scholarly journals Effect of Exclusive Primer and Adhesive on Microtensile Bond Strength of Self-Adhesive Resin Cement to Dentin

Materials ◽  
2020 ◽  
Vol 13 (10) ◽  
pp. 2353
Author(s):  
Bit-Na Kim ◽  
Sung-Ae Son ◽  
Jeong-Kil Park

The aim of this study was to investigate the effect of G-CEM One Primer (GCOP) and self-etching adhesive on the microtensile bond strength (µTBS) between self-adhesive resin cement G-CEM One (GCO) and dentin. Teeth were sectioned to expose the flat dentin surface and randomly assigned into five groups (n = 15) according to the dentin surface treatment: 1) no surface treatment, 2) GCOP, 3) All-Bond Universal (ABU), 4) GCOP followed by ABU (GCOP/ABU), 5) ABU followed by GCOP (ABU/GCOP). The composite resin blocks were bonded to the dentin surface using GCO. The specimens were stored in distilled water at 37 °C for 24 h, then sectioned into sticks (1 mm × 10 mm). The μTBS values were statistically analyzed using 1-way analysis of variance (ANOVA) and Tukey’s honestly significant difference (HSD) test (α = 0.05) and failure mode was examined under a stereomicroscope. The bonding interface of each specimen was evaluated using confocal laser scanning microscopy. The GCOP group exhibited the highest µTBS value and there were no significant differences observed between GCOP, GCOP/ABU, ABU/GCOP groups (p > 0.05). The use of GCOP with GCO results in the improved µTBS between GCO and dentin. In conclusion, using only GCOP with GCO for bonding of indirect restoration is extremely simple and increasing bond strength.

2019 ◽  
Vol 21 (5) ◽  
pp. 477-482
Author(s):  
Lucas Campagnaro Maciel ◽  
Amanda Pádua Proeza ◽  
Hélyda Coelho Guimarães Balbino ◽  
Marcela Moráo Corteletti ◽  
Ricardo Huver De Jesus ◽  
...  

AbstractThe evolution of dental materials and the improvement of ceramic systems stimulated the increased use of Y-TZP zirconia-based ceramics. Despite the excellent mechanical performance, this material has low adhesion potential. The objective of this work was to evaluate the surface treatments and resin cements influence on bond strength between Y-TZP zirconia and composite resin interface. A total of 60 blocks of Y-TZP zirconia (3x8x8mm) were prepared and divided into 3 groups according to the surface treatments: (C) control - extra fine diamond bur, (J) sandblasting with Al2O3 and (JP) sandblasting with Al2O3 + ceramic primer. Each group was subdivided into two groups according to type of resin cement used for cementing composite resin discs (2mm thick x 5mm diameter): self-adhesive and conventional (n=10). The samples were stored in distilled water for 24 hours at 37±1°C in a incubator and subsequently submitted to the shear bond test to determine the bond strength (RU). There was no significant difference in RU among the  surface treatments when using conventional resin cement. For the self-adhesive resin cement, Al2O3 blasting and Al2O3 + primer blasting increased the RU but did not present significant differences between them (p<0.05). Comparing the cements, it was observed that regardless of the surface treatment, the highest values were for the self-adhesive resin cement (p<0.05). Application of the primer after blasting with Al2O3 did not increase RU. Keywords: Dental Prosthesis. Ceramics. Dental cements. Shear Strength.  ResumoA evolução dos materiais odontológicos e o aprimoramento dos sistemas cerâmicos impulsionaram o aumento da utilização da cerâmica a base de zircônia Y-TZP. Apesar do excelente desempenho mecânico, este material apresenta baixo potencial de adesão. O objetivo deste trabalho foi avaliar a influência dos tratamentos de superfícies e dos cimentos resinosos na resistência de união entre a interface zircônia Y-TZP e resina composta. Foram confeccionados 60 blocos de zircônia Y-TZP (3x8x8 mm) e divididos em 03 grupos de acordo com os tratamentos de superfícies que receberam: (C) controle - ponta diamantada extrafina, (J) jateamento com Al2O3 e (JP) jateamento com Al2O3 + primer cerâmico. Cada grupo foi subdividido em dois novos grupos de acordo com tipo de cimento resinoso utilizado para cimentação de discos de resina composta (2mm de espessura x 5mm de diâmetro): autoadesivo e resinoso convencional (n=10). As amostras foram armazenadas em água destilada por 24 horas a 37±1°C em estufa e posteriormente submetidas ao teste de cisalhamento para averiguar a resistência de união (RU). Não houve diferença significativa na RU entre os tratamentos de superfície quando utilizado o cimento resinoso convencional. Para o cimento resinoso autoadesivo o jateamento com Al2O3 e o jateamento de Al2O3 + primer aumentaram a RU porém não apresentaram diferenças significativas entre si (p<0,05). Comparando os cimentos observou-se que, independente do tratamento de superfície, os maiores valores foram para o cimento resinoso autoadesivo (p<0,05). A aplicação do primer após o jateamento com Al2O3 não proporcionou aumento da RU. Palavras-chave: Prótese Dentária. Cerâmica. Cimentos Dentários. Resistência ao Cisalhamento.


