Graphite Ion Source Geometry and Ne-Gas Pressure Dependent Growth and Morphology of Carbon Nanoclusters: AFM Analysis

The understanding of the growth and morphological evolution of nanoclusters with process parameters such as ion source geometry, voltage, current, time, and gas pressure are highly important to achieve their desired sizes, morphology, and concentration. Carbon nanoclusters (0-dimensional) were synthesized using the DC glow discharge technique at different process parameters (such as Ne-gas pressures, current, voltage, etc.) using custom fabricated graphite ion sources of cylindrical and U-shaped geometries. The morphology and density of carbon nanoclusters were studied with an atomic force microscope (AFM) to understand their evolution at different process parameters. The study suggests that the U-shaped hollow cathode ion source produces tiny carbon nanoclusters at greater concentration as compared to the cylindrical cathode. Similarly, the density of tiny nanoclusters enhances greatly with the increasing pressures (e.g., 75 mbar). In addition, the AFM morphology of the nanoclusters shows that they are more agglomerated at relatively lower pressure (e.g., 25 mbar). This may be due to the higher fragmentation of carbon soot with the increasing pressure because of more collisions among gas molecules and carbonaceous species. At controlled and optimized Ne-gas pressures and source geometry, carbon nanoclusters of the desired sizes can be fabricated, which may become promising candidates for nanoscale electronics, optoelectronic, and spintronic devices.

Металлопористые катоды, модифицированные наноуглеродом, с высокой долговечностью для применения в приборах СВЧ

The results of calculations of the physical and energy parameters of nanocarbon structures with components of the active substance of the dispenser cathode, which are in good agreement with experience, are presented. It was experimentally determined that the active substance modified by the sulfoadduct of carbon nanoclusters has an evaporation rate of 1.5 times lower than the typical one. Tests of cathodes modified by nanocarbon as part of space-based TWTs showed a durability of 1740800 hours with a current density of 0.645 A / cm2.

An evaporation induced self-assembly approach to prepare polymorphic carbon dot fluorescent nanoprobes for protein labelling

Herein, we report a novel route to prepare polymorphic carbon dot fluorescent probes via the evaporation-induced self-assembly of glutaraldehyde and carbon dots, which first usually form carbon nanoclusters which then could self-assemble to form carbon nanocrystals, nanospheres or nanofibers in different ionic strength solutions at room temperature.