scholarly journals Prodigious Azocalix[4] Pyrrole Super-molecule: Effective Reagent for Liquid-liquid Extraction, Preconcentration and Transport of Cu(II) Ions

Author(s):  
Hiren C. Mandalia ◽  
Vinod K. Jain

2016 ◽  
Vol 8 (28) ◽  
pp. 5676-5683 ◽  
Author(s):  
Mir Ali Farajzadeh ◽  
Ali Mohebbi ◽  
Behruz Feriduni

In this study, a simple and rapid sample pretreatment technique named pH-dependent continuous homogenous liquid–liquid extraction followed by gas chromatography-flame ionization detection has been developed for the extraction, preconcentration, and determination of four pesticides including diazinon, oxadiazon, bromopropylate, and fenazaquin in fruit juice and vegetable samples.





1983 ◽  
Vol 15 (6-7) ◽  
pp. 149-159 ◽  
Author(s):  
V C Blok ◽  
G P Slater ◽  
E M Giblin

Several commercially available adsorbents were compared with solvent extraction methods for their utility in recovering trace organics from water. The adsorbents examined included Amberlite XAD-2, XAD-4 and XAD-8, Ambersorb XE340 and XE348 and Tenax-GC. All were found to produce high artifact levels, even after extensive clean-up, making them unsuitable for the analysis of trace organics in water. Quantitatively, Likens-Nickerson or continuous liquid-liquid extraction with méthylene chloride gave better recoveries than the adsorbents. Qualitatively, extractive methods were preferred as they yielded much lower levels of impurities than the adsorbents. These methods of recovering trace organics were evaluated using a standard mixture of compounds added to the water at a level of 55 µg/l. Likens-Nickerson extraction gave comparable recoveries of this mixture at 55 µg/l and 11 µg/l.





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