THE DEVELOPMENT OF GLUCOSE SENSOR BASED ON SiO2-CuO MATERIALS USING SCREEN PRINTED CARBON ELECTRODE (SPCE)

2016 ◽  
Vol 12 (1) ◽  
Author(s):  
Intan Frina Utamiyanti
Keyword(s):  
Cyclic Voltammetry ◽  
Glucose Sensor ◽  
Reference Electrode ◽  
Synthesis Process ◽  
Potential Range ◽  
Carbon Electrode ◽  
Screen Printed Carbon Electrode ◽  
Cyclic Voltammetry Method ◽  
Cyclic Voltammetry Analysis ◽  
Screen Printed

<p>The development of material-based glucose sensor SiO<sub>2</sub>-CuO using Screen Printed Carbon Electrode (SPCE) had been done. Three types of materials were used to detect glucose, i.e Multi Wall Carbon Nanotube (MWCNT)-SiO2-CuO, SiO2-CuO (A) dan SiO2-CuO (B). The differences composition of SiO<sub>2</sub>-CuO(A) and SiO<sub>2</sub>-CuO(B) occurred during the addition of NaOH in synthesis process of SiO2-CuO (B). The prepared materials were analyzed by Scanning Electron Microscopy (SEM), cyclic voltammetry method and chrono-amperometry. Cyclic voltammetry analysis was conducted at a potential range of -1.0 - 1.5 V with Ag/AgCl as reference electrode. The scan rate was 100 mV/sec and the potential was varied at (-0.6), (-0.5) and (-0.4) V, in which the duration of each analysis was 5 second. Based on the result of analysis, whether by SEM, cyclic voltammetry and chrono-amperometry, the SiO<sub>2</sub>-CuO (B) was found to be the best material for detection of glucose.</p>

scholarly journals THE DEVELOPMENT OF GLUCOSE SENSOR BASED ON SiO2-CuO MATERIALS USING SCREEN PRINTED CARBON ELECTRODE (SPCE)

2016 ◽  
Vol 12 (1) ◽  
pp. 50
Author(s):  
Intan Frina Utamiyanti ◽  
Barlah Rumhayati ◽  
Ani Mulyasuryani
Keyword(s):  
Cyclic Voltammetry ◽  
Glucose Sensor ◽  
Reference Electrode ◽  
Synthesis Process ◽  
Potential Range ◽  
Carbon Electrode ◽  
Screen Printed Carbon Electrode ◽  
Cyclic Voltammetry Method ◽  
Cyclic Voltammetry Analysis ◽  
Screen Printed

The development of material-based glucose sensor SiO<sub>2</sub>-CuO using Screen Printed Carbon Electrode (SPCE) had been done. Three types of materials were used to detect glucose, i.e Multi Wall Carbon Nanotube (MWCNT)-SiO2-CuO, SiO2-CuO (A) dan SiO2-CuO (B). The differences composition of SiO<sub>2</sub>-CuO(A) and SiO<sub>2</sub>-CuO(B) occurred during the addition of NaOH in synthesis process of SiO2-CuO (B). The prepared materials were analyzed by Scanning Electron Microscopy (SEM), cyclic voltammetry method and chrono-amperometry. Cyclic voltammetry analysis was conducted at a potential range of -1.0 - 1.5 V with Ag/AgCl as reference electrode. The scan rate was 100 mV/sec and the potential was varied at (-0.6), (-0.5) and (-0.4) V, in which the duration of each analysis was 5 second. Based on the result of analysis, whether by SEM, cyclic voltammetry and chrono-amperometry, the SiO<sub>2</sub>-CuO (B) was found to be the best material for detection of glucose.

scholarly journals THE DEVELOPMENT OF GLUCOSE SENSOR BASED ON SiO2-CuO MATERIALS USING SCREEN PRINTED CARBON ELECTRODE (SPCE)

2016 ◽  
Vol 12 (1) ◽  
pp. 50
Author(s):  
Intan Frina Utamiyanti ◽  
Barlah Rumhayati ◽  
Ani Mulyasuryani
Keyword(s):  
Cyclic Voltammetry ◽  
Glucose Sensor ◽  
Reference Electrode ◽  
Synthesis Process ◽  
Potential Range ◽  
Carbon Electrode ◽  
Screen Printed Carbon Electrode ◽  
Cyclic Voltammetry Method ◽  
Cyclic Voltammetry Analysis ◽  
Screen Printed

