scholarly journals Investigation on the Effect of Roasting and Leaching Parameters on Recovery of Gallium from Solid Waste Coal Fly Ash

Metals ◽  
2019 ◽  
Vol 9 (12) ◽  
pp. 1251 ◽  
Author(s):  
Jing Huang ◽  
Yingbin Wang ◽  
Guanxuan Zhou ◽  
Yu Gu

Coal fly ash (CFA) provides important resources of gallium, which is regarded as an irreplaceable material in many technologies. A prospective roasting reagent assisted acid leaching process was proposed for the purpose of extracting gallium. The extraction efficiency of gallium by NaF (sodium fluoride) roasting followed by HNO3 (nitric acid) leaching process was demonstrated. The effect of roasting temperature, roasting time, the NaF-CFA mass ratio, acid leaching temperature, acid leaching time, and acid concentration were investigated. The results revealed that under optimal conditions (roasting temperature of 800 °C, roasting time of 10 min, acid leaching in 2 mol/L HNO3 for 1 h, and the NaF-CFA mass ratio of 0.75:1), 94% of gallium was extracted. Compared to previous studies, the process is a cost-effective method which can greatly shorten reaction time. It can reduce environmental pollution as it requires fewer acid reagents with low concentration and additives. It is expected to provide a method for the extraction of gallium from CFA.

2014 ◽  
Vol 522-524 ◽  
pp. 1467-1470 ◽  
Author(s):  
Xiang Zhong Kong ◽  
Hua Ye ◽  
Yu Qin

Sulfate roasting and dilute sulphuric acid leaching were applied to extract lithium from lepidolite. Several conditions including roasting temperature, roasting time, K2SO4and CaO were investigated to improve the lithium extraction efficiency, the final lithium extraction efficiency could attain 94% with the conditions as follows: roasting temperature 850°C, roasting time 2 h, K2SO4to lepidolite mass ratio 0.15 and CaO to lepidolite mass ratio 0.75.


2010 ◽  
Vol 113-116 ◽  
pp. 2039-2044 ◽  
Author(s):  
Wen Ning Mu ◽  
Yu Chun Zhai

A technology was studied to prepare -alumina from fly ash, and the integrated process flow including sintering with sulfuric acid, leaching, recrystallization, calcination was established in this paper. The influences including the particle size of fly ash, sintering temperature, sintering time and the mass ratio of sulfuric acid to fly ash on the extraction ratio of alumina were investigated and discussed during sintering process, and the optimal parameters were determined. The product of -alumina was examined by chemical analysis, XRD and SEM, and the results show that α-alumina reach the national standards.


2021 ◽  
Vol 100 (8) ◽  
pp. 102-109
Author(s):  
Ulung Muhammad SUTOPO ◽  
Erda Rahmilaila DESFITRI ◽  
Farrah Fadhillah HANUM ◽  
Yukio HAYAKAWA ◽  
Shinji KAMBARA

Metals ◽  
2017 ◽  
Vol 7 (7) ◽  
pp. 272 ◽  
Author(s):  
Shenyong Li ◽  
Shenjun Qin ◽  
Lianwei Kang ◽  
Jianjun Liu ◽  
Jing Wang ◽  
...  

2000 ◽  
Vol 42 (5-6) ◽  
pp. 79-85 ◽  
Author(s):  
P. Ricou-Hoeffer ◽  
V. Héquet ◽  
I. Lécuyer ◽  
P. Le Cloirec

Experimental design methodology was used to define conditions for the adsorption and the stabilization of nickel ions (initial concentration of 500 mg.L-1) on coal fly ash/lime sorbent. This type of sorbent allows the reuse of by-products and increases the stabilization of metallic ions by lime addition. It was shown that the solution pH, the metal/adsorbent mass ratio, the type of fly ash used as sorbent, and the fly ash/lime mass ratio are the most influential factors. A set of parameters was finally obtained (pH 5, metal/adsorbent ratio of 0.01 g.g-1, fly ash/lime ratio of 4 g.g-1, fly ash with the lowest content of iron oxide) for which the removal of Ni2+ is 96% and the leaching 0.03% by permuted water and 0.2% by acid solution of pH 2.


2017 ◽  
Vol 169 ◽  
pp. 418-425 ◽  
Author(s):  
Yanxia Guo ◽  
Zesen Zhao ◽  
Qian Zhao ◽  
Fangqin Cheng
Keyword(s):  
Fly Ash ◽  

2015 ◽  
Vol 57 (23) ◽  
pp. 10894-10904 ◽  
Author(s):  
Long Yan ◽  
Junfei Shang ◽  
Yufei Wang ◽  
Jian Li ◽  
Huijin Liu ◽  
...  

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