2020 ◽  
Vol 45 (4) ◽  
pp. E185-E195
Author(s):  
RV Machry ◽  
PE Fontana ◽  
TC Bohrer ◽  
LF Valandro ◽  
OB Kaizer

Clinical Relevance When luting relined fiber posts with self-adhesive cement, the surface treatment of the posts influences the adhesion of the fiber posts to root dentin. SUMMARY This study evaluated the effect of surface treatment and silanization of resin composite on the bond strength of relined fiber posts cemented with self-adhesive resin cement. Push-out and microtensile bond strength (MTBS) tests were performed in this study. The endodontic treatment of 80 single-rooted bovine teeth was first performed in the push- out test segment, followed by weakening the intracanal walls by diamond bur. Then, the glass fiber posts were adapted with resin composite to fill the root canals, followed by photoactivation and resin surface conditioning according to four different experimental conditions: no conditioning as control, 10% hydrofluoric acid, 35% hydrogen peroxide, or air abrasion with alumina particle (all groups were subdivided into “with silanization” or “without silanization,” thus totaling eight experimental groups). Self-adhesive resin cement was used for the post cementation. Four slices per tooth were obtained for the push-out tests. Next, 160 blocks of resin composite were first produced for the MTBS tests; their bonding surfaces were conditioned (as mentioned, ie, eight treatments), and they were cemented to each other. The 80 sets (n=10/treatment) were then cut into microbars (16/set): eight were immediately tested, while the other eight were thermocycled (12,000×) and stored (120 days) before MTBS. Failure modes and topographic analyses were performed after treatments. There was no statistically significant difference for the push-out results. In MTBS, surface treatment and silanization had a significant effect (p&lt;0.001). Aging decreased bond strength for all groups. Considering the aged groups, air abrasion promoted the highest values and silanization improved bond strength for all treatments except air abrasion. The alumina particle air abrasion of the relining resin composite promoted the highest bond strengths when luting with self-adhesive resin cement.


2016 ◽  
Vol 27 (5) ◽  
pp. 537-542 ◽  
Author(s):  
Amanda Mahammad Mushashe ◽  
◽  
Carla Castiglia Gonzaga ◽  
Leonardo Fernandes da Cunha ◽  
Adilson Yoshio Furuse ◽  
...  

Abstract The aim of this study was to evaluate the effect of enamel and dentin surface treatment on the micro-shear bond strength of self-adhesive cement. Seventy-two extracted third molars had their crowns embedded in acrylic resin and worn to obtain a flat enamel or dentin surface. The enamel and dentin specimens were randomly assigned to 8 groups (n=12) that were based on surface treatment (11.5% polyacrylic acid solution or no treatment), substrate condition (wet or dry) and storage period (1 day or 90 days), and treated accordingly. Cylinders (1 × 1 mm) were fabricated using self-adhesive resin cement (RelyX U200) following the manufacturer's instructions. The specimens were stored in distilled water at 37 °C for either 1 day or 90 days and subjected to micro-shear bond strength test (EMIC DL 2000 at 0.5 mm/min). After this, the failure type of the specimens was determined. Data were subjected to statistical analysis (a=0.05). According to the results, the 11.5% polyacrylic acid application decreased the bond strength in both enamel and dentin samples. The moist groups showed higher bond strength than the dry ones, regardless of the substrate and surface treatment. Storage period did not influence bond strength. In conclusion, surface treatment with 11.5% polyacrylic acid and absence of moisture decreased the bond strength of the resin-cement (RelyU200), regardless of the storage period.


2016 ◽  
Vol 95 (13) ◽  
pp. 1487-1493 ◽  
Author(s):  
N. Hirose ◽  
R. Kitagawa ◽  
H. Kitagawa ◽  
H. Maezono ◽  
A. Mine ◽  
...  

An experimental cavity disinfectant (ACC) that is intended to be used for various direct and indirect restorations was prepared by adding an antibacterial monomer 12-methacryloyloxydodecylpyridinum bromide (MDPB) at 5% into 80% ethanol. The antibacterial effectiveness of ACC and its influences on the bonding abilities of resin cements were investigated. To examine the antibacterial activity of unpolymerized MDPB, the minimum inhibitory and bactericidal concentrations (MIC and MBC) were determined for Streptococcus mutans, Lactobacillus casei, Actinomyces naeslundii, Parvimonas micra, Enterococcus faecalis, Fusobacterium nucleatum, and Porphyromonas gingivalis. Antibacterial activities of ACC and the commercial cavity disinfectant containing 2% chlorhexidine and ethanol (CPS) were evaluated by agar disk diffusion tests through 7 bacterial species and by MIC and MBC measurement for S. mutans. The effects of ACC and CPS to kill bacteria in dentinal tubules were compared with an S. mutans–infected dentin model. Shear bond strength tests were used to examine the influences of ACC on the dentin-bonding abilities of a self-adhesive resin cement and a dual-cure resin cement used with a primer. Unpolymerized MDPB showed strong antibacterial activity against 7 oral bacteria. ACC produced inhibition zones against all bacterial species similar to CPS. For ACC and CPS, the MIC value for S. mutans was identical, and the MBC was similar with only a 1-step dilution difference (1:2). Treatment of infected dentin with ACC resulted in significantly greater bactericidal effects than CPS ( P < 0.05, analysis of variance and Tukey’s honest significant difference test). ACC showed no negative influences on the bonding abilities to dentin for both resin cements, while CPS reduced the bond strength of the self-adhesive resin cement ( P < 0.05). This study clarified that the experimental cavity disinfectant containing 5% MDPB is more effective in vitro than the commercially available chlorhexidine solution to eradicate bacteria in dentin, without causing any adverse influences on the bonding abilities of resinous luting cements.


