Shear Bond Strength of Different Adhesive Systems to Primary Dentin and Enamel

2007 ◽  
Vol 31 (1) ◽  
pp. 35-40 ◽  
Author(s):  
Carla Miranda ◽  
Luiz Henrique Maykot Prates ◽  
Ricardo de Souza Vieira ◽  
Maria Cristina Marino Calvo

The aims of this study were to evaluate the shear bond strength (SBS) of four adhesive systems applied to primary dentin and enamel and verify, after SBS testing, the failure mode of the adhesive interface. Sixty extracted sound primary molars were selected and crowns were sectioned in a mesial-distal direction. Specimens were randomly assigned into two groups (adhesion to enamel and adhesion to dentin) and then subdivided into four subgroups according to the adhesive system (n=15): Scotchbond Multi-Purpose (SMP) – Single Bond (SB) – Clearfil SE Bond (and Adper Prompt LPop (APL) – SBS tests were performed and the obtained values were statistically analyzed using ANOVA and Tukey tests (p<0.05). The failure mode analysis was performed with a Scanning Electron Microscope (XL-30, Philips). SBS mean values on enamel were [MPa (SD)]: SMP – 27.89 (7.49); SB – 23.92 (8.8); CSB – 24.36 (6.69); APL – 25.96 (4.08); and on dentin: SMP – 17.29 (4.25); SB – 18.2 (8.74); CSB – 16.13 (7.14); APL – 6.04 (3.35). The predominant failure mode was cohesive (primarily of the bonding agent). On enamel SBS was statistically similar for all four adhesives. On dentin SBS of APL was lower than the other tested adhesives.

2015 ◽  
Vol 5 (3) ◽  
pp. 153-157
Author(s):  
Manoj Hans ◽  
Abhinav Sharma ◽  
Shashit Shetty

ABSTRACT Background The purpose of this study was to evaluate the shear bond strength (SBS) of two different adhesives to normal and deproteinized dentin at an interval of 24 hours and 6 months. Materials and Methods Sixty human molars were sectioned and embedded in acrylic resin. Enamel was worn out and dentin was exposed over which acid etching was performed and the specimens were divided into 12 groups (n = 10) depending on the adhesive system used, the dentin treatment performed and the length of evaluation. A resin composite was inserted over the prepared area followed by assessment for shear bond strength evaluation. Results The application of Sodium hypochlorite (NaOCl) significantly increased the SBS values of prime and bond NT but for adper single bond it was decreased. The means values of SBS standard deviation (SD) in MPa for adhesive systems with 5% NaOCI for 60 seconds, 120 seconds and without NaOCl treatment were: prime and bond NT = 12.48 (1.25), 13.01 (1.00) and 17.74 (4.26) and for adper single bond = 10.92 (1.65), 10.96 (2.45) and 7.57 (1.45). Shear bond strength after storage time of 6 months was decreased significantly. Conclusion According to the statistical analysis, the results only partly supported the hypotheses and greatly depend on the composition of adhesive system. How to cite this article Sharma A, Shetty S, Hans M. Shear Bond Strength Evaluation of Two Adhesive Systems Applied to Etched and Deproteinized Dentin: A Longitudinal Study. J Contemp Dent 2015;5(3):153-157.


2017 ◽  
Vol 28 (5) ◽  
pp. 624-631
Author(s):  
Isabela Sousa de Araújo ◽  
Célio Jesus do Prado ◽  
Luís Henrique Araújo Raposo ◽  
Carlos José Soares ◽  
Rayssa Ferreira Zanatta ◽  
...  

Abstract The aim of this study was to evaluate the degree of conversion, color stability, chemical composition, and bond strength of a light-cured resin cement contaminated with three different hemostatic solutions. Specimens were prepared for the control (uncontaminated resin cement) and experimental groups (resin cement contaminated with one of the hemostatic solutions) according to the tests. For degree of conversion, DC (n = 5) and color analyses (n = 10), specimens (3 mm in diameter and 2 mm thick) were evaluated by Fourier transform infrared spectroscopy (FTIR) and CIELAB spectrophotometry (L*, a*, b*), respectively. For elemental chemical analysis (n = 1), specimens (2 mm thick and 6 mm in diameter) were evaluated by x-ray energy-dispersive spectroscopy (EDS). The bond strengths of the groups were assessed by the microshear test (n = 20) in a leucite-reinforced glass ceramic substrate, followed by failure mode analysis by scanning electron microscopy (SEM). The mean values, except for the elemental chemical evaluation and failure mode, were evaluated by ANOVA and Tukey’s HSD test. The color stability was influenced by storage time (p<0.001) and interaction between contamination and storage time (p<0.001). Hemostop and Viscostat Clear contamination did not affect the DC, however Viscostat increased the DC. Bond strength of the resin cement to ceramic was negatively affected by the contaminants (p<0.001). Contamination by hemostatic agents affected the bond strength, degree of conversion, and color stability of the light-cured resin cement tested.


