A New Facility for the Planetary Science Community at DLR: the Planetary Sample Analysis Laboratory (SAL).

<p><strong>Introduction:</strong> Laboratory measurements of extra-terrestrial materials like meteorites and ultimately materials from sample return missions can significantly enhance the scientific return of the global remote sensing data.</p> <p>This motivated the addition of a dedicated Sample Analysis Laboratory (SAL) to complement the work of well established facilities like the Planetary Spectroscopy Laboratory (PSL) and the Astrobiology Laboratories within the Department of Planetary Laboratories at DLR, Berlin. SAL is being developed in preparation to receive samples from sample return missions such as JAXA Hayabusa 2 and MMX missions, the Chinese Chang-E 5 and 6 missions as well as the NASA Osiris-REX mission. SAL will be focusing on spectroscopic, geochemical, mineralogical analyses at microscopic level with the ultimate aim to derive information on the formation and evolution of planetary bodies and surfaces, search for traces of organic materials or even traces of extinct or extant life and presence of water.</p> <p><strong>Sample Analysis Laboratory:</strong> The near-term goalis to set up the facilities  on time to receive samples from the Hayabusa 2 mission. The operations have already started in 2018 with the acquisition of a vis-IR-microscope and it will continue with the acquisition of: Field Emission Gun - scanning electron microscope (FEG-SEM), Field Emission Gun – electron microprobe analyser (FEG-EMPA), X-ray diffraction (XRD) system with interchangeable optics for μXRD analysis anda polarised light microscope for high resolution imaging and mapping</p> <p>The facilities will be hosted in a clean room (ISO 5) equipped with glove boxes and micromanipulators to handle and prepare samples. All samples will be stored under dry nitrogen and can be transported between the instruments  with dedicated shuttles in order to avoid them to enter in contact with the external environment. Based on current planning the first parts of SAL will be operational and ready for certification by end of 2022.</p> <p><strong>Current facilities:</strong> To characterize and analyse the returned samples, SAL facilities will work jointly with the existing spectroscopic capabilities of PLL.</p> <p>PLL has the only spectroscopic infrastructure in the world with the capability to measure emissivity of powder materials, in air or in vacuum, from low to very high temperatures [1-3], over an extended spectral range from 0.2 to 200 µm. Emissivity measurements are complemented by reflectance and transmittance measurements produced simultaneously with the same set-up. Recently a vis-IR-microscope was added to extend spectral analysis to the sub-micron scale. In addition, the department is operating a Raman micro-spectrometer with a spot size on the sample in focus of <1.5 μm. The spectrometer is equipped with a cryostat serving as a planetary simulation chamber which permits simulation of environmental conditions on icy moons and planetary surfaces.</p> <p>PLL leads MERTIS on BepiColombo as well as the BioSign exposure experiment on the ISS. The labs have performed laboratory measurements for nearly every planetary remote sensing mission. PLL has team members on instruments on the MarsExpress, VenusExpress, MESSENGER and JAXA Hayabusa 2 and MMX missions. Most recently we joined the Hayabusa 2 Initial Sample Analysis Team.The samples analyzed at PLL range from rocks, minerals, meteorites and Apollo and Luna lunar soil samples to biological samples (e.g. pigments, cell wall molecules, lichens, bacteria, archaea and other) and samples returned from the ISS (BIOMEX) [4, 5, 6] and the asteroid Itokawa (Hayabusa sample).</p> <p>PLL is part of the “Distribute Planetary Simulation Facility” in European Union funded EuroPlanet Research Infrastructure (http://www.europlanet-2020-ri.eu/). Through this program (and its predecessor) over the last 9 years more than 80 external scientists have obtained time to use the PLL facilities. PLL has setup all necessary protocols to support visiting scientist, help with sample preparation, and archive the obtained data.</p> <p><strong>Outlook:</strong> DLR has started establishing a Sample Analysis Laboratory. Following the approach of a distributed European sample analysis and curation facility as discussed in the preliminary recommendations of EuroCares (http://www.euro-cares.eu/) the facility at DLR could be expanded to a curation facility. The timeline for this extension will be based on the planning of sample return missions. The details will depend on the nature of the returned samples. Moreover, SAL will be running in close cooperation with the Museum für Naturkunde in Berlin and it will be operated as a community facility (e.g. Europlanet), supporting the larger German and European sample analysis community.</p> <p> </p> <p><strong>References:</strong> [1] Ferrari et al., Am. Min., (2014), 99(4): p. 786-792. [2] Maturilli and Helbert, JARS (2014), 8(1): p. 084985. [3] A. Maturilli, et al., (2019) Infrared Remote Sensing and Instrumentation XXVII, 10.1117/12.2529266. [4] de Vera et al. (2012), PSS, 74(1): p. 103-110. [5] Serrano et al. (2014), PSS, 98: 191–197. [6] Serrano et al. (2015), FEMS Microbiology Ecology, 91(12): 2015, fiv126.</p>

