Large-scale Enrichment of Sulfur-containing Acid in Acetonitrile Using Triazine Analog as the Derivatizing Reagent for Desorption from Humic-fraction-modified Silica Gel
Abstract
A large-scale method, using custom-made apparatus, is described for making potassium hydroxide-modified silica gel. Batches as large as 2.3 kg can be made in 16 man-hours. A smaller-scale version of the method, requiring no specialized apparatus, is also described. The method can be used to integrate this adsorbent into many sampleenrichment procedures.