Fourier Transform Infrared and Fluorescence Spectral Features of Organic Matter in Conventional and Organic Dairy Manure

2012 ◽  
Vol 41 (3) ◽  
pp. 911-919 ◽  
Author(s):  
Zhongqi He ◽  
Tsutomu Ohno
2002 ◽  
Vol 16 (3-4) ◽  
pp. 245-250
Author(s):  
V. Crupi ◽  
S. Galli ◽  
D. Majolino ◽  
P. Migliardo ◽  
S. Pergolizzi ◽  
...  

In the present work, we report on a vibrational study performed on rat encephalon samples and on human tissue affected by cancer, using Fourier Transform Infrared absorbance spectroscopy. As the brain rat tissue is concerned, the FT-IR measurements, performed in the CH–OH vibrational stretching region (2400–3800 cm−1), permitted us to reveal the presence of a very diffuse commercial benzodiazepine: VALIUM®. The comparison between the spectral features of normal brain and the ones of samples with administrated substance has unambiguously showed that the CH stretching region seems not to be affected by any change for the pharmacological treatment, instead the OH band is strongly modified probably due to the presence of a new spectral contribution characteristic of diazepam molecule. In the case of skin tissue the investigation was addressed to characterize the presence of two different pathologies, namely epithelioma and basalioma, and to show clear different spectral features passing from the normal tissue to the malignant one in particular in the region (1500–2000 cm−1) which is typical of the lipids vibrational bands.


2021 ◽  
Vol 10 (3) ◽  
pp. 291-298
Author(s):  
Jusup Suprijanto ◽  
Juwita Lesly Senduk ◽  
Dewi Basthika Makrima

Mikroplastik adalah salah satu pencemar laut. Mikroplastik tidak dapat terdegradasi dengan cepat. Mikroplastik merupakan partikel plastik yang berukuran <5mm. Ukurannya yang kecil menyebabkannya dapat tertransportasikan ke seluruh tempat termasuk sistem tubuh ikan dan cumi-cumi. Penelitian dilakukan bertujuan mengetahui mikroplastik pada cumi – cumi (Loligo sp.) dan ikan kembung (Rastrelliger sp.). Penelitian dilakukan bulan Juli 2020 – November 2020 di Semarang Jawa Tengah. Pengambilan sampel dilakukan di TPI Tambak Lorok Semarang.  Pengukuran cumi-cumi dilakukan menggunakan jangka sorong dan ikan diukur menggunakan penggaris. Pembedahan cumi-cumi dan ikan dilakukan menggunakan gunting bedah untuk memisahkan alat pencernaan, tentakel serta insang ikan yang akan digunakan sebagai sampel. Pelarutan dilakukan menggunakan perendaman KOH 10% selama 24 jam untuk melarutkan bahan organik. Pemisahan partikel mikroplastik dilakukan setelah seluruh bahan organik pada sampel larut seluruhnya. Pemisahan partikel mikroplastik dilakukan menggunakan perendaman ZnCl2 selama 24 jam. Penyaringan sampel dilakukan setelah sampel mempunyai 2 layer, layer pertama diambil 10 ml kemudian disaring menggunakan kertas whatman dengan vacump pump. Sampel yang telah disaring dikeringkan, dilanjutkan uji FTIR. Hasil penelitian menunjukkan bahwa terdapat mikroplastik dalam cumi – cumi dan ikan kembung yang ada di TPI Tambak Lorok Semarang, FTIR menunjukkan terdapat polimer plastik jenis nitrile dan nylon. Microplastic is one of the pollutants of the sea. Microplastics do not degrade quickly. Microplastics are plastic particles <5mm in size. Its small size allows it to be transported all over the place including the body systems of fish and squid. The research was conducted to determine the microplastics in squid (Loligo sp.) And mackerel fish (Rastrelliger sp.). The research was conducted in July 2020 - November 2020 in Semarang, Central Java. Sampling was carried out at TPI Tambak Lorok Semarang. Measurements of squid were carried out using a caliper and fish were measured using a ruler. Squid and fish surgery is performed using surgical scissors to separate the digestive organs, tentacles and fish gills that will be used as samples. Dissolving was carried out using 10% KOH immersion for 24 hours to dissolve organic matter. The separation of microplastic particles is carried out after all the organic material in the sample is completely dissolved. The separation of microplastic particles was carried out using ZnCl2 immersion for 24 hours. Filtering of the sample is carried out after the sample has 2 layers, 10 ml of the first layer is taken then filtered using Whatman paper with a vacump pump. The filtered sample was dried, followed by the FTIR test. The results showed that there were microplastics in the squid and mackerel in Tambak Lorok Semarang, FTIR showed that there were plastic polymers of nitrile and nylon types. 


Soil Science ◽  
2007 ◽  
Vol 172 (7) ◽  
pp. 501-515 ◽  
Author(s):  
Zhongqi He ◽  
C. Wayne Honeycutt ◽  
Baoshan Xing ◽  
Richard W. McDowell ◽  
Perry J. Pellechia ◽  
...  

2014 ◽  
Vol 43 (2) ◽  
pp. 690-700 ◽  
Author(s):  
Heidi M. Waldrip ◽  
Zhongqi He ◽  
Richard W. Todd ◽  
James F. Hunt ◽  
Marty B. Rhoades ◽  
...  

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