Organic chemistry in space and the search for life in our Solar System

<p>One of the most fascinating questions in planetary science is how life originated on Earth and whether life exists beyond Earth. Life on Earth originated approximately 3.5 billion years ago and has adapted to nearly every explored environment including the deep ocean, dry deserts and ice continents. What were the chemical raw materials available for life to develop? Many carbonaceous compounds are identified by astronomical observations in our Solar System and beyond. Small Solar System bodies hold clues to both processes that formed our Solar System and the processes that probably contributed carbonaceous molecules and volatiles during the heavy bombardment phase to the young planets in our Solar System. The latter process may have contributed to life’s origin on Earth. Space missions that investigate the composition of comets and asteroids and in particular their organic content provide major opportunities to determine the prebiotic reservoirs that were available to early Earth and Mars. Recently, the Comet rendezvous mission Rosetta has monitored the evolution of comet 67P/Churyumov-Gerasimenko during its approach to the Sun. Rosetta observed numerous volatiles and complex organic compounds on the cometary surface and in the coma. JAXA’s Hayabusa-2 mission has returned samples from near-Earth asteroid Ryugu in December 2020 and we may have some interesting scientific results soon. Hayabusa-2 also carried the German-French landing module MASCOT (mobile asteroid surface scout) that provided new insights into the structure and composition of the asteroid Ryugu during its 17-hour scientific exploration.</p><p>Presently, a fleet of robotic space missions target planets and moons in order to assess their habitability and to seek biosignatures of simple extraterrestrial life beyond Earth. Prime future targets in the outer Solar System include moons that may harbor internal oceans such as Europa, Enceladus, and Titan. Life may have emerged during habitable periods on Mars and evidence of life may still be preserved in the subsurface, evaporite deposits, caves, or polar regions. On Mars, a combination of solar ultraviolet radiation and oxidation processes are destructive to organic material and life on and close to the surface. However, the progress and the revolutionary quality and quantity of data on “extreme life” on Earth has transformed our view of habitability. In 2021, we will hopefully have three robotic missions arriving at Mars from China, the United Arab Emirates and NASA (Tianwen-1, Hope, and Mars2020 respectively). In 2022, ESA’s ExoMars program will launch the Rosalind Franklin Rover and landing platform, and drill two meters deep into the Martian subsurface for the first time. Mars is still the central object of interest for habitability studies and life detection beyond Earth, paving the way for returned samples and human exploration.</p><p>Measurements from laboratory, field, and space simulations are vital in the preparation phase for future planetary exploration missions. This Cassini lecture will review the evolution and distribution of organic matter in space, including results from space missions, field and laboratory research, and discuss the science and technology preparation necessary for robotic and human exploration efforts investigating habitability and biosignatures in our Solar System.</p>

The Planetary Terrestrial Analogues Library (PTAL)