2012 ◽  
Vol 3 (2) ◽  
pp. 176-179
Author(s):  
Daphne Câmara Barcellos ◽  
Cesar Rogério Pucci ◽  
Maria Filomena Rocha Lima Huhtala ◽  
Eduardo Bresciani ◽  
Daniel Gomes Duarte ◽  
...  

ABSTRACT Purpose The objective of this study was to evaluate the influence of the Grander technology on the shear bond strength of total-etch adhesive system Single Bond 2 to dentin. Materials and methods Forty bovine incisors were used. They were sectioned and the buccal surfaces worn down with abrasive paper. Acid etching was performed, and the specimens were divided into two groups (n = 20): Group G1—Single Bond 2 adhesive system (3M ESPE) under normal conditions; group G2—Single Bond 2 adhesive system modified by physical contact for 48 hours with the flexible unit Grander system. The resin composite was inserted with the aid of a metallic matrix over the prepared area. After the mechanical shear test, data were submitted to the statistical t-test (5%). The t-test showed that the results for G1 and G2 were similar (p > 0.05). The mean values (± SD) were: G1—6.66 (± 2.40); G2—5.26 (± 2.15). Conclusion Grander technology did not influence the initial shear bond strength of the Single Bond 2 adhesive system to dentin. How to cite this article Duarte DG, de Paiva Gonçalves SE, Barcellos DC, Huhtala MFRL, Bresciani E, Pucci CR. Evaluation of Shear Bond Strength of a Grander-Modified Adhesive System to Bovine Dentin. World J Dent 2012;3(2):176-179.


2021 ◽  
Vol 24 (2) ◽  
Author(s):  
Fateme Vasei ◽  
Farahnaz Sharafeddin

Objective: To assess the shear bond strength (SBS) of resin composite to deep dentin, using 1 and 2.5% chitosan pretreatment as well as different adhesive systems. Material and Methods: 80 human maxillary molars were randomly divided to eight groups according to the type of adhesive system and dentin pretreatment (n = 10): I) two-step self-etch system (Clearfil SE bond); II) two-step etch-andrinse system (Adper single bond 2); III) 2.5% chitosan + Clearfil SE bond; IV) 2.5% chitosan +etch + Adper single bond 2; V) etch + 2.5% chitosan + Adper single bond 2; VI) 1% chitosan + Clearfil SE bond; VII) 1% chitosan + etch + Adper single bond 2; VIII) etch + 1% chitosan + Adper single bond 2 (chitosan solution (w/v): 2.5 g and 1 g of chitosan (Sigma Aldrich, USA) was dissolved in 100 ml of 1% acetic acid). Plastic molds were positioned on dentin and filled with composite (Z350, 3M ESPE, USA). SBS (MPa) was tested using a universal testing machine. ANOVA tests, Tukey’s test, and independent t test were used to analyze data (p < 0.05). Results: The highest SBS value among self-etch groups was observed with 1% chitosan (p = 0.001). In the etch-and-rinse group, the SBS of 1% chitosan was significantly lower than the other groups. Chitosan treatment following acid etching led to higher SBS in comparison to when chitosan was applied before etching, with the significant difference in 1% concentration (p = 0.030). A predominance of mix fractures was observed in dentin. Conclusion: Improved dentin bond strength can be achieved through immediate dentin pretreatment with 1% chitosan in self-etch adhesive systems. Chitosan Pretreatment may not be advantageous for etch-and-rinse adhesive systems. Keywords Adhesive system; Chitosan; Deep dentin; Shear strength.


2017 ◽  
Vol 2017 ◽  
pp. 1-7 ◽  
Author(s):  
Maurizio D’Amario ◽  
Chiara Piccioni ◽  
Stefano Di Carlo ◽  
Francesca De Angelis ◽  
Silvia Caruso ◽  
...  

