scholarly journals Fabrication of Custom-Designed and Cost-Effective Spin-Spray Pyrolysis Unit

In this paper, an efficient, spin-spray pyrolysis unit is designed and constructed for the deposition of oxide thin films. The system is an effective combination of two independent techniques such as spin and spray methods. The rotation of the substrate by keeping the spray nozzle stationary makes the system unique. The system allows the decomposition of the solution before reaching the substrate. Spin-spray pyrolysis unit is capable of coating thin films on different substrates like float glass, FTO coated glass, and Aluminum coated glass, Teflon, and kepton, of dimensions up to 4-inch diameter, any contour and scalable to industrial applications. Metal oxides like Al2O3, GZO, ZnO etc., can be coated for many applications such as solar cells, thin-film transistors, sensors, etc. The elements required for construction of spray pyrolysis units are a heater, spray nozzle, thermocouple, solution feeding unit, airflow assembly, substrate rotator, and exhaust assembly. The elements of the system are discussed in accordance with the cost estimation. The working principle of each element of the system is explained in a separate block diagram. The system is optimized for deposition of ZnO thin films on a glass substrate and is characterized. The thinfilms can be used for development of TFT’s, heaters, thermistors, piezo-electronics devices, sensors, antireflection coatings and solar cell.

2011 ◽  
Author(s):  
V. Chaitra ◽  
K. S. Shamala ◽  
V. Uma ◽  
Alka B. Garg ◽  
R. Mittal ◽  
...  

2009 ◽  
Vol 79-82 ◽  
pp. 803-806
Author(s):  
Jing Kai Yang ◽  
Hong Li Zhao ◽  
Yan Li Liu ◽  
Fu Cheng Zhang

The cold spray TiO2 thin films were deposited on 5mm-thick float glass substrates using the sol containing nano-anatase TiO2. The effects of different heat treatment temperatures on optical properties were discussed. The properties of xerogel powder were analyzed using TG-DSC, the morphology and structure of TiO2 thin films were characterized by FESEM and XRD, the transmittance and absorption of TiO2 coated glass were investigated by UV-vis spectrophotometer. The results reveal that TiO2 in the film is still anatase phase after heat treatment at 350°C and 500°C. With the annealing temperatures increasing from 20°C to 500°C, the average crystal size increases just from 21.4 nm to 23.9nm, UV absorption of TiO2 coated glass increases from 2.2 to 2.7, visible light transmittance is high to about 80%.


2019 ◽  
Vol 11 (4) ◽  
pp. 04015-1-04015-6
Author(s):  
H. S. Gavale ◽  
◽  
M. S. Wagh ◽  
S. R. Gosavi ◽  
◽  
...  

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