Grain Growth Microstructures as Indicators of Sample Evolution

2004 ◽  
Vol 467-470 ◽  
pp. 1051-1056 ◽  
Author(s):  
M.W. Jessell

Grain growth simulations using the microstructure simulation system Elle have been performed in materials with a pre-existing grain shape preferred orientation. As might be expected, the microstructure is completely modified by the end of the experiment, and grain areas have increased by a factor of seven. The area of material swept by the migrating grain boundaries was monitored, and it was found that at every stage, virtually all of the grains which survived the grain growth process contain one and only one core of unswept material. Remarkably these remnant unswept cores preserve a useable record of the grain size and orientation of the original grains. This work suggests that it may be possible to see past a grain growth episode to estimate the original grain shape and grain size of the polycrystal, and perhaps even reconstruct the grain boundary kinematics. The identification of unswept cores also has the potential to help unravel the evolution of grain boundary chemistry during grain boundary migration.

2019 ◽  
Vol 58 (1) ◽  
pp. 98-106
Author(s):  
Haitao Ni ◽  
Jiang Zhu ◽  
Zhaodong Wang ◽  
Haiyang Lv ◽  
Yongyao Su ◽  
...  

Abstract This review focuses on grain growth behaviors and the underlying mechanisms of bulk electrodeposited nanocrystalline nickel and nickel-iron alloys. Effects of some important factors on grain growth are described. During thermal-induced grain growth process, grain boundary migration plays a key role. For similar thermal conditions, due to grain boundary mobility with solute drag, limited grain growth occurs in nanocrystalline alloys, as compared to pure metals. Nonetheless, in the case of stress-induced grain growth process, there are a variety of mechanisms in samples having various deformation histories. As an example the grain growth of nanocrystalline nickel and Ni-20%Fe alloy with nearly the same grain-size distribution and average grain size is compared in this paper. Thermal analysis indicates nanocrystalline nickel is much more prone to rapid grain growth than nanocrystalline Ni-20%Fe alloy. Nevertheless, grain growth of nanocrystalline Ni-20%Fe is found to be more pronounced than nanocrystalline nickel during rolling deformation.


1992 ◽  
Vol 279 ◽  
Author(s):  
Dale E. Alexander ◽  
L. E. Rehn ◽  
Peter M. Baldo ◽  
Y. Gao

ABSTRACTExperiments were performed demonstrating that ion irradiation enhances diffusion-induced grain boundary migration (DIGM) in polycrystalline Au/Cu bilayers. Here, a model is presented relating film-averaged Cu composition in Au with treatment time, grain size and film thickness. Application of this model to the experimental results indicates that irradiation enhances DIGM by increasing the grain boundary velocity. The effects of DIGM and irradiation-induced grain growth on the temperature dependence of ion mixing in bilayers are discussed.


2012 ◽  
Vol 625 ◽  
pp. 304-307 ◽  
Author(s):  
Hai Zhou Yu ◽  
Wen Jun Liu ◽  
Lian Ying ◽  
Min You

Four series of cermets with the SiC whisker content between 0 and 1.0 wt.% were prepared by vacuum sintering. The transverse rupture strength (TRS), hardness (HRA) and fracture toughness (KIC) were also measured. The SiC whiskeraddition was located at the grain boundaries, which prevented grain boundary migration and restrained the grain growth. However, an increasing SiC whisker content decreased the wettability of the binder on the Mo2FeB2 hard phase. The highest TRS and fracture toughness was found for the cermets with 0.5 wt.% SiC whisker addition, whereas the cermets without SiC whisker addition exhibited the maximum hardness.


2021 ◽  
Author(s):  
Mark Coleman ◽  
Bernhard Grasemann ◽  
David Schneider ◽  
Konstantinos Soukis ◽  
Riccardo Graziani

