Neither Sphere nor Cube - Analyzing the Particle Shape Using Small-Angle Scattering and the Superball Model

<div>Accurate characterization of the nanocrystal shape with high statistical relevance is essential for exploiting the strongly shape-dependent properties of cuboidal nanoparticles towards applications. <br></div><div>This work presents the development of a new small-angle scattering form factor based on the superball geometry. The superball quantifies the characteristic rounding of corners and edges of cuboidalnanoparticles with a single parameter. Applied to small-angle scattering data of sufficiently monodisperse nanoparticles, the superball form factor enables differentiation between the effects of extended<br></div>particle size distribution and irregular particle shape. The quantitative application of the superball form factor is validated against microscopy data for a series of monodisperse nanoparticles and implemented into the user-friendly, open source software Sasview.

Neither Sphere nor Cube - Analyzing the Particle Shape Using Small-Angle Scattering and the Superball Model

<div>Accurate characterization of the nanocrystal shape with high statistical relevance is essential for exploiting the strongly shape-dependent properties of cuboidal nanoparticles towards applications. <br></div><div>This work presents the development of a new small-angle scattering form factor based on the superball geometry. The superball quantifies the characteristic rounding of corners and edges of cuboidalnanoparticles with a single parameter. Applied to small-angle scattering data of sufficiently monodisperse nanoparticles, the superball form factor enables differentiation between the effects of extended<br></div>particle size distribution and irregular particle shape. The quantitative application of the superball form factor is validated against microscopy data for a series of monodisperse nanoparticles and implemented into the user-friendly, open source software Sasview.

Direct visualization of the ouzo zone through aggregation-induced dye emission for the synthesis of highly monodispersed polymeric nanoparticles

We report a new enhanced solvent displacement method for the synthesis of highly monodisperse nanoparticles with direct visualization of the ouzo zone.

Monodisperse nanoparticles for catalysis and nanomedicine

Monodisperse nanoparticles are successful model systems for understanding structure–property relationships at the nanoscale and applications like catalysis and nanomedicine.

Экспериментально обучаемый метод фильтрации шумов рассеяния в сигналах оптической когерентной томографии-=SUP=-*-=/SUP=-

A method for wavelet filtration procedure training for optical coherence tomography (OCT) images using the experimental measurements of test objects that were constructed by means of water solutions of monodisperse nanoparticles and several microscopic inclusions has been described in the present paper. The choice of test-object parameters (concentration of water solution, size of nanoparticles, and shape, dimensions, and mutual position of inclusions) has allowed the modeling of various working conditions of OCT and setting different criteria for estimation of filtration efficiency. In the present work, the optimal filter for the considered example of a test object has been selected among the combinations of various basic functions of five wavelet families, soft and hard threshold filtering methods, four decomposition levels, and threshold values in a range of 0.05–3.05. The mutual position of the micro-inclusions has been used as a criterion for evaluating the filtration efficiency. As a result, it has been shown that the determined wavelet filter leads to effective suppression of the scattering noise in OCT images and preserve information about the structure of the object under study.

Analysis of Synthesis Mechanism of Gold Nanoparticles Using Glass Microfluidics

According to LaMer diagram, a clearly separate of nucleation and grows step is required to synthesis of monodisperse nanoparticles. However, a critical mixing time Tc until the growth process is started, is not clear experimentally. In this paper, we prepared gold nanoparticles (GNPs) by liquid-phase reduction using citric acid on microfluidics with different flow rates. From relationship of the diameter of the prepared nanoparticle and the mixing time, Tc for the preparation of monodisperse GNPs was found for the first time.