scanning electron microscopy measurement
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2021 ◽  
Vol 887 ◽  
pp. 151-155
Author(s):  
S.G. Shuklin ◽  
I.M. Velm

Carbon nanotubes have been studied by scanning electron microscopy. Measurement modes - accelerating voltage 10 kV, current in microscopy mode 10-9 A. The sample was applied to a metal mesh. Spectroscopic data indicate that this sample consists of carbon (peak at 280 eV). There are no other intense peaks in the spectrum; no impurities were detected by this method. Determination of physical and mechanical characteristics was carried out on a testing machine model N5K-S.


2019 ◽  
Vol 969 ◽  
pp. 237-241
Author(s):  
R. Sivanand ◽  
S. Chellammal ◽  
S. Manivannan

Cadmium sulphide nanocrystallites have been synthesized using precipitation method. The average sizes of the prepared samples is determined by XRD (x-ray diffraction) method. Morphological studies are carried out by SEM (scanning electron microscopy) measurement. Necesssary elements present in prepared samples, are confirmed by EDAX (energy dispersive analysis of x-ray spectroscopy) method. By Ultraviolet visible spectroscopy measurement, the value of absorption wavelength, band gap values are calculated in optical method. The electrical properties are analysed using impedance analyser measurement for the Nanocrystallites.


2018 ◽  
Vol 96 (11) ◽  
pp. 975-983
Author(s):  
Faiza Bouazza ◽  
Belkacem Benguella ◽  
Sarah Soussi

The objective of this study is the variation of natural and modified clays and their use in industrial waste treatment. For this purpose, we carried out several elimination tests of the effluents by adsorption by using two natural clays from different deposits, namely bentonite located in Maghnia and Djabel Debbagh of Ain Berbar and bentonite coupled with cellulose. The adsorption test was performed on a Decis pesticide. The clays that we tested, in the natural state and in the modified state, are the object of a mineralogical and physicochemical characterization by various techniques of analysis: X-ray diffraction, chemical composition, spectroscopy infrared, cation exchange capacity, scanning electron microscopy, measurement of specific surface area, and various adsorption tests concerning kinetics and capacity, as well as kinetic and thermodynamic modeling and adsorption isotherms. The results showed the practical use of clays for the decontamination of waters contaminated by organic pollutants.


Blood ◽  
1992 ◽  
Vol 80 (11) ◽  
pp. 2774-2780 ◽  
Author(s):  
CM Smith ◽  
SM Burris ◽  
GH Rao ◽  
JG White

Abstract This study contrasts the protein composition of the detergent-resistant cytoskeleton of platelets fully spread on glass with the cytoskeletal composition of resting platelets and platelets aggregated in suspension with thrombin. Complete Triton X-100-insoluble cytoskeletons were isolated from spread, resting, and suspension-activated platelets in the presence of protease inhibitors, solubilized in sodium dodecyl sulfate/EDTA and analyzed on reduced, one-dimensional polyacrylamide gels. The protein composition of the cytoskeletons differed both qualitatively and quantitatively. Most notable were more extensive incorporation of total protein, talin, and vinculin into the cytoskeleton of spread platelets than the cytoskeleton of suspension- activated platelets. Varying the concentration and time of exposure to thrombin during suspension activation did not mimic the cytoskeletal changes of surface activation. Scanning electron microscopy, measurement of lipid phosphorus content, and varying the duration of Triton extraction did not show incomplete solubilization or nonspecific trapping of constituents in the spread platelet cytoskeleton. Proteolysis of talin was minimal in suspension-activated platelets and in platelets spread for 50 minutes. The differences in the detergent- resistant cytoskeletons of surface- and suspension-activated platelets indicate significant divergence in the physiologies of platelet spreading on surfaces and platelet activation in suspension.


Blood ◽  
1992 ◽  
Vol 80 (11) ◽  
pp. 2774-2780 ◽  
Author(s):  
CM Smith ◽  
SM Burris ◽  
GH Rao ◽  
JG White

This study contrasts the protein composition of the detergent-resistant cytoskeleton of platelets fully spread on glass with the cytoskeletal composition of resting platelets and platelets aggregated in suspension with thrombin. Complete Triton X-100-insoluble cytoskeletons were isolated from spread, resting, and suspension-activated platelets in the presence of protease inhibitors, solubilized in sodium dodecyl sulfate/EDTA and analyzed on reduced, one-dimensional polyacrylamide gels. The protein composition of the cytoskeletons differed both qualitatively and quantitatively. Most notable were more extensive incorporation of total protein, talin, and vinculin into the cytoskeleton of spread platelets than the cytoskeleton of suspension- activated platelets. Varying the concentration and time of exposure to thrombin during suspension activation did not mimic the cytoskeletal changes of surface activation. Scanning electron microscopy, measurement of lipid phosphorus content, and varying the duration of Triton extraction did not show incomplete solubilization or nonspecific trapping of constituents in the spread platelet cytoskeleton. Proteolysis of talin was minimal in suspension-activated platelets and in platelets spread for 50 minutes. The differences in the detergent- resistant cytoskeletons of surface- and suspension-activated platelets indicate significant divergence in the physiologies of platelet spreading on surfaces and platelet activation in suspension.


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