Residual Lifetime Determination of Low Temperature Co-Fired Ceramics

2016 ◽  
Vol 713 ◽  
pp. 266-269
Author(s):  
Zdeněk Majer ◽  
Kateřina Štegnerová ◽  
Pavel Hutař ◽  
Martin Pletz ◽  
Raul Bermejo ◽  
...  
Keyword(s):  
Low Temperature ◽  
Residual Stresses ◽  
Crack Propagation ◽  
Crack Growth ◽  
Subcritical Crack Growth ◽  
Particulate Composite ◽  
Ceramic Materials ◽  
Ceramic Composites ◽  
Residual Lifetime ◽  
Density Factor

The effect of subcritical crack growth is nowadays intensively studied mainly in relation to the strength of ceramic materials. The main aim of the contribution is to describe behavior of micro-crack propagating in the Low Temperature Co-fired Ceramics (LTCC) under subcritical crack growth (SCCG) conditions. The micro-crack behavior is significantly influenced by residual stresses developed in the LTCC due to different coefficients of thermal expansion of individual components. Two-dimensional numerical model was developed to simulate micro-crack propagation through the composite. The micro-crack propagation direction was determined using Sih’s criterion based on the strain energy density factor and the micro-crack path was obtained. The residual lifetime of the specific ceramic particulate composite (LTCC) was estimated on the basis of experimental data. The paper contributes to a better understanding of micro-crack propagation in particulate ceramic composites in the field of residual stresses.

Study of Influence of Residual Stresses on Crack Propagation in Particulate Ceramic Composites

2016 ◽  
Vol 258 ◽  
pp. 178-181 ◽  
Author(s):  
Zdeněk Majer ◽  
Luboš Náhlík ◽  
Kateřina Štegnerová ◽  
Pavel Hutař ◽  
Raúl Bermejo
Keyword(s):  
Residual Stresses ◽  
Crack Propagation ◽  
Element Model ◽  
Ceramic Composites ◽  
Particulate Composites ◽  
Micro Cracks ◽  
Dimensional Finite Element ◽  
Density Factor ◽  
Energy Density Factor

The aim of the present work is to analyze the influence of residual stresses in the particulate ceramic composite on the crack propagation. The crack propagation direction was estimated using Sih’s criterion based on the strain energy density factor. A two-dimensional finite element model was developed for determination of crack path. The residual stresses resulting from the mismatch of coefficients of thermal expansion during the fabrication process of the composite were implemented to the computational model. The effect of the particles shape on the crack propagation was investigated. Conclusions of this paper can contribute to a better understanding of the propagation of micro-cracks in particulate composites in the field of residual stresses.

Description of Strengthening Mechanism in Layered Ceramic Composites

2015 ◽  
Vol 665 ◽  
pp. 93-96 ◽  
Author(s):  
Kateřina Štegnerová ◽  
Luboš Náhlík ◽  
Pavel Hutař
Keyword(s):  
Residual Stresses ◽  
Crack Propagation ◽  
Ceramic Composite ◽  
Strengthening Mechanism ◽  
Ceramic Composites ◽  
Zirconia Ceramic ◽  
Linear Elastic ◽  
Density Factor ◽  
Elastic Fracture ◽  
Layered Ceramic

The aim of this paper is to describe specific crack behaviour in the layered alumina-zirconia ceramic composite with strong interfaces and its strengthening mechanism. Different coefficients of thermal expansion of individual constituents of ceramic composite cause high residual stresses inside the layers during the sintering process. Compressive residual stresses can significantly influence the crack propagation through the laminate hereby improve the resistance of the material to the crack propagation. Estimation of crack behaviour in laminate was performed assuming the validity of linear elastic fracture mechanics using the criterion based on the strain energy density factor derived by Sih. This paper describes the strengthening mechanism in layered ceramic composites and prediction of their failure which contributes to better understanding of the fracture behaviour of the layered ceramic composites.

Examination of Fracture Interfaces in Silicon Nitride

1975 ◽  
Vol 33 ◽  
pp. 60-61
Author(s):  
Nancy J. Tighe
Keyword(s):  
Silicon Nitride ◽  
Grain Boundary ◽  
Crack Growth ◽  
Subcritical Crack Growth ◽  
Slow Crack Growth ◽  
Ceramic Materials ◽  
Grain Boundary Sliding ◽  
Boundary Phase ◽  
Turbine Engines ◽  
Boundary Sliding

Silicon nitride is one of the ceramic materials being considered for the components in gas turbine engines which will be exposed to temperatures of 1000 to 1400°C. Test specimens from hot-pressed billets exhibit flexural strengths of approximately 50 MN/m2 at 1000°C. However, the strength degrades rapidly to less than 20 MN/m2 at 1400°C. The strength degradition is attributed to subcritical crack growth phenomena evidenced by a stress rate dependence of the flexural strength and the stress intensity factor. This phenomena is termed slow crack growth and is associated with the onset of plastic deformation at the crack tip. Lange attributed the subcritical crack growth tb a glassy silicate grain boundary phase which decreased in viscosity with increased temperature and permitted a form of grain boundary sliding to occur.

