Fabrication of High Performance Geopolymer Ceramic Part I - Microstructural Properties

2015 ◽  
Vol 754-755 ◽  
pp. 698-702 ◽  
Author(s):  
Romisuhani Ahmad ◽  
Mohd Mustafa Al Bakri Abdullah ◽  
Kamarudin Hussin ◽  
Andrei Victor Sandu ◽  
Mohammed Binhussain ◽  
...  
Keyword(s):  
Powder Metallurgy ◽  
High Performance ◽  
Sintered Sample ◽  
Microstructural Properties ◽  
Powder Metallurgy Technique ◽  
Electron Microscopic ◽  
X Ray ◽  
Scanning Electron Microscopic ◽  
Alkaline Activator ◽  
Scanning Electron

Geopolymer ceramic have been produced by the powder metallurgy (PM) technique. The samples were reacted by the alkaline activator to activate the geopolymerization process and crushed by using Mortar and Pestle to powderized the samples. Powder metallurgy technique was used and samples were heated at different temperature start from 700 °C until 1200°C and the strength were tested. The relative density and flexural strength of sintered sample ranged approximately 84%-95% and 20-100 MPa respectively. Microstructural properties was conducted by scanning electron microscopic (SEM) and the surface analysis by energy dispersive X-ray (EDX).

scholarly journals Preparation of Reswellable Amorphous Porous Celluloses through Hydrogelation from Ionic Liquid Solutions

Materials ◽  
2019 ◽  
Vol 12 (19) ◽  
pp. 3249 ◽  
Author(s):  
Satoshi Idenoue ◽  
Yoshitaka Oga ◽  
Daichi Hashimoto ◽  
Kazuya Yamamoto ◽  
Jun-ichi Kadokawa
Keyword(s):  
Mechanical Properties ◽  
Ionic Liquid ◽  
Amorphous Structure ◽  
X Ray Diffraction ◽  
Electron Microscopic ◽  
X Ray ◽  
Liquid Solutions ◽  
Scanning Electron Microscopic ◽  
Porous Morphology ◽  
Scanning Electron

In this study, we have performed the preparation of reswellable amorphous porous celluloses through regeneration from hydrogels. The cellulose hydrogels were first prepared from solutions with an ionic liquid, 1-butyl-3-methylimidazolium chloride (BMIMCl), in different concentrations. Lyophilization of the hydrogels efficiently produced the regenerated celluloses. The powder X-ray diffraction and scanning electron microscopic measurements of the products suggest an amorphous structure and porous morphology, respectively. Furthermore, the pore sizes of the regenerated celluloses, or in turn, the network sizes of cellulose chains in the hydrogels, were dependent on the concentrations of the initially prepared solutions with BMIMCl, which also affected the tensile mechanical properties. It was suggested that the dissolution states of the cellulose chains in the solutions were different, in accordance with the concentrations, which representatively dominated the pore and network sizes of the above materials. When the porous celluloses were immersed in water, reswelling was observed to regenerate the hydrogels.

scholarly journals Influence of the type of electrolyte on the morphological and crystallographic characteristics of lead powder particles

2013 ◽  
Vol 78 (9) ◽  
pp. 1387-1395 ◽  
Author(s):  
Nebojsa Nikolic ◽  
Vesna Maksimovic ◽  
Goran Brankovic ◽  
Predrag Zivkovic ◽  
Miomir Pavlovic
Keyword(s):  
X Ray Diffraction ◽  
Electron Microscopic ◽  
X Ray ◽  
Lead Powder ◽  
Scanning Electron Microscopic ◽  
Crystallographic Characteristics ◽  
Powder Particles ◽  
Primary Type ◽  
Secondary Type ◽  
Scanning Electron

Lead electrodeposition processes from the basic (nitrate) and complex (acetate) electrolytes were mutually compared by the scanning electron microscopic and the X-ray diffraction analysis of the produced powder particles. The shape of dendritic particles strongly depended on the type of electrolyte. The dendrites composed of stalk and weakly developed primary branches (the primary type) were predominantly formed from the basic electrolyte. The ramified dendrites composed of stalk and of both primary and secondary branches (the secondary type) were mainly formed from the complex electrolyte. In the both type of powder particles Pb crystallites were predominantly oriented in the (111) plane. Formation of powder particles of the different shape with the strong (111) preferred orientation was discussed and explained by the consideration of the general characteristics of the growth of a crystal in the electrocrystallization processes.

Scanning Electron Microscopic (SEM) Studies on the Effect of X-Ray Contrast Media on Aortic Endothelium in the Rat

1983 ◽  
Vol 18 (4) ◽  
pp. 382-386 ◽  
Author(s):  
CHRISTIAN GOSPOS ◽  
HERBERT KURT KOCH ◽  
K. MATHIAS ◽  
W. SEEMANN ◽  
K. G. TAN ◽  
...  
Keyword(s):  
Contrast Media ◽  
Electron Microscopic ◽  
X Ray ◽  
Aortic Endothelium ◽  
Scanning Electron Microscopic ◽  
Scanning Electron ◽  
Sem Studies
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