Aim of this study was to investigate a specific airborne particle abrasion pretreatment on dentin and its effects on microtensile bond strengths of four commercial total-etch adhesives. Midcoronal occlusal dentin of extracted human molars was used. Teeth were randomly assigned to 4 groups according to the adhesive system used: OptiBond FL (FL), OptiBond Solo Plus (SO), Prime & Bond (PB), and Riva Bond LC (RB). Specimens from each group were further divided into two subgroups: control specimens were treated with adhesive procedures; abraded specimens were pretreated with airborne particle abrasion using 50 μm Al2O3before adhesion. After bonding procedures, composite crowns were incrementally built up. Specimens were sectioned perpendicular to adhesive interface to produce multiple beams, which were tested under tension until failure. Data were statistically analysed. Failure mode analysis was performed. Overall comparison showed significant increase in bond strength (p<0.001) between abraded and no-abraded specimens, independently of brand. Intrabrand comparison showed statistical increase when abraded specimens were tested compared to no-abraded ones, with the exception of PB that did not show such difference. Distribution of failure mode was relatively uniform among all subgroups. Surface treatment by airborne particle abrasion with Al2O3particles can increase the bond strength of total-etch adhesives.


2021 ◽  
Vol 9 (12) ◽  
pp. 140
Author(s):  
Ahmed M. Ismail ◽  
Christoph Bourauel ◽  
Ahmed ElBanna ◽  
Tarek Salah Eldin

Shear bond strength (SBS) testing is a commonly used method for evaluating different dental adhesive systems. Failure mode analysis provides valuable information for better interpretation of bond strength results. The aim of this study was to evaluate the influence of specimen dimension and loading technique on shear bond strength and failure mode results. Eighty macro and micro flowable composite cylindrical specimens of 1.8 and 0.8 mm diameter, respectively, and 1.5 mm length were bonded to dentinal substrate. Four study groups were created (n = 20): Macroshear wireloop, Gp1; Microshear wireloop, Gp2; Macroshear chisel, Gp3; and Microshear chisel, Gp4. They were tested for SBS using chisel and wireloop loading devices followed by failure mode analysis using digital microscopy and SEM. Two- and one-way ANOVA were used to compare stress at failure values of different groups while the Kruskal–Wallis test was used to compare between failure modes of the tested groups. Gp4 recorded the highest mean stress at failure 54.1 ± 14.1 MPa, and the highest percentage of adhesive failure in relation to the other groups. Specimen dimension and loading technique are important parameters influencing the results of shear bond strength. Micro-sized specimens and chisel loading are recommended for shear testing.


2012 ◽  
Vol 3 (2) ◽  
pp. 150-155
Author(s):  
Eduardo Galera da Silva ◽  
Maria Filomena Rocha Lima Huhtala ◽  
Ana Paula Martins Gomes ◽  
Clovis Pagani ◽  
Carlos Rocha Gomes Torres ◽  
...  

ABSTRACT Aim This in vitro study evaluated the shear bond strength of a chemical resin cement to five adhesive systems in bovine dentin. Materials and methods One hundred and three bovine teeth were divided into five experimental groups (n = 19) and two control groups (n = 4). A flat dentin surface was exposed on each tooth after wet grinding the buccal enamel, in order to apply the adhesive systems (Adper Single Bond, Adper Scotchbond Multi-Purpose, Multi Bond Uno plus Duo, One Step, Prompt L-Pop) to 95 teeth, according to manufacture's instructions. Four teeth were etched with phosphoric acid (negative control) and four teeth were no etched with phosphoric acid (positive control). Light-cured composite blocks were sandblasted before the cementation with C&B Cement (Bisco) over the treated dentin. The specimens were stored in distilled water at 37°C and submitted to the shear bond strength test after 7 days. Results ANOVA and Tukey tests (p = 0.05) demonstrated that Adper Single Bond (7.47 ± 4.37), Adper Scotchbond Multi-Purpose (6.68 ± 5.11) and One Step (7.30 ± 4.29) presented the highest bond strength values. Prompt L-Pop (0.05 ± 0.17) and Multi Bond Uno plus Duo (0.72 ± 1.41) presented the lowest significant bond strength values. Conclusion The shear bond strength of composite resin cylinders cemented with chemically activated resin cement depends on the adhesive system used. Clinical significance Fourth and fifth generation light polymerized bonding systems are indicated when self-polymerizing cements are used. How to cite this article Kubo CH, Caneppele TMF, da Silva EG, Huhtala MFRL, Torres CRG, Pagani C, Gomes APM. Shear Bond Strength of a Chemical Resin Cement to Five Adhesive Systems in Bovine Dentin. World J Dent 2012;3(2):150-155.


2014 ◽  
Vol 62 (4) ◽  
pp. 365-370 ◽  
Author(s):  
Ricardo Alves dos SANTOS ◽  
Eliane Alves de LIMA ◽  
Mônica Maria de Albuquerque PONTES ◽  
Alexandre Batista Lopes do NASCIMENTO ◽  
Marcos Antônio Japiassú Resende MONTES ◽  
...  

