particulate composites
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2022 ◽  
Vol 172 ◽  
pp. 107278
Author(s):  
Santiago Alvarez-Guerrero ◽  
Jose Ordonez-Miranda ◽  
Romeo de Coss ◽  
Juan Jose Alvarado-Gil


Materials ◽  
2021 ◽  
Vol 14 (23) ◽  
pp. 7200
Author(s):  
Kamil Zalegowski

In this paper an analysis of the influence of polymer concrete sample shape and dimensions on ultrasonic wave propagation is carried out. Compositions of tested fly ash polymer concretes were determined using a material optimization approach. The tests were carried out on the samples of three shapes: cubes, beams, and plates. The ultrasonic testing was done by a direct method (transmission method) using a digital ultrasonic flow detector and piezoelectric transducers of 100 kHz central frequency. Propagation of the ultrasonic wave was characterized by pulse velocity. Frequency spectra and time-frequency spectrograms obtained using Fourier transform and Fourier-based synchrosqueezing transform were also presented. The correlation analysis showed that neither the path length nor the lateral dimension to the direction of wave propagation are not statistically significant for the UPV variability. However, a general trend of decrease in the UPV with increasing the path length was noticed. The analysis of the signal in time-frequency domain seemed to be useful in the analysis of particulate composites properties, especially when UPV changes are not clear enough, since it revealed greater differences in relation to changes in sample geometry than frequency spectra analysis.



Author(s):  
Scott Newacheck ◽  
George Youssef

Achieving efficient magnetoelectric coupling of core-shell and particulate multiferroic composites has been a challenging hurdle; however, research has shown unwavering interest to overcome this barrier in pursuit of their implementation into promising potential applications. Herein, a fully coupled computational model of core-shell and particulate composites is developed and verified to investigate the magnetoelectric interactions of the particle and matrix on the microscale. The effects of particle geometry, settling, and agglomeration were exhaustively studied by investigating seven different shapes and a wide range of vertical and lateral particle spacing. Overall, it was found that utilizing particle geometries and positioning that closely resemble a laminate configuration, such as a prolate ellipsoid and horizontal particle alignment, enhances the magnetoelectric coupling of the composite structure. The results coincided with the experimental results concerning settling and agglomeration.



Materials ◽  
2021 ◽  
Vol 14 (22) ◽  
pp. 6913
Author(s):  
Zuzana Murčinková ◽  
Pavel Adamčík ◽  
Jozef Živčák

In this paper, we report the results of an experimental study of a re-design approach using filling polymers and particulate composites with a polymer matrix, thus creating a macroscopic hybrid structure. The re-design is focused on the joint of a textile machine. It is a re-design of already existing machine parts of a joint in order to increase the damping of components, reduce the amplitudes of high-frequency vibrations and acoustic emission for high-speed operation of textile rotors, and to compare individual structural modifications of the rotor housing body and absorber of high-speed textile rotor in a spinning unit with respect to dynamic properties of that measured mechanical system. The experiments included a bump test, determination of logarithmic decrement, measurement of vibration acceleration, a wavelet analysis, and measurement of acoustic emission. When excited by high frequency signal amplitudes up to 5 g, the benefits of polymer filling were manifested by an approximately 50% reduction in amplitude vibrations, a 66% reduction in acoustic emission amplitude, and an 85% reduction of the maximum peak in the acoustic emission FFT spectrum. In the area above 10 g, the stiffness of the component dominated to reduce the magnitude of vibrations.



