scholarly journals Enhanced Interfacial Shear Strength and Critical Energy Release Rate in Single Glass Fiber-Crosslinked Polypropylene Model Microcomposites

Materials ◽  
2018 ◽  
Vol 11 (12) ◽  
pp. 2552 ◽  
Author(s):  
Uwe Gohs ◽  
Michael Mueller ◽  
Carsten Zschech ◽  
Serge Zhandarov

Continuous glass fiber-reinforced polypropylene composites produced by using hybrid yarns show reduced fiber-to-matrix adhesion in comparison to their thermosetting counterparts. Their consolidation involves no curing, and the chemical reactions are limited to the glass fiber surface, the silane coupling agent, and the maleic anhydride-grafted polypropylene. This paper investigates the impact of electron beam crosslinkable toughened polypropylene, alkylene-functionalized single glass fibers, and electron-induced grafting and crosslinking on the local interfacial shear strength and critical energy release rate in single glass fiber polypropylene model microcomposites. A systematic comparison of non-, amino-, alkyl-, and alkylene-functionalized single fibers in virgin, crosslinkable toughened and electron beam crosslinked toughened polypropylene was done in order to study their influence on the local interfacial strength parameters. In comparison to amino-functionalized single glass fibers in polypropylene/maleic anhydride-grafted polypropylene, an enhanced local interfacial shear strength (+20%) and critical energy release rate (+80%) were observed for alkylene-functionalized single glass fibers in electron beam crosslinked toughened polypropylene.

Materials ◽  
2019 ◽  
Vol 12 (23) ◽  
pp. 4015
Author(s):  
Hyuk Lee ◽  
Vanissorn Vimonsatit ◽  
Priyan Mendis ◽  
Ayman Nassif

This paper presents a study of parameters affecting the fibre pull out capacity and strain-hardening behaviour of fibre-reinforced alkali-activated cement composite (AAC). Fly ash is a common aluminosilicate source in AAC and was used in this study to create fly ash based AAC. Based on a numerical study using Taguchi’s design of experiment (DOE) approach, the effect of parameters on the fibre pull out capacity was identified. The fibre pull out force between the AAC matrix and the fibre depends greatly on the fibre diameter and embedded length. The fibre pull out test was conducted on alkali-activated cement with a capacity in a range of 0.8 to 1.0 MPa. The strain-hardening behaviour of alkali-activated cement was determined based on its compressive and flexural strengths. While achieving the strain-hardening behaviour of the AAC composite, the compressive strength decreases, and fine materials in the composite contribute to decreasing in the flexural strength and strain capacity. The composite critical energy release rate in AAC matrix was determined to be approximately 0.01 kJ/m 2 based on a nanoindentation approach. The results of the flexural performance indicate that the critical energy release rate of alkali-activated cement matrix should be less than 0.01 kJ/m 2 to achieve the strain-hardening behaviour.


2010 ◽  
Vol 24 (01n02) ◽  
pp. 164-174 ◽  
Author(s):  
SHANE ZHI YUAN LOO ◽  
PUAY CHENG LEE ◽  
ZAN XUAN LIM ◽  
NATALIA YANTARA ◽  
TONG YAN TEE ◽  
...  

In the current work, a test scheme to evaluate solder joint interface fracture toughness using double cantilever beam (DCB) test has been successfully demonstrated. The obtained results, in terms of critical energy release rate, predict the joint failure based on the principle of fracture mechanics. The results can be used as a materials property in the reliability design of various types of solder-ball joined packages. DCB specimens made of 99.9 wt% copper were selected in the current work. Eutectic Sn -37 Pb and lead-free Sn -3.5 Ag -0.5 Cu solders were used to join two pieces of the copper beams with controlled solder thickness. The test record showed steady propagation of the crack along the solder / copper interface, which verifies the viability of such a testing scheme. Interface fracture toughness for as-joined, extensively-reflowed and thermally aged samples has been measured. Both the reflow treatment and the thermal aging lead to degradation of the solder joint fracture resistance. Reflow treatment was more damaging as it induces much faster interface reaction. Fractographic analysis established that the fracture has a mixed micromechanism of dimple and cleavage. The dimples are formed as a result of the separation between the hard intermetallic compound (IMC) particles and the soft solder material, while the cleavage is formed by the brittle split of the IMCs. When the IMC thickness is increased due to extended interface reaction, the proportion of IMC cleavage failure increases, and this was reflected in the decrease of the critical energy release rate.


2012 ◽  
Vol 525-526 ◽  
pp. 409-412 ◽  
Author(s):  
Guo Wei Zhu ◽  
Yu Xi Jia ◽  
Peng Qu ◽  
Jia Qi Nie ◽  
Yun Li Guo

Delamination is a particularly dangerous damage mode of high performance laminated composites. In order to describe the composites ductile cracking and its progressive evolution accurately, the adjusted exponential cohesive zone model (CZM) is adopted, which correlates the tensile traction with the corresponding interfacial separation along the fracturing interfacial zone. At first the adjusted exponential CZM is used to simulate the mode I delamination of the standard double cantilever beam (DCB). The simulated results are in good agreement with the corrected beam theory and the corresponding experimental results. Then in order to research how the interfacial properties influence the mode I fracture, the interfacial strength and the critical energy release rate are studied. The main results are obtained as follows. The interfacial strength plays a crucial role in the laminated composites delamination onset, and it affects the peak load significantly if there is not a pre-crack. Once the delamination propagation begins to occur in the laminated composites, the responses of the load-displacement plots are relatively insensitive to the interfacial strength, and only the critical energy release rate is of critical importance. Furthermore, the peak load increases with the increase of the critical energy release rate and interfacial strength.


Author(s):  
Vincent Robin ◽  
Philippe Gilles ◽  
Philippe Mourgue ◽  
David Tchoukien

Some flaws may appear in metal components, in the weld region, and more especially in the case of electron beam girth weld in the slope area of the process (start and stop of the welding operation). These initial flaws can growth with delay even without any external loads. Indeed close to the junction, the material undergoes the combination of high tensile residual stresses due to welding operation and the presence of hydrogen brought by manufacturing process. Hydrogen assisted cracking is then suspected to explain the origin of crack growth through hydrogen embrittlement of the base metal. To understand by numerical modeling, at least qualitatively, the scenario of appearance of such cracks and their evolution, without any external load or under pressure load, the proposed approach consists first in simulating the welding process and its consequences on residual stress distribution and hydrogen concentrations [1]. The hydrogen diffusion computation is pursued after the welding operation simulation in order to highlight the most critical moment at which macroscopic defects may appear. Then, a macroscopic defect is created in the so determined critical zone, the stability of which is studied by estimating the energy release rate at the crack front and by comparing these values with experimental data such as the critical energy release rate at initiation and the tearing resistance curves which may depend on the hydrogen content. So, it is numerically possible to propagate the defect in the time, considering hydrogen diffusion and residual stress rebalancing, by successive crack front definition performed as the crack tip region exceeds the critical energy release rate [14]. Finally, the evolution of the defect is estimated in the same way under pressure test loading conditions. Results and discussions are presented to propose an engineering approach for the design assessment of such specific weld junctions with a low and hydrogen dependant toughness.


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