silicate sample
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2021 ◽  
Vol 247 ◽  
pp. 06046
Author(s):  
K. Hossny ◽  
S. Magdi ◽  
F. Nasr ◽  
Y. Yasser ◽  
A. Magdy

Neutron depth profiling (NDP) is a non-destructive technique used for identifying the concentration of impurity isotopes below the sample surface. NDP is carried out by detection of the emitted charged particles resulting from bombarding the sample with neutrons. NDP specifies the isotopic concentration versus the sample depth for a few micrometers below the surface. The sample is bombarded inside a research reactor using a thermal neutron beam. Charged particles like alpha particles or protons are produced from the neutron induced reactions in the sample. Each neutron isotopic interaction produces a certain Q, indicating a specific kinetic energy for the emitted charged particle. As the charged particle travels through the sample to eject the surface, it loses energy to atoms (electrons) on its path. The charged particle energy loss holds information regarding the number of atoms by which the emitted particle passed, thus indicating its original depth. The purpose of this work is to check the capability of Artificial Neural Networks (ANNs) in predicting the boron concentration profile across a boro-silicate sample of thickness 3.5 μm divided into 10 layers. Each layer included different boron concentration than the other. Also, the boron concentration had the values {0.1, 0.2, 0.3, 0.4, 0.5, 0.6, 0.7, 0.8, 0.9, 1}. Training, validation, and test data were generated synthetically using MCNP6 in which the boron concentrations varied in the layer number from one sample to another. MCNP6 model consisted of a silicon barrier detector, boro-silicate sample, chamber body and an idealized thermal neutron source. The detector, sample, and the source were located in a voided chamber. The samples were irradiated with a 0.025 eV monoenergetic thermal neutron beam from a monodirectional disk source. To cover the whole area of the samples, the thermal neutron beam had a radius of 3 cm. The silicon detector active volume was modelled as a 100 μm thick and 3 cm radius facing the sample directly. The sample, beam, and the detector were placed on the same axis. Ten ANN regression models were developed, one for each layer boron concentration prediction where the input for each model was the alpha spectrum read by the detector, while the output was the boron concentration for each layer. Results showed regression values higher than 0.94 for all of the developed models. ANNs proved its capability of predicting the boron profile form the alpha spectrum read by the detector regarding neutron depth profiling in a boro-silicate samples.


2019 ◽  
Vol 9 (1) ◽  
pp. 102-109 ◽  
Author(s):  
Mostafa Mabrouk ◽  
Sayed Hamed Kenawy ◽  
Gehan El Tabie El-Bassyouni ◽  
Ahmed Abd El-Fattah Ibrahim Soliman ◽  
Esmat Mahmoud Aly Hamzawy

Purpose: Different compositions of copper oxide (CuO)-doped calcium silicate clusters wereused to treat the cancer cells.Methods: The influence of CuO content on the morphology, drug delivering ability,physicochemical properties and cytotoxicity was investigated.Results: The microcrystalline structure revealed the decrement of the size from (20-36 nm) to(5-7 nm) depending on the copper content percentages. Drug delivering ability of doxycyclinehyclate (Dox) was down regulated from 58% to 28%in the presence of the CuO. The inclusionof CuO and Dox didn’t show any remarkable changes on the physicochemical properties of theCuO-doped calcium silicate nanoparticles.Conclusion: The CuO-doped calcium silicate sample (5 weight %) exhibited great cytotoxicityagainst the tested cell lines compared to the CuO-free sample. CuO-doped materials displayedsignificant anticancer effect; this sheds light on its implication in the treatment of cancer.


2014 ◽  
Vol 937 ◽  
pp. 652-658
Author(s):  
Xin Hua Zhu ◽  
Zhao Zhang ◽  
Jun Shen

The silica, one of the by-products of fluorine industry, contains soluble fluoride which is harmful to the environment. Therefore, a study on fixing soluble fluoride was conducted by hydrothermal method with the silica as raw material and adding hydrated lime (HL), and the nanowires-reticulated calcium silicate with high specific surface area up to 143.8m2/g was prepared at the same time. The prepared calcium silicate was used as adsorbent in the experiments of phosphorus (P) adsorption from aqueous solution, the adsorption capacity, adsorption rate and P removability were characterized. The results show that the preparation conditions affect distinctly the adsorption performances of calcium silicate, especially, the dosage Ca/Si molar ratio. For the optimized calcium silicate sample, the total P adsorption capacity is 125.7mg/g and the exchange rate of Ca2+reaches 95.8%, the P residual concentration is only 0.3mg/L, the saturated adsorption time is 3900 min, when the simulation solution with P concentration of 100 mg/L is treated. The P residual concentration is only 0.1mg/L for the simulation solution of 56.12mg/L.


2002 ◽  
Vol 32 (1) ◽  
pp. 65-70 ◽  
Author(s):  
Fabienne Méducin ◽  
Christine Noı̈k ◽  
Alain Rivereau ◽  
Hélène Zanni

1978 ◽  
Vol 32 (3) ◽  
pp. 272-275 ◽  
Author(s):  
A. A. Fakhry ◽  
M. A. Eid ◽  
M. S. Hashem

In the present investigation opposing magnetic fields are applied to the free burning carbon arc with a silicate sample (granodiorite) in its anode crater. The magnetic field promoted the selective volatilization of the elements present in the sample. As a result, a depression in the spectral line intensities of Mn, Ti, Th, and Fe as well as the background was observed. At the same time the intensity of the spectral lines of Ag, Ge, Pb, In, and Cu is enhanced. The latter elements are of great significance since they are used as pathfinders for gold.


1970 ◽  
Vol 24 (2) ◽  
pp. 241-245 ◽  
Author(s):  
P. W. J. M. Boumans ◽  
F. J. M. J. Maessen

The transfer of atomized material from the electrode cavity to the discharge region of a dc arc is quantitatively defined in terms of the efficiency with which elements enter the excitation region. Equations inherent in the determination of efficiencies from spectral-line intensities are given. Relative efficiencies were experimentally determined for a synthetic silicate sample containing some 20 test elements as trace or minor constituents. The elements were selected according to volatility and carbide forming properties. The influences of the following variables on the efficiency were investigated: (a) type of element, (b) preliminary fusion of test sample with lithium metaborate, (c) dilution of test sample with lithium carbonate or lithium fluoride, (d) two different types of Stallwood-jet devices for arc stabilization and control of atmosphere, (e) the composition of the stabilizing gas, viz., the oxygen content of an oxygen—argon gas mixture, and (f) the flow rate of the stabilizing gas.


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