Processing Effect on the Compressive Strength and Bioactivity of Ti-Based Composites Produced with TiH2 and Calcium Phosphate

2014 ◽  
Vol 906 ◽  
pp. 45-50
Author(s):  
Enori Gemelli ◽  
Fabio Nery ◽  
Nelson Heriberto Almeida Camargo ◽  
Vinicius André Rodrigues Henriques ◽  
Daiara Floriano da Silva

Titanium-based composites with bioactive phases were produced with TiH2and 10% in volume of calcium phosphate. The mixtures were prepared either by conventional powder metallurgy processing or by ultrasound, dried in a rotary evaporator, pressed at 600 MPa and vacuum-sintered at 1200 °C for 2 hours. Crystal phases of the as-fabricated composites are found to be α-Ti, CaTiO3and TixPyphase (s). The TixPyand CaTiO3phases resulted from the reaction between titanium and tricalcium phosphate at about 1130 °C. Calcium phosphate was better dispersed by ultrasound leading to a higher compressive strength of the composite and a more uniform Ca-P deposition in simulated body fluid solution.

2006 ◽  
Vol 309-311 ◽  
pp. 861-864 ◽  
Author(s):  
Byung Hyun Lee ◽  
Min Chul Kim ◽  
Kyoung Nam Kim ◽  
Kwang Mahn Kim ◽  
Seong Ho Choi ◽  
...  

In preliminary ageing test, the cement using only calcium phosphate glass as power phase cracked with 1 day in simulated body fluid because of high dissolution rate of the cement. We added 30 wt% of either β-TCP or HA to 70 wt% calcium phosphate glass as powder phase to control the dissolution rate of the cement and performed in vitro ageing test in simulated body fluid by dynamic protocol as well as static protocol to confirm the possibility of controlling. Adding either β-TCP or HA to the cement increases the setting time and decreases the compressive strength. In dynamic assay, the pH of extract is maintained over 7. However, pH decreased to around 5 in static assay. Therefore, weight loss by static protocol continuously increased for 14 days, while weight loss by dynamic protocol almost saturated. In XRD patterns of ageing cements, CaO peaks appeared. CaO peak was maximized most lately in dynamic assay of the cement adding HA and within 7 days, the cement adding HA showed higher weight loss. It is indicated that CaO formed in surface of the cement hinder the dissolution of the cement. In addition, compressive strength increased when the CaO peak was maximized.


Author(s):  
Thi Mai Thanh Dinh ◽  
Thi Thom Nguyen ◽  
Thi Nam Pham ◽  
Thu Phuong Nguyen ◽  
Thi Thu Trang Nguyen ◽  
...  

2015 ◽  
Vol 15 (5) ◽  
pp. 3887-3892 ◽  
Author(s):  
Dinh Thi Mai Thanh ◽  
Pham Thi Nam ◽  
Ho Thu Huong ◽  
Nguyen Thu Phuong ◽  
To Thi Xuan Hang ◽  
...  

Vacuum ◽  
2021 ◽  
pp. 110850
Author(s):  
Baishen Liu ◽  
Yaotian Yan ◽  
Jinghuang Lin ◽  
Jian Cao ◽  
Junlei Qi

2015 ◽  
Vol 280 ◽  
pp. 384-395 ◽  
Author(s):  
I. Mejía-Caballero ◽  
M. Palomar-Pardavé ◽  
J. Martínez Trinidad ◽  
M. Romero-Romo ◽  
R. Pérez Pasten-Borja ◽  
...  

Sign in / Sign up

Export Citation Format

Share Document