Influence of the Interface and Residual Stresses on the Apparent Fracture Toughness of Layered Ceramic Composites Based on Alumina-Zirconia

2014 ◽  
Vol 606 ◽  
pp. 209-212
Author(s):  
Luboš Náhlík ◽  
Bohuslav Máša ◽  
Pavel Hutař
Keyword(s):  
Residual Stresses ◽  
Crack Propagation ◽  
Ceramic Composites ◽  
Layered Composites ◽  
Material Interfaces ◽  
Linear Elastic ◽  
Apparent Fracture Toughness ◽  
Elastic Fracture ◽  
Layered Ceramic ◽  
Good Agreement

This paper deals with the fracture behaviour of layered ceramic composite with residual stresses. The main goal is to investigate the effect of residual stresses and material interfaces on crack propagation by more complex 3D finite element models. The crack behaviour was described by analytical procedures based on linear elastic fracture mechanics (LEFM) and generalized LEFM. The influence of laminate composition with residual stresses on critical values for crack propagation through the laminate interfaces was also determined. Good agreement has been found to exist between numerical results and experimental data. The results obtained can be used for a design of new layered composites with improved resistance against crack propagation.

Lifetime Assessment of Particulate Ceramic Composite with Residual Stresses

2017 ◽  
Vol 754 ◽  
pp. 107-110
Author(s):  
Luboš Náhlík ◽  
Zdeněk Majer ◽  
Kateřina Štegnerová ◽  
Pavel Hutař
Keyword(s):  
Residual Stresses ◽  
Crack Propagation ◽  
Mechanical Loading ◽  
Ceramic Composite ◽  
Subcritical Crack Growth ◽  
Particulate Composites ◽  
Time To Failure ◽  
Complex Load ◽  
Composite Surface

A micro-crack propagation in particulate ceramic based composite was studied using finite element method (FEM). Subcritical crack growth (SCG) was numerically simulated under complex load conditions (mechanical loading and loading by internal residual stresses). The effect of residual stresses on the crack propagation was studied. Two-dimensional computational model of particulate ceramic composite with material properties corresponding to low temperature co-fired ceramics (LTCC) was developed. The results indicate that the presence of residual stresses significantly reduces values of stress intensity factor in the vicinity of composite surface and the direction of residual stresses around the particles contributes to the micro-crack deflection from the particles. The time to failure of the composite under mechanical loading was determined. Results obtained contribute to a better understanding of the role of residual stresses during micro-crack propagation in ceramic particulate composites.

Mechanical Behavior of Alumina Toughened Zirconia Nanocomposites with Different Alumina Additions

2014 ◽  
Vol 96 ◽  
pp. 61-66 ◽  
Author(s):  
Luis Antonio Díaz ◽  
Sergio Rivera ◽  
Adolfo Fernández ◽  
Anna Okunkova ◽  
Yu.G. Vladimirov ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Crack Propagation ◽  
Mechanical Behavior ◽  
Crack Growth ◽  
Disperse Phase ◽  
Subcritical Crack Growth ◽  
The Other ◽  
Structural Components ◽  
Monolithic Ceramics

ZrO2 and Al2O3 are monolithic ceramics used today in a wide variety of structural components. However, both materials present important drawbacks for some specific applications. In the case of Al2O3, its moderate strength (500 MPa) and toughness (4 MPa.√m) makes it unsuitable for high loading conditions. On the other hand, ZrO2 presents higher strength and toughness values (900 MPa and 6 MPa.√m) than Al2O3 but it is a material limited in its long-term behaviour due to its bad response to hydrothermal ageing and a pronounced tendency for subcritical crack growth. Due to this fact, ceramic nanocomposites made of Al2O3 and ZrO2 (ATZ and ZTA) have been developed in the last years in order to overcome the main drawbacks of the monolithic materials as they can combine the properties of both, strong and tough materials, simultaneously, with null ageing and even higher biocompatibility. In this work, several amounts of Al2O3 disperse phase (15, 35 and 50 vol %) were added to one ZrO2 matrix (CeO2 - 10 mol %) in order to see their effect on the mechanical properties, subcritical crack propagation and long-term reliability.

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