<p>The Planetary Terrestrial Analogues Library project aims to build and exploit a spectral data base for the characterization of the mineralogical and geological evolution of terrestrial planets and small Solar System bodies. Basis for the library is our collection of natural field-collected and artificial planetary (often Martian) analogue materials as well as materials, which have been altered in laboratory experiments. All samples were characterized by XRD, thin sections as base and as input for the spectral library with standard commercial and dedicated spacecraft instrumentation (NIR, RAMAN, LIBS) under laboratory conditions. The database will allow users to jointly interpret laboratory results and newly gathered in-situ or remote sensing data using instruments (LIBS, NIR, Raman) on board of current and future space missions (e.g., Hayabusa-2, Curiosity, ExoMars, Mars2020). The main aim of the database is the use of spectra stored for purposes related to comparison, identification, quantification and spectral calculation when spectroscopic instruments such as NIR, Raman and LIBS operate in planetary missions and/or analyzing materials in the field or in the laboratory. This database features spectral tools allowing for the spectral data treatment implementation plans are the integration of the database management and algorithms in an end-user platform with graphical interfaces for the use of the data and analyzing tools. The public release of the Planetary Terrestrial Analogues Library will be at the end of year 2020. We will have a demonstration and tutorial during the EGU-GA 2020.</p><p><strong>Acknowledgements: </strong>This project is financed through the European Research Council in the H2020-COMPET-2015 programme (grant 687302).</p>

Organic chemistry in space and the search for life in our Solar System

<p>One of the most fascinating questions in planetary science is how life originated on Earth and whether life exists beyond Earth. Carbonaceous compounds in the gas and solid state, refractory and icy are identified by astronomical observations in our Solar System, and distant galaxies. Among them are a large number of molecules that are essential in prebiotic chemistry and used in contemporary biochemistry on Earth. Life on Earth originated approximately 3.5 billion years ago and has adapted to nearly every explored environment. What was chemical raw materials available for life to develop? Small Solar System bodies hold clues to processes that formed our Solar System and probably contributed carbonaceous molecules and volatiles during the heavy bombardment phase to the young planets. This process may have contributed to life’s origin on Earth. Space missions that investigate the composition of comets and asteroids and in particular their organic content provide major opportunities to determine the prebiotic reservoirs available to the early Earth and Mars. Recently, the Comet rendezvous mission Rosetta has monitored the evolution of comet 67P/Churyumov-Gerasimenko during its approach to the Sun and observed numerous volatiles and complex organic compound on the cometary surface and in the coma. Several asteroid sample return missions are currently operational such as JAXA’s Hayabusa-2 which was launched in 2014 and will return samples to Earth in 2020. Hayabusa-2 also carried the German-French landing module MASCOT (mobile asteroid surface scout) that provided during the 17 hours of intensive scientific exploration new insights into the structure and composition of the asteroid Ryugu.</p><p>A fleet of robotic space missions currently targets planets and moons in order to assess their habitability and to seek biosignatures of simple extraterrestrial life beyond Earth. Prime targets in the outer Solar System include moons that may harbor internal oceans such as Europa, Enceladus, and Titan. Life may have emerged during habitable periods on Mars and remains may still be preserved in the subsurface, evaporite deposits, caves or polar regions. On Mars, a combination of solar ultraviolet radiation and oxidation processes are destructive to organic material and life on and close to the surface. However, the progress and the revolutionary quality and quantity of data on “extreme life” on Earth have transformed our view of habitability. In 2020, ESA’s ExoMars program will launch the Rosalind Franklin Rover and landing platform, and drill for the first time 2m deep into the Martian subsurface. Mars is still the central object of interest for habitability studies and life detection beyond Earth, paving the way for returned samples and human exploration.</p><p>Knowledge on the evolution of organic material in space environment such as their photochemistry and preservation potential are crucial to advance life detection strategies and instrument development. This Cassini lecture will review the evolution of organic matter in space including recent observations, space missions and laboratory research and discuss the science and technology preparation necessary for robotic and human exploration efforts investigating habitability and biosignatures in our Solar System.</p>