scholarly journals Mixing time in yield stress fluids

Author(s):  
Ihuaku Ihejirika

Yield stress fluids are commonly encountered in the pharmaceutical, wastewater and bioprocess industries. On agitation of these fluids with an impeller, a zone of significant motion (cavern) is formed surrounded by stagnant regions. These inhomogeneous conditions are undesirable from a product quality standpoint. Therefore, to evolve a mixing system design that would eliminate these problems, experimental measurements of mixing time were obtained and combined with power consumption to provide a measure of mixing system efficiency. The effect of different parameters such as fluid rheology, impeller rotational speed, impeller type and impeller clearance on the mixing times was also investigated. In addition, using CFD, numerical mixing times were calculated and a comparison of the numerical and experimental mixing times were conducted to investigate the capability of the CFD tool to correctly predict the homogenization process in mixing tanks. In general, it was observed that the power characteristics of the different agitators were well reproduced by the computational package. In addition, CFD was able to correctly predict the effect of impeller rotational speed and fluid yield stress on the mixing times. However, the effect of impeller clearance on the mixing time was not correctly predicted by the CFD package when compared with experimental results obtained in this work as well as those obtained by other researchers. A comparison of the impellers used in this study (Pitched Blade Turbine (PBT), marine propeller and Lightnin A320) using the mixing time correlations available in the literature to fit the experimental data revealed that the PBT was superior to the other impellers in mixing yield stress fluids. In addition, the validated CFD model was used to measure the dimensions of the cavern formed around the impeller and it showed good agreement with the Elson's cavern model.

2021 ◽  
Author(s):  
Ihuaku Ihejirika

Yield stress fluids are commonly encountered in the pharmaceutical, wastewater and bioprocess industries. On agitation of these fluids with an impeller, a zone of significant motion (cavern) is formed surrounded by stagnant regions. These inhomogeneous conditions are undesirable from a product quality standpoint. Therefore, to evolve a mixing system design that would eliminate these problems, experimental measurements of mixing time were obtained and combined with power consumption to provide a measure of mixing system efficiency. The effect of different parameters such as fluid rheology, impeller rotational speed, impeller type and impeller clearance on the mixing times was also investigated. In addition, using CFD, numerical mixing times were calculated and a comparison of the numerical and experimental mixing times were conducted to investigate the capability of the CFD tool to correctly predict the homogenization process in mixing tanks. In general, it was observed that the power characteristics of the different agitators were well reproduced by the computational package. In addition, CFD was able to correctly predict the effect of impeller rotational speed and fluid yield stress on the mixing times. However, the effect of impeller clearance on the mixing time was not correctly predicted by the CFD package when compared with experimental results obtained in this work as well as those obtained by other researchers. A comparison of the impellers used in this study (Pitched Blade Turbine (PBT), marine propeller and Lightnin A320) using the mixing time correlations available in the literature to fit the experimental data revealed that the PBT was superior to the other impellers in mixing yield stress fluids. In addition, the validated CFD model was used to measure the dimensions of the cavern formed around the impeller and it showed good agreement with the Elson's cavern model.


2011 ◽  
Vol 166 (5-6) ◽  
pp. 262-278 ◽  
Author(s):  
S. Hormozi ◽  
K. Wielage-Burchard ◽  
I.A. Frigaard

2016 ◽  
Vol 56 (3) ◽  
pp. 177-188 ◽  
Author(s):  
Alexander Malkin ◽  
Valery Kulichikhin ◽  
Sergey Ilyin