The development of material-based glucose sensor SiO<sub>2</sub>-CuO using Screen Printed Carbon Electrode (SPCE) had been done. Three types of materials were used to detect glucose, i.e Multi Wall Carbon Nanotube (MWCNT)-SiO2-CuO, SiO2-CuO (A) dan SiO2-CuO (B). The differences composition of SiO<sub>2</sub>-CuO(A) and SiO<sub>2</sub>-CuO(B) occurred during the addition of NaOH in synthesis process of SiO2-CuO (B). The prepared materials were analyzed by Scanning Electron Microscopy (SEM), cyclic voltammetry method and chrono-amperometry. Cyclic voltammetry analysis was conducted at a potential range of -1.0 - 1.5 V with Ag/AgCl as reference electrode. The scan rate was 100 mV/sec and the potential was varied at (-0.6), (-0.5) and (-0.4) V, in which the duration of each analysis was 5 second. Based on the result of analysis, whether by SEM, cyclic voltammetry and chrono-amperometry, the SiO<sub>2</sub>-CuO (B) was found to be the best material for detection of glucose.

scholarly journals Development of Potentiometric Phenol Sensors by Nata de Coco Membrane on Screen-Printed Carbon Electrode

2019 ◽  
Vol 2019 ◽  
pp. 1-8 ◽  
Author(s):  
Ani Mulyasuryani ◽  
Afifah Muhimmatul Mustaghfiroh
Keyword(s):  
Mechanical Stability ◽  
Conductive Polymer ◽  
Reference Electrode ◽  
Membrane Thickness ◽  
Carbon Electrode ◽  
Cross Sectional ◽  
Accuracy And Precision ◽  
Screen Printed Carbon Electrode ◽  
Electrode Membrane ◽  
Screen Printed

Nata de coco, a bacterial cellulose as a result of coconut water fermentation, is a conductive polymer with a electrical conductivity of 553 μS/cm and has high mechanical stability. In this study, nata de coco was used as a supporting membrane for the development of phenol sensors in potentiometry. Nata de coco membrane containing phenol is coated on the surface of the printed carbon electrode (screen-printed carbon electrode). The cross-sectional area of the carbon electrode coated with the membrane is 1.5 × 3 mm2, while the reference electrode is Ag/AgCl. The thickness of the electrode membrane affects the Nernstian factor. The optimum Nernstian factor is produced by 100 μm membrane thickness containing 117.5 μg of phenol. Measurement of phenol solution was carried out at pH 11, in the concentration range of 10−8 to 10−2 mol/L, resulting in a Nernstian factor of 41.8 ± 1.3 mV/decade. The Nernstian factor increased to 55.7 ± 0.4 mV/decade if the membrane of the electrode contained 0.1% Fe3O4 nanoparticles. This sensor has been applied in the real sample of river water, resulting in good accuracy and precision.

An anti-HCT-interference glucose sensor based on a fiber paper-based screen-printed carbon electrode

2019 ◽  
Vol 297 ◽  
pp. 126763
Author(s):  
XinXin He ◽  
Shwu Jen Chang ◽  
Kalpana Settu ◽  
Ching-Jung Chen ◽  
Jen-Tsai Liu
Keyword(s):  
Glucose Sensor ◽  
Carbon Electrode ◽  
Screen Printed Carbon Electrode ◽  
Screen Printed

Laser Photocatalysis of the Chlorophyll Dye Using the Cyclic Voltammetry Method

2021 ◽  
Vol 882 ◽  
pp. 143-154
Author(s):  
Huda S. Alhasan
Keyword(s):  
Cyclic Voltammetry ◽  
Laser Light ◽  
Potential Range ◽  
Carbon Electrode ◽  
Total Chlorophyll ◽  
Tetrabutylammonium Perchlorate ◽  
Oxidation Peak ◽  
Solution Ph ◽  
Cyclic Voltammetry Method ◽  
Wide Potential

Cyclic voltammetry is a widely used technique in electrochemistry due to its simplicity and large amount of data and information that can be obtained. This study utilises this technique to study chlorophyll a and total chlorophyll (Tchl) alongside a laser light to induce photosynthesis. No oxidative peak was observed, regardless of the solution pH in either a dark or light environment when using a solution with an electrolyte of tetrabutylammonium perchlorate (TBAP) in both dichloromethane (DCM) and acetonitrile (MeCN), whereas in a solution of aqueous HCl a small anodic peak was observed. The concentration of the droplet of Tchl pigment on the surface of macro glassy carbon electrode (GCE) was increased, which resulted in a similar trend and the oxidation peak was observed to be slightly larger when in the presence of light. It was observed that the filtered solution of Tchl pigment produced a weaker signal than the unfiltered solution and there were slightly reduced oxidative peak currents when the concentration of VK1 was increased. were no observed changes in the peak charges or currents over a wide potential range (0.0, 0.2, 0.4, 0.6 and 0.8 V) in the presence or absence of light by using coulometry and amperometry methods, therefore, more information on the 3-D formation is required for the photoreduction processes.

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