2014 ◽  
Vol 72 (8) ◽  
pp. 762-769 ◽  
Author(s):  
Edilausson Moreno Carvalho ◽  
Ceci Nunes Carvalho ◽  
Alessandro Dourado Loguercio ◽  
Darlon Martins Lima ◽  
José Bauer

Materials ◽  
2019 ◽  
Vol 12 (20) ◽  
pp. 3321 ◽  
Author(s):  
Dae-Sung Kim ◽  
Jong-Ju Ahn ◽  
Eun-Bin Bae ◽  
Gyoo-Cheon Kim ◽  
Chang-Mo Jeong ◽  
...  

The purpose of this study was to evaluate the effect of non-thermal atmospheric pressure plasma (NTP) on shear bond strength (SBS) between yttria-stabilized tetragonal zirconia polycrystal (Y-TZP) and self-adhesive resin cement. For this study, surface energy (SE) was calculated with cube-shaped Y-TZP specimens, and SBS was measured on disc-shaped Y-TZP specimens bonded with G-CEM LinkAce or RelyX U200 resin cylinder. The Y-TZP specimens were classified into four groups according to the surface treatment as follows: Control (no surface treatment), NTP, Sb (Sandblasting), and Sb + NTP. The results showed that the SE was significantly higher in the NTP group than in the Control group (p < 0.05). For the SBS test, in non-thermocycling, the NTP group of both self-adhesive resin cements showed significantly higher SBS than the Control group (p < 0.05). However, regardless of the cement type in thermocycling, there was no significant increase in the SBS between the Control and NTP groups. Comparing the two cements, regardless of thermocycling, the NTP group of G-CEM LinkAce showed significantly higher SBS than that of RelyX U200 (p < 0.05). Our study suggests that NTP increases the SE. Furthermore, NTP increases the initial SBS, which is higher when using G-CEM LinkAce than when using RelyX U200.


2016 ◽  
Vol 17 (2) ◽  
pp. 149-153 ◽  
Author(s):  
Cristina Parise Gré ◽  
Renan C de Ré Silveira ◽  
Shizuma Shibata ◽  
Carlo TR Lago ◽  
Luiz CC Vieira

ABSTRACT Aim This study evaluated the influence of a silane-coupling agent on the bond strength of a self-adhesive cement and a conventional resin cement to a lithium disilicate glass ceramic. Materials and methods A total of eight ceramic blocks were fabricated and divided into four groups (n = 2). In groups 1 and 3, ceramic surfaces were etched with hydrofluoric acid 10% for 20 seconds, rinsed for 30 seconds, and air-dried. One layer of a silane agent was applied onto all ceramic specimens and air-dried for 30 seconds. In groups 2 and 4, ceramic surfaces were etched with hydrofluoric acid, rinsed, and air-dried without application of the silane-coupling agent. The ceramic blocks were bonded to a block of composite with a self-adhesive resin cement or with a conventional resin cement, according to the manufacturer's instructions. After 24 hours in distilled water at 37°C, the specimens were sectioned perpendicular to the bonding interface area to obtain beams with a bonding area of 0.8 mm2 and submitted to a microtensile bond strength test at a crosshead speed of 0.5 mm/min. Data were statistically analyzed with one-way analysis of variance and the Games–Howell post hoc test (p = 0.05). Fractured specimens were examined under optical microscopy at 40× magnification. Results Silanization resulted in higher microtensile bond strength compared to groups without silane. No significant differences were found between the conventional resin cement and the self-adhesive resin cement with silane agent (p = 0.983), and without silane agent (p = 0.877). Conclusion Silanization appears to be crucial for resin bonding to a lithium disilicate-based ceramic, regardless of the resin cement used. The self-adhesive resin cement performed as well as the conventional resin cement. Clinical significance Applying one layer of a silane-coupling agent after etching the ceramic surface with hydrofluoric acid 10% enhanced the bond strength between resin cements and a glass ceramic. How to cite this article Gré CP, de Ré Silveira RC, Shibata S, Lago CTR, Vieira LCC. Effect of Silanization on Microtensile Bond Strength of Different Resin Cements to a Lithium Disilicate Glass Ceramic. J Contemp Dent Pract 2016;17(2):149-153.


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