groups (n = 30). Group I (dry) was air-dried for 30 seconds and in group II (wet) surfaces were blotted with absorbent paper to remove excess water. These groups were further divided into six subgroups (n = 10) according to the adhesives used. The resin composite, Filtek Z 250, was bonded to flat enamel surfaces that had been treated with one of the adhesives, following the manufacturer's instructions. After being stored in water at 37°C for 24 hours, bonded specimens were stressed in universal testing machine (Fig. 3) at a crosshead speed of 1 mm/min. The data were evaluated with one-way and two-way analysis of variance (ANOVA), t-test, and Tukey's Multiple Post hoc tests (α = 0.05). Results The two-way ANOVA and Tukey's Multiple Post hoc tests showed significant differences among adhesive systems, but wetness did not influence microshear bond strength (p = 0.1762). The one-way ANOVA and t-test showed that the all-in-one adhesive (Xeno-V) was the only material influenced by the presence of water on the enamel surface. Xeno-V showed significantly higher microshear bond strength when the enamel was kept wet. Single Bond 2 adhesive showed significantly higher microshear bond strength as compared with Xeno-V adhesive but no significant difference when compared with Clearfil SE Bond adhesive in dry enamel. Single Bond 2 adhesive showed no significant difference in microshear bond strength as compared with self-etching adhesive systems (Clearfil SE Bond and Xeno-V), when the enamel was kept wet. Conclusion From the findings of the results, it was concluded that self-etching adhesives were not negatively affected by the presence of water on the enamel surface. Clinical significance The all-in-one adhesive showed different behavior depending on whether the enamel surface was dry or wet. So the enamel surface should not be desiccated, when self-etching adhesives are used. How to cite this article Kulkarni G, Mishra VK. Enamel Wetness Effects on Microshear Bond Strength of Different Bonding Agents (Adhesive Systems): An in vitro Comparative Evaluation Study. J Contemp Dent Pract 2016;17(5):399-407.


2016 ◽  
Author(s):  
Patricia F. Cassimiro-Silva ◽  
Denise M. Zezell ◽  
Gabriela Q. d. M. Monteiro ◽  
Carolina Benetti ◽  
Carlos de Paula Eduardo ◽  
...  

2013 ◽  
Vol 16 (4) ◽  
pp. 84
Author(s):  
Cláudio Hideki Kubo ◽  
Ana Paula Martins Gomes ◽  
Paloma Grasso Madureira ◽  
Eduardo Galera Da Silva ◽  
Frederico Canato Martinho ◽  
...  

<p><strong>Objective: </strong>This study evaluated the effect of rootperforations on the bond strength of fiberglassposts cemented to the root canal with two adhesivesystems and resin cement. <strong>Material and Methods:</strong>Forty single-rooted human teeth received endodontictreatment and were prepared for the cementationof fiberglass posts (Exacto Mini, Angelus). Theteeth were divided into four experimental groups(n = 10) according to the root condition (with orwithout perforation) and the adhesive system used:G1: without perforation + Adper Single Bond 2(3M ESPE), G2: without perforation + Clearfil SEBond (Kuraray), G3: with perforation + AdperSingle Bond 2, G4: with perforation + Clearfil SEBond. The perforation was executed on the rootsurface with a diamond bur and sealed with whitemineral trioxide aggregate (MTA). The specimenswere sectioned and a push-out test was carriedout (1 mm/min speed and 50 kgf). The data werestatistically analyzed by ANOVA and Tukey Test(5%). <strong>Results: </strong>Adper Single Bond 2 promoted thegreatest values of bond strength to the roots withoutroot perforation. The presence of root perforation ledto the reduction in bond strength values regardlessof the bonding system used (p &lt; 0.05). <strong>Conclusion:</strong>The root perforations caused a direct effect on thebond strength of the fiberglass posts cemented byreducing the bond strength values to the root dentinregardless of the adhesive system used.</p><p>Keywords<br />Adhesion; Cementation; Dental adhesives; Dental cements; Fiberglass pins.</p>


2012 ◽  
Vol 06 (02) ◽  
pp. 169-177
Author(s):  
Gislaine Cristine Martins ◽  
Alfonso Sánchez-Ayala ◽  
Paulo Henrique Perlatti D’Alpino ◽  
Abraham Lincoln Calixto ◽  
João Carlos Gomes ◽  
...  

