In situ measurement of crystal surface dynamics in pure and contaminated solutions by Confocal Microscopy and Atomic Force Microscopy

2013 ◽  
Vol 48 (10) ◽  
pp. 919-941 ◽  
Author(s):  
Alexander E. S. Van Driessche ◽  
Mike Sleutel
2016 ◽  
Vol 6 (12) ◽  
pp. 1600099 ◽  
Author(s):  
Insun Yoon ◽  
Daniel P. Abraham ◽  
Brett L. Lucht ◽  
Allan F. Bower ◽  
Pradeep R. Guduru

1995 ◽  
Vol 66 (4) ◽  
pp. 2848-2852 ◽  
Author(s):  
S. Hudlet ◽  
M. Saint Jean ◽  
D. Royer ◽  
J. Berger ◽  
C. Guthmann

2020 ◽  
Vol 37 (4) ◽  
pp. 417-422
Author(s):  
Eri Akita ◽  
Yaxiaer Yalikun ◽  
Kazunori Okano ◽  
Yuki Yamasaki ◽  
Misato Ohtani ◽  
...  

2002 ◽  
Vol 16 (01n02) ◽  
pp. 25-33 ◽  
Author(s):  
MANIJEH M. REYHANI ◽  
ALLAN OLIVEIRA ◽  
GORDON M. PARKINSON ◽  
FRANCA JONES ◽  
ANDREW L. ROHL ◽  
...  

Real time in situ monitoring of calcite growth and inhibition on the cleavage plane [Formula: see text] is investigated using atomic force microscopy (AFM). Calcite growth and inhibition were studied using a Molecular Imaging microscope in contact mode, equipped with an in situ fluid cell. As has been reported previously, it is observed that calcite growth from aqueous solution is by motion of mono-molecular steps, and dissolution by a combination of step motion and etch pit expansion. The measured step heights were between 2.7 to 3 Å. Our aim is to study the effects of a range of phosphonate-based crystal growth inhibitors of related structure, in order to provide insight into the mechanism of inhibition as a function of the additive structure. Results of this study demonstrate the effect of inhibitors on the growth steps and terraces on the [Formula: see text] surface of calcite in real time. The organic additives bind to the crystal surface, with selective binding to the step edges particularly evident in some cases. In other cases, it appears that the additive acts by binding to the terraces on the crystal surface, resulting in inhibition by coating the surface. Efforts to correlate the observations made by atomic force microscopy with bulk crystallization experiments have been made.


1999 ◽  
Vol 353 (1-2) ◽  
pp. 194-200 ◽  
Author(s):  
C. Coupeau ◽  
J.F. Naud ◽  
F. Cleymand ◽  
P. Goudeau ◽  
J. Grilhé

2001 ◽  
Vol 167 (1) ◽  
pp. 139-151 ◽  
Author(s):  
Connie J. Rossini ◽  
Justinn F. Arceo ◽  
Evan R. McCarney ◽  
Brian H. Augustine ◽  
Douglas E. Dennis ◽  
...  

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