Synthesis of Monodisperse CdSe QDs Using Controlled Growth Temperatures

2011 ◽  
Vol 364 ◽  
pp. 485-488 ◽  
Author(s):  
Mohammad Hafizuddin Haji Jumali ◽  
Razinah Rahmat Noor ◽  
Muhammad Yahaya ◽  
Muhamad Mat Salleh ◽  
Akrajas Ali Umar

This paper reports on the effect of growth temperatures on optical properties of monodisperse CdSe QDs synthesized via wet chemical method. The growth temperature was varied from 260 – 310 °C while growth period was fixed at 60 s. The resulting colloidal was in strong quantum confinement regime and having yield as high as 53%. As the growth temperature increased, the monodispersed CdSe QDs with diameter in the range of 3-7 nm were obtained. Both absorption and PL spectra of the QDs revealed a strong red-shift with the increment of growth temperature. Thus, the size of QDs was enlarged with increment of the wavelength from both the spectra. Consequently, the energy gap of resulting QDs can be tuned by tuning the size of QDs. More importantly, the narrow widths of the PL emissions with different colors make these colloidal to be a potential candidate for different optical and optoelectronic devices.

2015 ◽  
Vol 649 ◽  
pp. 50-53 ◽  
Author(s):  
K. Kaviyarasu ◽  
E. Manikandan ◽  
Z.Y. Nuru ◽  
M. Maaza

2014 ◽  
Vol 904 ◽  
pp. 25-28
Author(s):  
C. Lan ◽  
H. Wang ◽  
Z.Y. Zhong ◽  
T. Zhang ◽  
C.Y. Yang ◽  
...  

Transparent conducting gallium doped zinc oxide (GaZnO) films were prepared by magnetron sputtering technique. The influence of growth temperature on the microstructural and optical properties of the films were investigated by means of X-ray diffraction (XRD), spectrophotometer and optical characterization method, respectively. The results show that all the samples are polycrystalline in nature having a hexagonal wurtzite type crystal structure with a preferred grain orientation in the (002) direction. The growth temperature significantly affects the crystal structure and optical properties of the samples. The film deposited at the growth temperature of 670 K possesses the largest grain grain, the minimum dislocation density and the lowest microstrain. The average visible transmittance and optical energy gap of the samples increase gradually with the increment of growth temperature.


2013 ◽  
Vol 2013 ◽  
pp. 1-5 ◽  
Author(s):  
Jutarat Kavinchan ◽  
Titipun Thongtem ◽  
Somchai Thongtem ◽  
Eksuree Saksornchai

Antimony sulfide (Sb2S3) was successfully synthesized from antimony chloride (SbCl3) and sodium thiosulfate pentahydrate (Na2S2O3·5H2O) in ethylene glycol (EG) without using any template by a facile wet-chemical method. X-ray diffraction (XRD), scanning electron microscopy (SEM), and transmission electron microscopy (TEM) show that the products were orthorhombic Sb2S3nanorods forming the coral-like, straw-tied-like, and flower-like architectures with the nanorods growing along the [001] direction. The energy gap (Eg) was determined by UV-visible absorption to be 1.52 eV.


Author(s):  
Jose Eduardo Barcelon ◽  
Marco Smerieri ◽  
Giovanni Carraro ◽  
Pawel Wojciechowski ◽  
Luca Vattuone ◽  
...  

Graphene nanoribbons (GNRs) are at the frontier of research on graphene materials since the 1D quantum confinement of electrons allows for the opening of an energy gap.


Ionics ◽  
2021 ◽  
Vol 27 (4) ◽  
pp. 1465-1475
Author(s):  
Ning Zhang ◽  
Ying Li ◽  
Yadan Luo ◽  
Zhen Yang ◽  
Jiayao Lu

RSC Advances ◽  
2016 ◽  
Vol 6 (60) ◽  
pp. 55546-55551 ◽  
Author(s):  
Shu-Qing Lv ◽  
Ya-Fei Pan ◽  
Pei-Bo Yang ◽  
Guang-Sheng Wang

By using a simple wet chemical method and hot-molding procedure, a kind of flexible film with enhance absorption properties based on binary cobalt nanochains/polyvinylidene fluoride (PVDF) hybrids has been successfully fabricated.


2010 ◽  
Vol 500 (2) ◽  
pp. L17-L21 ◽  
Author(s):  
Shao-Hwa Hu ◽  
Yi-Chuan Chen ◽  
Chyi-Ching Hwang ◽  
Cheng-Hsiung Peng ◽  
Dah-Chuan Gong

2017 ◽  
Vol 8 ◽  
pp. 1257-1265 ◽  
Author(s):  
Urszula Klekotka ◽  
Magdalena Rogowska ◽  
Dariusz Satuła ◽  
Beata Kalska-Szostko

Ferrite nanoparticles with nominal composition Me0.5Fe2.5O4 (Me = Co, Fe, Ni or Mn) have been successfully prepared by the wet chemical method. The obtained particles have a mean diameter of 11–16 ± 2 nm and were modified to improve their magnetic properties and chemical activity. The surface of the pristine nanoparticles was functionalized afterwards with –COOH and –NH2 groups to obtain a bioactive layer. To achieve our goal, two different modification approaches were realized. In the first one, glutaraldehyde was attached to the nanoparticles as a linker. In the second one, direct bonding of such nanoparticles with a bioparticle was studied. In subsequent steps, the nanoparticles were immobilized with enzymes such as albumin, glucose oxidase, lipase and trypsin as a test bioparticles. The characterization of the nanoparticles was acheived by transmission electron microscopy, X-ray diffraction, energy dispersive X-ray and Mössbauer spectroscopy. The effect of the obtained biocomposites was monitored by Fourier transform infrared spectroscopy. The obtained results show that in some cases the use of glutaraldehyde was crucial (albumin).


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