The Use of High Energies Radiations to Characterise Solid-Liquid Systems

Author(s):  
F.O. Arouca ◽  
João Jorge Ribeiro Damasceno
2005 ◽  
Vol 498-499 ◽  
pp. 49-54 ◽  
Author(s):  
Fábio de Oliveira Arouca ◽  
João Jorge Ribeiro Damasceno

The behavior of an isothermal and non-reaction solid-liquid system can be model using a mathematical model based on the Mixtures’ Theory of Continuum Mechanics. The knowledge of the constitutive equations of this phenomenon, as pressure on the solids and medium permeability, is very important in the design and performance evaluation of the continuous thickeners or filters. In this work the batch sedimentation phenomena of a kaolin aqueous suspensions was investigated. The technique consists on measuring of the gamma rays attenuation when they cross the physical media as a function of the local concentration at several vertical positions in a reservoir. Using the experimental data and local concentration as a function of the attenuation curve, it is possible to determine the constitutive equations. The results were satisfactory, allowing simulations of this phenomenon for steady and transient regimes in future papers.


2006 ◽  
Author(s):  
Bhagavatula Venkata Ramana Murthy

Fluidized beds are widely used in industries for mixing solid particles with liquids as the solid is vigorously agitated by the liquid passing through the bed and the mixing of the solid ensures that there are practically no temperature gradients in the bed even with exothermic or endothermic reactions (Mixing and the segregation in a liquid fluidized of particles with different sizes and densities", The Canadian Journal of Chemical Engineering, 1988). The violent motion of the solid particles also gives high heat transfer rates to the wall or to cooling tubes immersed in the bed. Because of the fluidity of the solid particles, it is easy to pass solid from one vessel to another. In the present experimental work, the relative density between solid and liquid phases on pressure drop under fluidized condition has been studied using the solid-liquid systems namely, glass beads-water, glass beads-kerosene, plastic beads-kerosene and diamond sugar-kerosene. Pressure drop - liquid velocity and void fraction - liquid velocity relationships have been found for all the mentioned solid-liquid systems under fluidized condition and results have been noted. The effect of the nature of the fluid on the minimum fluidization velocity and the pressure drop has been studied. In addition to the pressure drop studies, mass transfer studies have also been conducted with diamond sugar-water system with and without fluidization and results have been obtained. In addition to these, comparison of bed voidage, pressure drop and minimum fluidization velocity between denser and lighter liquids have been studied and the results have been obtained. Also, the value of rate of mass transfer with fluidization is compared that without fluidization for diamond sugar-water system and the results have been obtained.


2003 ◽  
Vol 68 (1) ◽  
pp. 9-16 ◽  
Author(s):  
Nada Nikolic ◽  
Mihajlo Stankovic

Dried and milled haulm of potato (Solanum tuberosum L) was used as the solid phase. An ethanolic solution of hydrochloric acid mixed with chloroform in different volume ratios was the liquid phase. The aim of paper was to unite in a single step the processes of glycoalkaloids extraction from haulm, their hydrolysis to solanidine and the extraction of solanidine. This could make the procedure of obtaining solanidine faster and simpler. The best degree of solanidine hydrolytic extraction of 84.5% was achieved using 10% w/v hydrochloric acid in 96% vol. ethanol mixed with chloroform in a volume ratio of 2:3, after 120 min of hydrolytic extraction.


Author(s):  
Rufat Abiev

Analysis of hydrodynamics and mass transfer Taylor flows in micro channels of both gas-liquid and liquid-liquid systems on the basis of classical theoretical approach with some simplifying assumptions was performed. Results of theoretical analysis for description of hydrodynamic parameters and mass transfer characteristics were confirmed by comparison with the author's own and available in literature experimental data. It was shown that the main parameters of two-phase Taylor flows could be quite precisely described theoretically: mean bubble/droplet velocity, liquid film thickness, real gas holdup (which is always smaller than so-called dynamic holdup), pressure drop. Peculiarities of liquid-liquid flows compared to gas-liquid Taylor flows in capillaries are discussed. Wettability effect on hydrodynamics was examined. Tools of mass transfer intensification of gas-liquid and liquid-liquid Taylor flow in micro channels are analyzed. Three-layer model for heat and mass transfer has been proposed and implemented for the case of solid-liquid mass transfer for gas-liquid Taylor flows; optimal process conditions for this process are found theoretically and discussed from physical point of view.


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