Simultaneous Assessment of Wettability and Water Saturation Through Integration of 2D NMR and Electrical Resistivity Measurements

2020 ◽  
Author(s):  
Zulkuf Azizoglu ◽  
Artur Posenato Garcia ◽  
Chelsea Newgord ◽  
Zoya Heidari
Geophysics ◽  
2009 ◽  
Vol 74 (1) ◽  
pp. E57-E73 ◽  
Author(s):  
Jesús M. Salazar ◽  
Carlos Torres-Verdín

Some laboratory and qualitative studies have documented the influence of water-based mud(WBM)-filtrate invasion on borehole resistivity measurements. Negligible work, however, has been devoted to studying the effects of oil-based mud(OBM)-filtrate invasion on well logs and the corresponding impact on the estimation of petrophysical properties. We quantitatively compare the effects of WBM- and OBM-filtrate invasion on borehole resistivity measurements. We simulate the process of mud-filtrate invasion into a porous and permeable rock formation assuming 1D radial distributions of fluid saturation and fluid properties while other petrophysical properties remain constant. To simulate the process of mud-filtrate invasion, we calculate a time-dependent flow rate of OBM-filtrate invasion by adapting the available formulation of the physics of WBM-filtrate invasion. This approach includes the dynamically coupled effects of mud-cake growth and multiphase filtrate invasion. Simulations are performed with a commercial adaptive-implicit compositional formulation that enables the quantification of effects caused by additional components of mud-filtrate and native fluids. The formation under analysis is 100% water saturated (base case) andis invaded with a single-component OBM. Subsequently, we perform simulations of WBM filtrate invading the same formation assuming that it is hydrocarbon bearing, and compare the results to those obtained in the presence of OBM. At the end of this process, we invoke Archie’s equation to calculate the radial distribution of electrical resistivity from the simulated radial distributions of water saturation and salt concentration and compare the effects of invasion on borehole resistivity measurements acquired in the presence of OBM and WBM. Simulations confirm that the flow rate of OBM-filtrate invasion remains controlled by the initial mud-cake permeability and formation petrophysical properties, specifically capillary pressure and relative permeability. Moreover, WBM causes radial lengths of invasion 15%–40% larger than those associated with OBM as observed on the radial distributions of electrical resistivity. It is found also that, in general, flow rates of WBM-filtrate invasion are higher than those of OBM-filtrate invasion caused by viscosity contrasts between OBM filtrate and native fluids, which slow down the process of invasion. Such a conclusion is validated by the marginal variability of array-induction resistivity measurements observed in simulations of OBM invasion compared with those of WBM invasion.


Geophysics ◽  
2016 ◽  
Vol 81 (6) ◽  
pp. D643-D655 ◽  
Author(s):  
Anqi Yang ◽  
Gama Firdaus ◽  
Zoya Heidari

Low electrical resistivity measurements in organic-rich mudrocks are commonplace in highly mature zones. These low resistivity values are usually difficult to justify and lead to overestimation of water saturation when using conventional resistivity-porosity-saturation models (e.g., dual water and Waxman-Smits). Previous publications suggest that the electrical conductivity of kerogen increases when it thermally matures. This increase in thermal maturity of kerogen might contribute to low resistivity measurements in organic-rich mudrocks. However, electrical properties of kerogen within these rocks have not yet been quantified experimentally. We have introduced a technique to quantify electrical resistivity of kerogen through combined experimental and numerical approaches and quantified electrical resistivity of kerogen samples from the Haynesville and Eagle Ford Formations. We first isolated kerogen from mudrock samples using physical and chemical treatments. The isolated kerogen powder was then compressed into a homogeneous disk. Then, we synthetically matured mudrock and kerogen samples to controlled maturity levels and measured the electrical resistivity and geochemical properties of each sample. The true electrical resistivity of kerogen was then estimated by minimizing the difference between the numerically simulated and measured electrical resistivity of the molded kerogen samples. We have observed a significant decrease in the electrical resistivity of kerogen isolated from the Haynesville (i.e., up to four orders of magnitude) and Eagle Ford (i.e., up to nine orders of magnitude) Formations upon heat treatment from 300°C to 800°C. The decrease in resistivity can be reasoned by the chemical transformations of organic matter through thermal maturation. The results of solid-state [Formula: see text] nuclear magnetic resonance spectroscopy and transmission electron microscopy imaging confirmed increase in graphitization and aromaticity in the kerogen samples as thermal maturity increases. Our outcomes can potentially improve interpretation of electrical resistivity logs in organic-rich mudrocks, such as enhancing well-log-based assessment of in situ hydrocarbon saturation.


Fuel ◽  
2020 ◽  
Vol 270 ◽  
pp. 117431 ◽  
Author(s):  
Chelsea Newgord ◽  
Saurabh Tandon ◽  
Zoya Heidari

Author(s):  
W. E. King

A side-entry type, helium-temperature specimen stage that has the capability of in-situ electrical-resistivity measurements has been designed and developed for use in the AEI-EM7 1200-kV electron microscope at Argonne National Laboratory. The electrical-resistivity measurements complement the high-voltage electron microscope (HVEM) to yield a unique opportunity to investigate defect production in metals by electron irradiation over a wide range of defect concentrations.A flow cryostat that uses helium gas as a coolant is employed to attain and maintain any specified temperature between 10 and 300 K. The helium gas coolant eliminates the vibrations that arise from boiling liquid helium and the temperature instabilities due to alternating heat-transfer mechanisms in the two-phase temperature regime (4.215 K). Figure 1 shows a schematic view of the liquid/gaseous helium transfer system. A liquid-gas mixture can be used for fast cooldown. The cold tip of the transfer tube is inserted coincident with the tilt axis of the specimen stage, and the end of the coolant flow tube is positioned without contact within the heat exchanger of the copper specimen block (Fig. 2).


1967 ◽  
Vol 6 (47) ◽  
pp. 599-606 ◽  
Author(s):  
Hans Röthlisberger

A brief description of the resistivity method is given, stressing the points which are of particular importance when working on glaciers. The literature is briefly reviewed.


Sign in / Sign up

Export Citation Format

Share Document