Paints and varnishes. Buchholz indentation test

1976 ◽  
Keyword(s):  
2021 ◽  
Vol 11 (1) ◽  
Author(s):  
Matthias Weber ◽  
Markus Alexander Rothschild ◽  
Anja Niehoff

AbstractCompared to articular cartilage, the biomechanical properties of costal cartilage have not yet been extensively explored. The research presented addresses this problem by studying for the first time the anisotropic elastic behavior of human costal cartilage. Samples were taken from 12 male and female cadavers and unconfined compression and indentation tests were performed in mediolateral and dorsoventral direction to determine Young’s Moduli EC for compression and Ei5%, Ei10% and Eimax at 5%, 10% and maximum strain for indentation. Furthermore, the crack direction of the unconfined compression samples was determined and histological samples of the cartilage tissue were examined with the picrosirius-polarization staining method. The tests revealed mean Young’s Moduli of EC = 32.9 ± 17.9 MPa (N = 10), Ei5% = 11.1 ± 5.6 MPa (N = 12), Ei10% = 13.3 ± 6.3 MPa (N = 12) and Eimax = 14.6 ± 6.6 MPa (N = 12). We found that the Young’s Moduli in the indentation test are clearly anisotropic with significant higher results in the mediolateral direction (all P = 0.002). In addition, a dependence of the crack direction of the compressed specimens on the load orientation was observed. Those findings were supported by the orientation of the structure of the collagen fibers determined in the histological examination. Also, a significant age-related elastic behavior of human costal cartilage could be shown with the unconfined compression test (P = 0.009) and the indentation test (P = 0.004), but no sex effect could be detected. Those results are helpful in the field of autologous grafts for rhinoplastic surgery and for the refinement of material parameters in Finite Element models e.g., for accident analyses with traumatic impact on the thorax.


2019 ◽  
Vol 813 ◽  
pp. 171-177 ◽  
Author(s):  
Giacomo Maculotti ◽  
Gianfranco Genta ◽  
Massimo Lorusso ◽  
Maurizio Galetto

Selective Laser Melting (SLM) is one of the leader metal Additive Manufacturing (AM) processes thanks to its capability of coupling freeform design and environmental and economical sustainability to high mechanical properties. AlSi10Mg is a light weight Al-alloy with interesting processing properties and enhanced strength thanks to the presence of Mg, which, hence, finds application in several industrial fields. Furthermore, SLM allows overcoming those design constraints set by casting and melt spinning; however, SLM AlSi10Mg components require to be heat treated, both to strengthen the material and to engineer the microstructure. In this work, in order to assess the effectiveness of heat treatments on AlSi10Mg by SLM, an ad hoc analysis procedure based on statistical tools is applied in combination with indentation characterisation tests. In particular, to achieve full scale characterisation, traditional Brinell hardness and Instrumented Indentation Test (IIT) in macro and nano-range are considered. In particular, IIT is applied both at the lower end of macro range to provide consistency and statistically investigate relationship with Brinell scale and in the nano-range, enabling local, i.e. grain, and surface properties to be characterised.


2009 ◽  
Vol 24 (3) ◽  
pp. 784-800 ◽  
Author(s):  
Ling Liu ◽  
Nagahisa Ogasawara ◽  
Norimasa Chiba ◽  
Xi Chen

Indentation is widely used to extract material elastoplastic properties from measured force-displacement curves. Many previous studies argued or implied that such a measurement is unique and the whole material stress-strain curve can be measured. Here we show that first, for a given indenter geometry, the indentation test cannot effectively probe material plastic behavior beyond a critical strain, and thus the solution of the reverse analysis of the indentation force-displacement curve is nonunique beyond such a critical strain. Secondly, even within the critical strain, pairs of mystical materials can exist that have essentially identical indentation responses (with differences below the resolution of published indentation techniques) even when the indenter angle is varied over a large range. Thus, fundamental elastoplastic behaviors, such as the yield stress and work hardening properties (functions), cannot be uniquely determined from the force-displacement curves of indentation analyses (including both plural sharp indentation and deep spherical indentation). Explicit algorithms of deriving the mystical materials are established, and we qualitatively correlate the sharp and spherical indentation analyses through the use of critical strain. The theoretical study in this paper addresses important questions of the application range, limitations, and uniqueness of the indentation test, as well as providing useful guidelines to properly use the indentation technique to measure material constitutive properties.


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