Simplified synthesis of spherical silica microparticles from rice husk

Author(s):  
Il-Seop Jang ◽  
Ji Yeon Park ◽  
Hayoung Park ◽  
Yang Mo Gu ◽  
Jin Hyung Lee ◽  
...  
2020 ◽  
Vol 54 (29) ◽  
pp. 4611-4620 ◽  
Author(s):  
Akm Samsur Rahman ◽  
Chirag Shah ◽  
Nikhil Gupta

The current research is focused on developing a geopolymer binder using rice husk ash–derived silica nanoparticles. Four types of rice husks were collected directly from various rice fields of Bangladesh in order to evaluate the pozzolanic activity and compatibility of the derived rice husk ashes with precursors of sodium-based geopolymers. Silicon carbide whiskers were introduced into sodium-based geopolymers in order to evaluate the response of silicon carbide whiskers to the interfacial bonding and strength of sodium-based geopolymers along with rice husk ashes. Compression, flexural and short beam shear tests were performed to investigate the synergistic effect of rice husk ashes–derived silica and commercially available silicon carbide whiskers. Results show that rice husk ashes–derived spherical silica nanoparticles reduced nano-porosity of the geopolymers by ∼20% and doubled the compressive strength. The simultaneous additions of rice husk ashes and silicon carbide whiskers resulted in flexural strength improvement by ∼27% and ∼97%, respectively. The increase in compressive strength due to the inclusion of silica nanoparticles is related to the reduction in porosity. The increase in flexural strength due to simultaneous inclusion of silica and silicon carbide whiskers suggest that silica particles are compatible with the metakaolin-based geopolymers, which is effective in consolidation. Finally, microscopy suggest that silicon carbide whiskers are effective in increasing bridged network and crack resistance.


2021 ◽  
Author(s):  
Seongseop Kim ◽  
Ji Yeon Park ◽  
Yang Mo Gu ◽  
Il-Seop Jang ◽  
Hayoung Park ◽  
...  

The valorization of inorganic silica components from rice husk has been considered an important research topic over the last few decades. However, owing to various problems, such as the difficulty...


2018 ◽  
Vol 44 (7) ◽  
pp. 8720-8724 ◽  
Author(s):  
S. Sankar ◽  
Narinder Kaur ◽  
Sejoon Lee ◽  
Deuk Young Kim

2016 ◽  
Vol 1133 ◽  
pp. 467-470
Author(s):  
Raja Nor Othman ◽  
Arthur N. Wilkinson

Carbon nanotube has been successfully grafted on the surface of spherical silica gel via floating-catalyst chemical vapour deposition method. The growth conditions were set to be 3 hours growth time and 5 wt. % of ferrocene catalyst (dissolved in toluene) injected into the furnace at a rate of 0.04 ml/min. It was found that the reaction temperature of 760°C yields the best quality hybrid particles. Decreasing and increasing the reaction temperature resulted in the formation of product that consists of thicker tubes, higher defects as analysed by Raman, as well as least carbon formation.


2020 ◽  
Vol 13 (11) ◽  
pp. 8119-8132 ◽  
Author(s):  
Revathi Rajan ◽  
Yusmazura Zakaria ◽  
Shaharum Shamsuddin ◽  
Nik Fakhuruddin Nik Hassan

In many rice producing countries of the world, including in Vietnam, various research aimed at using rice husk ash (RHA) as a finely dispersed active mineral additive in cements, concrete and mortars are being conducted. The effect of the duration of the mechanoactivation of the RHA, produced under laboratory conditions in Vietnam, on its pozzolanic activity were investigated in this study. The composition of ash was investigated by laser granulometry and the values of indicators characterizing the dispersion of its particles before and after mechanical activation were established. The content of soluble amorphous silicon oxide in rice husk ash samples was determined by photocolorimetric analysis. The pizzolanic activity of the RHA, fly ash and the silica fume was also compared according to the method of absorption of the solution of the active mineral additive. It is established that the duration of the mechanical activation of rice husk ash by grinding in a vibratory mill is optimal for increasing its pozzolanic activity, since it simultaneously results in the production of the most dispersed ash particles with the highest specific surface area and maximum solubility of the amorphous silica contained in it. Longer grinding does not lead to further reduction in the size of ash particles, which can be explained by their aggregation, and also reduces the solubility of amorphous silica in an aqueous alkaline medium.


2014 ◽  
Vol 27 (2) ◽  
pp. 148-160
Author(s):  
Hassan K. Hassan ◽  
Najla J. Al-Amiri ◽  
Mohammed M. Yassen

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