ZnO Nanostructures and Field Emission Properties on Cu Substrate Achieved by Electrodeposition Method

2011 ◽  
Vol 347-353 ◽  
pp. 3388-3391
Author(s):  
Jiang Feng Gong ◽  
Chang Yong Lan ◽  
Bo Zhang ◽  
Kai Xiao Zhang ◽  
Wei Hua Zhu

In the present work, ZnO nanostructures with tunable size were successfully synthesized on non-seeded Cu substrates by a simple electrodeposition method. The effects of growth conditions on the morphology of the products were studied in detail by scanning electron microscopy (SEM), and transmission electron microscopy (TEM). The as-prepared products exhibited flake-like morphology when the concentration of ZnCl2 was higher enough, while the products showed flower-like morphology when the concentration was lower enough. Field emission investigation indicated that the nanoflowers exhibited good emission properties. The ZnO nanoflowers show potential application as field emitters.

2000 ◽  
Vol 6 (3) ◽  
pp. 224-230
Author(s):  
Z.L. Wang ◽  
P. Poncharal ◽  
W.A. de Heer

Abstract Nanomaterials have attracted a great deal of research interest recently. The small size of nanostructures constrains the applications of well-established testing and measurement techniques, thus new methods and approaches must be developed for quantitative measurement of the properties of individual nanostructures. This article reports our progress in using in situ transmission electron microscopy to measure the electrical, mechanical, and field-emission properties of individual carbon nanotubes whose microstructure is well-characterized. The bending modulus of a single carbon nanotube has been measured by an electric field-induced resonance effect. A nanobalance technique is demonstrated that can be applied to measure the mass of a tiny particle as light as 22 fg (1 fg = 10−15 g), the smallest balance in the world. Quantum conductance was observed in defect-free nanotubes, which led to the transport of a superhigh current density at room temperature without heat dissipation. Finally, the field-emission properties of a single carbon nanotube are observed, and the field-induced structural damage is reported.


NANO ◽  
2011 ◽  
Vol 06 (05) ◽  
pp. 489-496 ◽  
Author(s):  
H. X. ZHONG ◽  
C. X. WANG

A simple hydrothermal route was employed to prepare flower-like SnS2 and In -doped SnS2 by using biomolecular L-cysteine as sulfur source. The synthetic samples were characterized by X-ray diffraction, scanning electron microscopy, high resolution transmission electron microscopy, X-ray photoelectron spectroscopy and Raman spectroscopy in detail. Furthermore, the field emission from both the materials was investigated, it was found that both of them have excellent field emission properties, and the doped In has enhanced the field emission properties.


2000 ◽  
Vol 6 (3) ◽  
pp. 224-230 ◽  
Author(s):  
Z.L. Wang ◽  
P. Poncharal ◽  
W.A. de Heer

AbstractNanomaterials have attracted a great deal of research interest recently. The small size of nanostructures constrains the applications of well-established testing and measurement techniques, thus new methods and approaches must be developed for quantitative measurement of the properties of individual nanostructures. This article reports our progress in using in situ transmission electron microscopy to measure the electrical, mechanical, and field-emission properties of individual carbon nanotubes whose microstructure is well-characterized. The bending modulus of a single carbon nanotube has been measured by an electric field-induced resonance effect. A nanobalance technique is demonstrated that can be applied to measure the mass of a tiny particle as light as 22 fg (1 fg = 10−15 g), the smallest balance in the world. Quantum conductance was observed in defect-free nanotubes, which led to the transport of a superhigh current density at room temperature without heat dissipation. Finally, the field-emission properties of a single carbon nanotube are observed, and the field-induced structural damage is reported.


2013 ◽  
Vol 9 (5) ◽  
pp. 619-623 ◽  
Author(s):  
Shama Parveen ◽  
Samina Husain ◽  
Avshish Kumar ◽  
Javid Ali ◽  
Mubashshir Husain ◽  
...  

2013 ◽  
Vol 34 (11) ◽  
pp. 1424-1429
Author(s):  
周雄图 ZHOU Xiong-tu ◽  
曾祥耀 ZENG Xiang-yao ◽  
张永爱 ZHANG Yong-ai ◽  
郭太良 GUO Tai-liang

2002 ◽  
Vol 728 ◽  
Author(s):  
Mark Ching-Cheng Lin ◽  
M.S. Lai ◽  
H. J. Lai ◽  
M. H. Yang ◽  
B.Y. Wei ◽  
...  

AbstractThe field emission properties of carbon nanotubes (CNTs) from various sources are investigated for the application of field emission displays. Comparisons are made between graphite with Ni metal as catalyst and polycyclic aromatic hydrocarbon as precursor by the arc discharge method. Cathode deposits are examined using scanning electron microscopy (SEM) and high-resolution transmission electron microscopy (HRTEM) to determine microstructure. Carbon structure is studied using Raman spectroscopy. Electron field emission characteristics are measured with the diode method at 10-6 torr pressure. In this study, SEM micrographs of cathode deposits show dense random fiber-like carbon nanotubes. The HRTEM images clearly exhibit characteristic features of multiwalled carbon nanotubes. Microstructural investigation provides evidence that both the metal catalyst and the precursor can be used to synthesize carbon nanotubes. The Raman spectrum shows a stronger peak at about 1580 cm-1 indicating formation of a well-graphitized carbon nanotube. The degree of carbon nanotube graphitization is high and is in good agreement with the HRTEM result. From field emission measurements, the lowest onset field is about 1.0 V/μm and can be attributed to highly sharp tips and the high density of carbon nanotubes. Based on microstructure characterization and field emission measurements, the influence on field emission properties including turn on voltage and threshold voltage of carbon nanotubes synthesized from different sources is discussed.


2017 ◽  
Vol 43 (15) ◽  
pp. 11753-11758 ◽  
Author(s):  
H. Algarni ◽  
Ahmad Umar ◽  
S.H. Kim ◽  
M.S. Al-Assiri ◽  
A.E. Al-Salami

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