ABSTRACTObjectives: Objective: To evaluate the effect of thermo-mechanical cycling (TMC) on the microleakage (μL) and axial gap width (AG) of Class V bonded restorations in premolars using self-etching adhesive systems. The bond strength of composite restorations to dentin (μTBS) using the same adhesives was also evaluated in third molars after water storage: 24 h and 6 months. The research hypotheses were tested for the results of two self-etching adhesives in comparison when a conventional two-step adhesive was used: (1) the μL and AG would be lower, regardless of TMC; (2) the μTBS of self-etching adhesives would be higher, irrespective of evaluation times.Methods: Sixty Class V composite restorations were made in 30 premolars and bonded with Adper Single Bond 2 (ASB2), AdheSE (ASE), and Adper Prompt L-Pop (APL-P) (n=20). Dentin μL and AG were immediately measured for half of the sample. The other half was evaluated after TMC. Eighteen third molars were also selected and bonded using the same adhesives to test the μTBS to dentin. Specimens were evaluated after 24 h and 6 months of water storage.Results: No differences in μL and AG were found among the groups (P>.05). The μTBS mean values were: ASB2>ASE>APL-P (P<.05); only Adper Single Bond 2 presented a significantly lower μTBS after water storage (P<.05)Conclusions: The bonding approach does not influence the microleakage and interfacial gap extension. Despite the decrease in the mean values, the bond strength to dentin of the conventional, two-step adhesive remains high after 6 months of water storage. (Eur J Dent 2012;6:169-177)


2017 ◽  
Vol 42 (3) ◽  
pp. 284-296 ◽  
Author(s):  
EC Martini ◽  
SO Parreiras ◽  
MF Gutierrez ◽  
AD Loguercio ◽  
A Reis

SUMMARY Objectives: The aim of this study was to investigate the effect of different protocols of 17% ethylene diamine tetra-acetic acid (EDTA) conditioning on the etching pattern and immediate bond strength of universal adhesives to enamel and sclerotic dentin. Methods and Materials: Forty bovine teeth with sclerotic dentin and 20 human third molars were randomly divided into eight groups resulting from the combination of the main factors surface treatment (none, two-minute EDTA conditioning manual application, 30-second EDTA manual application, 30-second EDTA sonic application) and adhesives systems (Scotchbond Universal Adhesive [SBU] and Prime & Bond Elect [PBE]). Resin-dentin and enamel-dentin bond specimens were prepared and tested under the microtensile bond strength (μTBS) and microshear bond strength (μSBS) tests, respectively. The etching pattern produced on the unground enamel and the sclerotic dentin surfaces under the different protocols and adhesive systems was evaluated under scanning electron microscopy. Results: For enamel, only the main factor adhesive was significant (p&lt;0.0001), with SBU showing the highest μSBS. In sclerotic dentin, the lowest mean was observed for the group without EDTA application and the highest mean in the group with EDTA application with the sonic device for 30 seconds. Regardless of the EDTA protocol, the highest means of μTBS were observed for SBU (p&lt;0.05). Conclusions: EDTA conditioning improves the bonding performance of universal adhesives in the self-etch mode on sclerotic dentin, mainly when applied for 30 seconds with the aid of a sonic device. EDTA pretreatment also improves the retentive etching pattern of enamel, but it does not result in higher enamel bond strength.


2007 ◽  
Vol 31 (1) ◽  
pp. 35-40 ◽  
Author(s):  
Carla Miranda ◽  
Luiz Henrique Maykot Prates ◽  
Ricardo de Souza Vieira ◽  
Maria Cristina Marino Calvo

The aims of this study were to evaluate the shear bond strength (SBS) of four adhesive systems applied to primary dentin and enamel and verify, after SBS testing, the failure mode of the adhesive interface. Sixty extracted sound primary molars were selected and crowns were sectioned in a mesial-distal direction. Specimens were randomly assigned into two groups (adhesion to enamel and adhesion to dentin) and then subdivided into four subgroups according to the adhesive system (n=15): Scotchbond Multi-Purpose (SMP) – Single Bond (SB) – Clearfil SE Bond (and Adper Prompt LPop (APL) – SBS tests were performed and the obtained values were statistically analyzed using ANOVA and Tukey tests (p&lt;0.05). The failure mode analysis was performed with a Scanning Electron Microscope (XL-30, Philips). SBS mean values on enamel were [MPa (SD)]: SMP – 27.89 (7.49); SB – 23.92 (8.8); CSB – 24.36 (6.69); APL – 25.96 (4.08); and on dentin: SMP – 17.29 (4.25); SB – 18.2 (8.74); CSB – 16.13 (7.14); APL – 6.04 (3.35). The predominant failure mode was cohesive (primarily of the bonding agent). On enamel SBS was statistically similar for all four adhesives. On dentin SBS of APL was lower than the other tested adhesives.


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