Particle Size Distribution of ZrO2:Pr3+ – Influences of pH, High Power Ultrasound, Surfactant and Dopant Quantity

2007 ◽  
pp. 97-100
Author(s):  
Stephanie Möller ◽  
Janusz D. Fidelus ◽  
Witold Łojkowski
Keyword(s):  
Particle Size ◽  
Particle Size Distribution ◽  
Size Distribution ◽  
High Power ◽  
Power Ultrasound ◽  
High Power Ultrasound

Particle Size Distribution of ZrO2:Pr3+ – Influences of pH, High Power Ultrasound, Surfactant and Dopant Quantity

2007 ◽  
Vol 128 ◽  
pp. 97-100 ◽  
Author(s):  
Stephanie Möller ◽  
Janusz D. Fidelus ◽  
Witold Łojkowski
Keyword(s):  
Particle Size ◽  
Particle Size Distribution ◽  
Size Distribution ◽  
High Power ◽  
Average Particle Size ◽  
Sodium Dodecyl ◽  
Average Particle ◽  
Power Ultrasound ◽  
High Power Ultrasound ◽  
Influence Of Ph

The aim of the work was to examine the influence of pH, high power ultrasound, surfactant and dopant quantity on the particle size distribution of ZrO2:Pr3+, with praseodymium content varying between 0.05 and 10 %. The nanopowders were obtained via a hydrothermal microwave driven process. To establish if the dopant was located on the surface of the zirconia nanoparticles, the particle size distribution, as a function of pH, was measured to obtain an estimate of the isoelectric point of the samples. All results indicated that the dopant was concentrated on the surface: the measurements of the particle size distribution show that the pH corresponding to maximum average particle size changes towards higher values when the Pr content increases. Measurements of the particle size distribution dependency on the application of high power ultrasound and the addition of the sodium dodecyl sulphate surfactant show that, under certain conditions, there is a better stabilisation of the nanopowders in a dispersion and undesirable agglomeration is hindered.

scholarly journals Aerosol droplet-size distribution and airborne nicotine portioning in particle and gas phases emitted by electronic cigarettes

2020 ◽  
Vol 10 (1) ◽  
Author(s):  
Hélène Lalo ◽  
Lara Leclerc ◽  
Jérémy Sorin ◽  
Jérémie Pourchez
Keyword(s):  
Particle Size ◽  
Particle Size Distribution ◽  
Low Power ◽  
Size Distribution ◽  
High Power ◽  
Electronic Cigarettes ◽  
Power Level ◽  
Particle Phase ◽  
Experimental Conditions ◽  
Aerosol Droplet

AbstractThe reliable characterization of particle size distribution and nicotine delivery emitted by electronic cigarettes (ECs) is a critical issue in their design. Indeed, a better understanding of how nicotine is delivered as an aerosol with an appropriate aerodynamic size is a necessary step toward obtaining a well-designed nicotine transfer from the respiratory tract to the bloodstream to better satisfy craving and improve smoking cessation rates. To study these two factors, recent models of EC devices and a dedicated vaping machine were used to generate aerosols under various experimental conditions, including varying the EC power level using two different types of atomizers. The aerodynamic particle sizing of the resulting aerosol was performed using a cascade impactor. The nicotine concentration in the refill liquid and the aerosol droplet was quantified by liquid chromatography coupled with a photodiode array. The vaporization process and the physical and chemical properties of the EC aerosol were very similar at 15 watts (W) and 25 W using the low-power atomizer but quite distinct at 50 W using the high-power atomizer, as follows: (1) the mass median aerodynamic diameters ranged from 1.06 to 1.19 µm (µm) for low power and from 2.33 to 2.46 µm for high power; (2) the nicotine concentrations of aerosol droplets were approximately 11 mg per milliliter (mg/mL) for low power and 17 mg/mL for high power; and (3) the aerosol droplet particle phase of the total nicotine mass emitted by EC was 60% for low power and 95% for high power. The results indicate that varying the correlated factors (1) the power level and (2) the design of atomizer (including the type of coil and the value of resistance used) affects the particle-size distribution and the airborne nicotine portioning between the particle phase and the gas phase in equilibrium with the airborne droplets.