OBJECTIVE: To assess the bond strength to dentin of the Single Bond (3M ESPE) and XP Bond (Dentsply) total-etch and Adper SE Plus (3M ESPE) self-etch adhesive systems. METHODS: Fifteen healthy human third molars were randomly allocated across three different groups of five teeth each according to the adhesive system. The occlusal portion of each tooth was removed under refrigeration using a flexible diamond disc (EXTEC, Enfield, CT, USA) down to an area of dentin that did not reveal enamel, as confirmed under a 40X stereo microscope (Ramsor, São Paulo, Brazil). A standardized smear layer was created with #600 grit silicon-carbide paper. The adhesive systems were applied as per manufacturer recommendations, with the exception of the Adper SE Plus system, which was triple-polymerized. Composite resin blocks (5 mm) were placed on the dentin surface. The specimens were stored in distilled water for 24 hours at 37ºC. Using a flexible diamond disc (EXTEC, Enfield, CT, USA), toothpick-like specimens with an adhesive area of less than 1 mm² were obtained. A microtensile bond test was then carried out using a universal testing machine (KRATOS) with a crosshead speed of 0.5 mm/min. Analysis of variance (ANOVA) and Tukey's test were used for comparisons. RESULTS: The bond strength values obtained with each adhesive system were as follows: XP Bond, 96.24 MPa; Adper Single Bond, 72.39 MPa; Adper SE Plus, 49.91 MPa. CONCLUSION: In terms of bond strength to dentin, conventional adhesives outperform self-etching systems.


2020 ◽  
Vol 2020 ◽  
pp. 1-7
Author(s):  
Mariana Almeida Mello Proença ◽  
Karime Tavares Lima da Silva ◽  
Alisson Costa e Silva ◽  
Edilausson Moreno Carvalho ◽  
José Bauer ◽  
...  

Objectives. The aim of this study was to evaluate the shear bond strength of metal brackets bonded with different universal adhesive systems containing 10-MDP and Transbond Plus Self Etching Primer after 20,000 thermal cycles. Materials and Methods. A total of 130 sound bovine teeth were used, which are divided into 5 groups (n = 26) according to the adhesive system used: All-Bond Universal (Bisco), Ambar Universal (FGM), Clearfil Universal Bond (Kuraray), Single Bond Universal (3M/ESPE), and Transbond Plus SEP (3M/ESPE) as control. The adhesives were applied for 20 seconds and bonded with a resin Transbond XT (3M/ESPE). After this, the teeth were submitted to 20,000 cycles at 5°C and 55°C. Afterwards, the shear bond strength test was performed in a universal test machine (Instron 3342). The adhesive remnant index (ARI) was evaluated under a stereomicroscope at 10x magnification and scanning electronic microscopy (SEM, Hitachi 3030). The shear bond strength data were submitted to One-Way ANOVA (α = 0.05) and the ARI to the Kruskal–Wallis test (α = 0.05). Results. Statistical analysis showed that the universal adhesive systems presented mean shear bond strength values similar to Transbond Plus SEP (p<0.05). The universal adhesive presented similar ARI values among them but differed from those of Transbond Plus SEP (p<0.001). Transbond Plus SEP presented a high ARI value when compared with the universal adhesive systems and high demineralization of enamel. Conclusions. The results show that universal adhesive systems may be used for bonding metal brackets if the orthodontist wants to maintain dental enamel health.


2018 ◽  
Vol 2018 ◽  
pp. 1-8 ◽  
Author(s):  
Katrin Zumstein ◽  
Anne Peutzfeldt ◽  
Adrian Lussi ◽  
Simon Flury

This study investigated the effect of SnCl2/AmF pretreatment on short- and long-term bond strength of resin composite to eroded dentin mediated by two self-etch, MDP-containing adhesive systems. 184 dentin specimens were produced from extracted human molars. Half the specimens (n=92) were artificially eroded, and half were left untreated. For both substrates, half the specimens were pretreated with SnCl2/AmF, and half were left untreated. The specimens were treated with Clearfil SE Bond or Scotchbond Universal prior to application of resin composite. Microtensile bond strength (μTBS) was measured after 24 h or 1 year. Failure mode was detected and EDX was performed. μTBS results were statistically analyzed (α=0.05). μTBS was significantly influenced by the dentin substrate (eroded < noneroded dentin) and storage time (24 h > 1 year; p<0.0001) but not by pretreatment with SnCl2/AmF or adhesive system. The predominant failure mode was adhesive failure at the dentin-adhesive interface. The content of Sn was generally below detection limit. Pretreatment with SnCl2/AmF did not influence short- and long-term bond strength to eroded dentin. Bond strength was reduced after storage for one year, was lower to eroded dentin than to noneroded dentin, and was similar for the two adhesive systems.


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