<p>Microstructures may be used to determine the processes, conditions and kinematics under which deformation occurred. For a given set of these variables, different microstructures are observed in various materials due to the material’s physical properties. Dolomite is a major rock forming mineral, yet the mechanics of dolomite are understudied compared to other ubiquitous minerals such as quartz, feldspar, and calcite. Our new study uses petrographic, structural and electron back scatter diffraction analyses on a series of dolomitic and calcitic mylonites to document differences in deformation styles under similar metamorphic conditions. The Attic-Cycladic Crystalline Complex, Greece, comprises a series of core complexes wherein Miocene low-angle detachment systems offset and juxtapose a footwall of high-pressure metamorphosed rocks against a low-grade hanging wall. This recent tectonic history renders the region an excellent natural laboratory for studying the interplay of the processes that accommodate deformation. The bedrock of Mt. Hymittos, Attica, preserves a pair of ductile-then-brittle normal faults dividing a tripartite tectonostratigraphy. Field observations, mineral assemblages and observable microstructures suggests the tectonic packages decrease in metamorphic grade from upper greenschist facies (~470 °C at 0.8 GPa) in the stratigraphically lowest package to sub-greenschist facies in the stratigraphically highest package. Both low-angle normal faults exhibit cataclastic fault cores that grade into the schists and marbles of their respective hanging walls. The middle and lower tectonostratigraphic packages exhibit dolomitic and calcitic marbles that experienced similar geologic histories of subduction and exhumation. The mineralogically distinct units (calcite vs. dolomite) of the middle package deformed via different mechanisms under the same conditions within the same package and may be contrasted with mineralogically similar units that deformed under higher pressure and temperature conditions in the lower package. In the middle unit, dolomitic rocks are brittlely deformed. Middle unit calcitic marble are mylonitic to ultramylonitic with average grain sizes ranging from 30 to 8 μm. These mylonites evince grain-boundary migration and grain size reduction facilitated by subgrain rotation. Within the lower package, dolomitic and calcitic rocks are both mylonitic to ultramylonitic with grain sizes ranging from 28 to 5 μm and preserve clear crystallographic preferred orientation fabrics. Calcitic mylonites exhibit deformation microstructures similar to those of the middle unit. Distinctively, the dolomitic mylonites of the lower unit reveal ultramylonite bands cross-cutting and overprinting an older coarser mylonitic fabric. Correlated missorientation angles suggest these ultramylonites show evidence for grain size reduction accommodated by microfracturing and subgrain rotation. In other samples the dolomitic ultramylonite is the dominant fabric and is overprinting and causing boudinage of veins and relict coarse mylonite zones. Isolated interstitial calcite grains within dolomite ultramylonites are signatures of localized creep-cavitation processes. Following grain size reduction, grain boundary sliding dominantly accommodated further deformation in the ultramylonitic portions of the samples as indicated by randomly distributed correlated misorientation angles. This study finds that natural deformation of dolomitic rocks may occur by different mechanisms than those identified by published experiments; notably that grain-boundary migration and subgrain rotation may be active in dolomite at much lower temperatures than previously suggested.</p>


1959 ◽  
Vol 37 (4) ◽  
pp. 496-498 ◽  
Author(s):  
E. L. Holmes ◽  
W. C. Winegard

Comparisons are made between theoretical and experimental rates of boundary migration during grain growth in zone-refined metals; these indicate that a single-atom process is involved. A model is proposed for the mechanism of grain-boundary migration based on the assumption of a single-atom process and the fact that the energies of activation for grain growth, both in zone-refined lead and tin, are similar to the energy barrier to be overcome by an atom in transferring from the solid to the liquid state during melting.


2004 ◽  
Vol 467-470 ◽  
pp. 3-10 ◽  
Author(s):  
Mats Hillert

The historical development of the two approaches to the interaction between solute atoms and a migrating interface, based on dissipation of Gibbs energy and on solute drag, are reviewed and compared. In the way the solute drag was formulated long ago for recrystallization and grain growth, it does not apply to phase transformations. With a new solute drag equation, which was recently proposed, it turns out that the two approaches are completely equivalent for phase transformations as well as grain boundary migration.


1994 ◽  
Vol 40 (134) ◽  
pp. 46-55
Author(s):  
C.J. L. Wilson ◽  
Y. Zhang

AbstractAn examination of both experiments and computer models of polycrystalline ice undergoing a simple shear suggests that there is good agreement. The model has correctly reproduced the deformational and microstructural features caused by glide on (0001) in the ice aggregates. This success is particularly prominent for those ice grains with a lattice orientation suitable for hard or easy glide or kinking, and where there is a sub-horizontal с axis and a larger grain-size. A limitation may be that the model cannot explicitly simulate recrystallization and grain-boundary migration, which are two other important processes operating jointly with glide in experimentally deformed ice. However, through the use of the models, it is possible to show how kinematic factors can control the processes of recrystallization. The localization of recrystallization in the polycrystalline ice aggregate is determined by the stress and strain variations between neighbouring grains.


Sign in / Sign up

Export Citation Format

Share Document