scholarly journals Гомогенизационный отжиг и магнитные свойства образца фазы Лавеса GdNi-=SUB=-2-=/SUB=-

2021 ◽  
Vol 63 (12) ◽  
pp. 1994
Author(s):  
А.В. Маширов ◽  
И.И. Мусабиров ◽  
М.С. Аникин ◽  
М.А. Сёмкин ◽  
В. Митюк ◽  
...  

The paper shows the effect of homogenization annealing on the ferromagnet-paramagnet phase transition in the GdNi2 alloy. In the cast sample, at the Curie point, a temperature hysteresis is observed, which in an external magnetic field of 13.5 T can be at least 3 degrees. The data of scanning electron microscopy of the electropolished samples showed a decrease in the impurity phase of GdNi and practically no temperature hysteresis of the phase transition in the annealed GdNi2 sample. The value of the isothermal change entropy DSm = - 18.931 J/(kg*K) for an annealed sample of the GdNi2 alloy at the Curie point of 75 K in a magnetic field of 13.5 T.

2005 ◽  
Vol 70 (10) ◽  
pp. 1213-1217 ◽  
Author(s):  
Nebojsa Nikolic

Nickel deposits obtained from a Watt solution both without and with a perpendicularly oriented magnetic field were examined by scanning electron microscopy (SEM). The nickel deposit obtained without an imposed magnetic field was very rough, with a clearly visible clustered structure. The nickel deposit obtained under a perpendicularly oriented magnetic field has a very developed dendritic structure, which can be denoted as arboreous ? bead dendritic structure. The ob- served difference is essentially ascribed to the effect of a magnetic field on the magnetic properties of nickel.


2013 ◽  
Vol 200 ◽  
pp. 261-266
Author(s):  
Igor Virt ◽  
Igor Rudyi ◽  
Ivan Kurilo ◽  
Ivan Lopatynskyi ◽  
Marian Frugynskyi ◽  
...  

Structural and magnetic properties of ceramics Zn1-xCoxO and Zn1-xCrxO are studied. Average sizes of grains are determined by scanning electron microscopy. The magnetic field dependences of magnetic susceptibility are investigated by Faraday method. The relevant theoretical models are chosen.


2017 ◽  
Vol 371 ◽  
pp. 44-48
Author(s):  
Young Min Kim ◽  
Min Jung Kang

In this study, we analyzed weld cracking in Ni-based superalloys. Alloys with about 64 wt.% Ni and 31 wt.% Ni were used for the weld metal analysis. Phase transition predicted by thermodynamic calculation were compared with experimental results. The weld metal’s microstructure was analyzed by scanning electron microscopy (SEM) and energy dispersive X-ray spectroscopy (EDX) mapping, and its mechanical properties tested. From EDX mapping, it was established that the alloying elements (Nb and Mo) were segregated around the weld crack as a result of the formation of a niobium carbide (NbC).


2009 ◽  
Vol 154 ◽  
pp. 107-112 ◽  
Author(s):  
Anna Boczkowska ◽  
Stefan F. Awietjan

In this paper studies on urethane magnetorheological elastomers (MREs) microstructure in respect to their magnetic and mechanical properties are reported. MREs were obtained from a mixture of polyurethane gel and carbonyl-iron particles cured in a magnetic field of 100 and 300 mT. The amount of particles was varied from 1.5 to 33 vol. %. Samples with different arrangements of particles were produced. Effect of the amount of ferromagnetic particles and their arrangement on microstructure and properties in relation to the external magnetic field was investigated. The microstructure was studied using scanning electron microscopy. Magnetic properties were measured using vibrating sample magnetometer. Rheological and mechanical properties under compression were also examined.


2012 ◽  
Vol 182-183 ◽  
pp. 167-173
Author(s):  
Ming Li ◽  
Zhi Ming Shi ◽  
Dong Fang

This paper studies iron-rich phase transformation law and mechanism of Al-20Si-10Fe alloy under the effect of plate magnetic field. with optical microscopy(OM),scanning electron microscopy(SEM),energy dispersive spectrum(EDS)and transmission electron microscopy(TEM). The results show that plate magnetic field is directly involved in the phase transformation of iron-rich phase, making iron-rich phase change from lath-shaped β-Al5FeSi to herringbone-shapedα-Al8SiFe2. The enforcement of plate magnetic field during the phase-transforming process of β-Al5FeSi→α-Al8Si Fe2makes block α-Al1.3Si7.8Fe2.1phase yield out. And precipitation of α-Al1.3Si7.8Fe2.1phase is affected by the transforming process ofβ-Al5SiFe phase→α-Al8Si Fe2phase.


2007 ◽  
Vol 72 (8-9) ◽  
pp. 787-797 ◽  
Author(s):  
Nebojsa Nikolic

The morphologies of nickel and copper deposits obtained without applied magnetic fields, and with both parallel and perpendicular applied magnetic fields were examined by the scanning electron microscopy (SEM) technique. Changes in the morphologies of the metals caused by the effect of the magnetic fields are explained by the concept of "effective overpotential". The morphologies of the nickel and copper deposits obtained under parallel oriented magnetic fields were similar to those obtained at some lower cathodic potentials without an applied magnetic field. The magnetic field with a perpendicular orientation to the electrode surface increased the dispersity of the nickel and copper deposits. Nickel and copper deposits obtained under this orientation of the magnetic field were similar to those obtained at some higher cathodic potentials without an applied magnetic field. .


2014 ◽  
Vol 931-932 ◽  
pp. 157-161 ◽  
Author(s):  
Pongthep Jansanthea ◽  
Pusit Pookmanee ◽  
Sirirat Phaisansuthichol ◽  
Sakchai Satienperakul ◽  
Supaporn Sangsrichan ◽  
...  

Bismuth vanadate (BiVO4) powder was synthesized via the solvothermal method at 100200 °C for 26h by using acetic acid as solvent without calcination steps. The phase transition of BiVO4 powder was studied by Xray diffraction (XRD). The morphology and chemical composition of BiVO4 powder were investigated by scanning electron microscopy (SEM) and energy dispersive spectroscopy (EDS). The functional groups of BiVO4 powder was identified by Fourier transform infrared spectroscopy (FTIR).


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