2021 ◽  
Author(s):  
Michael Sandmann

Abstract Objective The aim of this work was to develop a simple optical method to determine the mixing time in a photobioreactor. The image processing method should be based on freeware tools and should not require programming skills. Results An optical method has been established to analyze images from recorded videos of mixing experiments. The basic steps are: 1. Extraction of a sequence of images from the video file; 2. Cropping of the pictures; 3. Background removal; and 4. Image analysis and mixing time evaluation based on quantification of pixel-to-pixel heterogeneity (standard deviation over pixel intensities) within a given area of interest. The novel method was generally able to track the dependency between aeration rate and mixing time within the investigated photobioreactor. In a direct comparison, a Pearson correlation coefficient of rho = 0.9957 was obtained. Gas flow rates between 10 L h−1, and 300 L h−1 resulted from mixing times of between 48 sec and 14 sec, respectively. This simple technique is applicable even without programming skills and can be used in education within high schools and in early stages of undergraduate programs.


2010 ◽  
Author(s):  
Robert Sawko ◽  
Chris P. Thompson ◽  
Theodore E. Simos ◽  
George Psihoyios ◽  
Ch. Tsitouras

Materials ◽  
2020 ◽  
Vol 13 (9) ◽  
pp. 2173
Author(s):  
Mareike Thiedeitz ◽  
Inka Dressler ◽  
Thomas Kränkel ◽  
Christoph Gehlen ◽  
Dirk Lowke

Cementitious pastes are multiphase suspensions that are rheologically characterized by viscosity and yield stress. They tend to flocculate during rest due to attractive interparticle forces, and desagglomerate when shear is induced. The shear history, e.g., mixing energy and time, determines the apparent state of flocculation and accordingly the particle size distribution of the cement in the suspension, which itself affects suspension’s plastic viscosity and yield stress. Thus, it is crucial to understand the effect of the mixing procedure of cementitious suspensions before starting rheological measurements. However, the measurement of the in-situ particle agglomeration status is difficult, due to rapidly changing particle network structuration. The focused beam reflectance measurement (FBRM) technique offers an opportunity for the in-situ investigation of the chord length distribution. This enables to detect the state of flocculation of the particles during shear. Cementitious pastes differing in their solid fraction and superplasticizer content were analyzed after various pre-shear histories, i.e., mixing times. Yield stress and viscosity were measured in a parallel-plate-rheometer and related to in-situ measurements of the chord length distribution with the FBRM-probe to characterize the agglomeration status. With increasing mixing time agglomerates were increasingly broken up in dependence of pre-shear: After 300 s of pre-shear the agglomerate sizes decreased by 10 µm to 15 µm compared to a 30 s pre-shear. At the same time dynamic yield stress and viscosity decreased up to 30% until a state of equilibrium was almost reached. The investigations show a correlation between mean chord length and the corresponding rheological parameters affected by the duration of pre-shear.


Metals ◽  
2021 ◽  
Vol 11 (12) ◽  
pp. 1942
Author(s):  
Gerardo Aguilar ◽  
Gildardo Solorio-Diaz ◽  
Alicia Aguilar-Corona ◽  
José Angel Ramos-Banderas ◽  
Constantin A. Hernández ◽  
...  

The use of porous plugs in injecting gas through the bottom of a ladle forms vertical plumes in a very similar way to a truncated cone. The gas plume when exiting the plug has a smaller diameter compared to that formed in the upper zone of the ladle because inertial forces predominate over buoyancy forces in this zone. In addition, the magnitude of the plume velocity is concentrated in an upward direction, which increases the likelihood of low velocity zones forming near the bottom of the ladle, especially in lower corners. In this work, a plug with spiral-shaped channels with different torsion angles is proposed, with the objective that the gas, when passing through them, has a tangential velocity gain or that the velocity magnitude is distributed in the three axes and does not just focus on the upward direction, helping to decrease low velocity zones near the bottom of the ladle for better mixing times. For the experimentation, we worked in a continuous casting ladle water model with two configuration injections, which in previous works were reported as the most efficient in mixing the steel in this ladle. The results obtained using the PIV technique (particle image velocimetry) and conductimetry technique indicate that the plugs with the torsion channels at angles of 60° and 120° improve the mixing times for the two injection configurations.


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