Effects of Particle Size Distribution on Corrosion Rate of Carbon Steel in Soil

2020 ◽  
Vol 69 (4) ◽  
pp. 102-106
Author(s):  
Shota Ohki ◽  
Shingo Mineta ◽  
Mamoru Mizunuma ◽  
Soichi Oka ◽  
Masayuki Tsuda
Keyword(s):  
Particle Size ◽  
Carbon Steel ◽  
Corrosion Rate ◽  
Particle Size Distribution ◽  
Size Distribution

DENSE SPRAY CORRECTIONS FOR DIFFRACTION-BASED PARTICLE SIZE DISTRIBUTION MEASUREMENTS

1995 ◽  
Vol 5 (1) ◽  
pp. 75-87 ◽  
Author(s):  
Christine M. Woodall ◽  
James E. Peters ◽  
Richard O. Buckius
Keyword(s):  
Particle Size ◽  
Particle Size Distribution ◽  
Size Distribution

Influence of Cementite Particle Size Distribution on Machinability and Tool Life of High Carbon Cr-bearing Steels

1998 ◽  
Vol 84 (5) ◽  
pp. 387-392 ◽  
Author(s):  
Takashi INOUE ◽  
Yuzo HOSOI ◽  
Koe NAKAJIMA ◽  
Hiroyuki TAKENAKA ◽  
Tomonori HANYUDA
Keyword(s):  
Particle Size ◽  
Particle Size Distribution ◽  
Size Distribution ◽  
Tool Life ◽  
Cementite Particle ◽  
High Carbon ◽  
Bearing Steels

Study of the microstructure and particles of vanadium (III) oxide, vanadium (V) oxide and lithium aluminate powders

2020 ◽  
Vol 86 (1) ◽  
pp. 32-37
Author(s):  
Valeria A. Brodskaya ◽  
Oksana A. Molkova ◽  
Kira B. Zhogova ◽  
Inga V. Astakhova
Keyword(s):  
Particle Size ◽  
Particle Size Distribution ◽  
Vanadium Oxide ◽  
Size Distribution ◽  
Microstructural Analysis ◽  
Coherent Scattering ◽  
Powder Materials ◽  
Lithium Aluminate ◽  
Range Limit ◽  
Oxide Particles

Powder materials are widely used in the manufacture of electrochemical elements of thermal chemical sources of current. Electrochemical behavior of the powders depends on the shape and size of their particles. The results of the study of the microstructure and particles of the powders of vanadium (III), (V) oxides and lithium aluminate obtained by transmission electron and atomic force microscopy, X-ray diffraction and gas adsorption analyses are presented. It is found that the sizes of vanadium (III) and vanadium (V) oxide particles range within 70 – 600 and 40 – 350 nm, respectively. The size of the coherent-scattering regions of the vanadium oxide particles lies in the lower range limit which can be attributed to small size of the structural elements (crystallites). An average volumetric-surface diameter calculated on the basis of the surface specific area is close to the upper range limit which can be explained by the partial agglomeration of the powder particles. Unlike the vanadium oxide particles, the range of the particle size distribution of the lithium aluminate powder is narrower — 50 – 110 nm. The values of crystallite sizes are close to the maximum of the particle size distribution. Microstructural analysis showed that the particles in the samples of vanadium oxides have a rounded (V2O3) or elongated (V2O5) shape; whereas the particles of lithium aluminate powder exhibit lamellar structure. At the same time, for different batches of the same material, the particle size distribution is similar, which indicates the reproducibility of the technologies for their manufacture. The data obtained can be used to control the constancy of the particle size distribution of powder materials.

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