Author(s):  
Scott Newacheck ◽  
Anil Singh ◽  
George Youssef

Abstract In the current work, quantitative analysis of magnetoelectric particulate composite material system explicated the main mechanisms responsible for the below-optimal performance of this class of materials. We considered compliant particulate composite materials, with constituents relevant to technological and scientific interest, leading to 0-3 Terfenol-D/PVDF-TrFE composite samples. To this objective, thick Terfenol-D/PVDF-TrFE films (10-15 µm) were fabricated and analyzed for chemical, mechanical, and magnetic properties to demonstrate their suitability for energy applications in harsh environmental conditions. The vigorous experimental characterization of the composite exemplified the multifunctional properties, quantifying the interrelationship between the composition and performance. We observed that the addition of magnetic particles to the electroactive copolymer matrix resulted in improvement in the mechanical and electrical properties since the particles acted as pinning sites, hindering the deformation of the chains and enhancing polarization. The effective modulus model was amended to account for the crystallization-induced change in material stiffness. We also measured and computed the magnetic particles motion to explicate the detrimental effect of mobility and migration on the overall magnetoelectric coupling performance of the composite. Thereby, we derived an analytical model based on the magnetic force due to the co-presence of alternating and constant magnetic fields, and the viscous drag force due to the viscoelastic properties of the electroactive copolymer matrix. We demonstrated that the mobility of the particles plays a crucial role in the short and long term performance of magnetoelectric coupling in multiferroic particulate composites, uncovering the underpinnings of the dichotomy in performance between experimentally measured and analytically predicted coupling coefficients., thus, allowing for the proposal of new approaches to realize the scientific potential of magnetoelectric particulate composites in energy applications.



Materials ◽  
2021 ◽  
Vol 14 (21) ◽  
pp. 6676
Author(s):  
Damian Sokołowski ◽  
Marcin Kamiński

The main aim of this study is determination of the basic probabilistic characteristics of the effective stiffness for inelastic particulate composites with spherical reinforcement and an uncertain Gaussian volume fraction of the interphase defects. This is determined using a homogenization method with a cubic single-particle representative volume element (RVE) of such a composite and the finite element method solution. A reinforcing particle is spherical, located centrally in the RVE, surrounded by the thin interphase of constant thickness, and remains in an elastic reversible regime opposite to the matrix, which is hyper-elastic. The interphase defects are represented as semi-spherical voids, which are placed on the outer surface of this particle. The interphase is modeled as hyper-elastic and isotropic, whose effective stiffness is calculated by the spatial averaging of hyper-elastic parameters of the matrix and of the defects. A constitutive relation of the matrix is recovered experimentally by its uniaxial stretch. The 3D homogenization problem solution is based upon a numerical determination of strain energy density in the given RVE under specific uniaxial and biaxial stretches as well as under shear deformations. The analytical relation of the effective composite stiffness to the input uncertain parameter is recovered via the response function method, using a polynomial basis and an optimized order. Probabilistic calculations are completed using three concurrent approaches, namely the iterative stochastic finite element method (SFEM), Monte Carlo simulation and by the semi-analytical method. Previous papers consider the composite fully elastic, which limits the applicability of the resulting effective stiffness tensor computed therein. The current study voids this assumption and defines the composite as fully hyper-elastic, thus extending applicability of this tensor to strains up to 0.25. The most important research finding is that (1) the effective stiffness tensor is sensitive to random interface defects in its hyper-elastic range, (2) its resulting randomness is not close to Gaussian, (3) the semi-analytical method is not perfectly suited to stochastic calculations in this region of strains, as opposed to the linear elastic region, and (4) that the increase in random dispersion of defects volume fraction has a much higher effect on the stochastic characteristics of this stiffness tensor than fluctuation of the strain.



2021 ◽  
Author(s):  
Adrien Rigobello ◽  
Phil Ayres

Abstract Mycelium Based Composites (MBC) exhibit many properties that make them promising alternatives for less sustainable materials. However, there is no unified approach to their testing. We hypothesise that the two-phase particulate composite model and use of ASTM D1037 could provide a basis for systematisation. An experimental series of MBC were produced using four substrate particle sizes and subjected to compression testing. We report on their effect over Young’s modulus and ultimate strength. We extend the study by investigating three anistropic substrate designs through orientated fibre placement as a strategy for modifying compressive behaviour. We find that the two-phase particulate model is appropriate for describing the mechanical behaviour of MBC and that mechanical behaviour can be modified through anisotropic designs using orientated fibres. We also confirm that fibre orientation and particle size are significant parameters in determining ultimate strength.



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