Large-Scale Preparation of Potassium Hydroxide-Modified Silica Gel Adsorbent

1989 ◽  
Vol 72 (2) ◽  
pp. 371-373
Author(s):  
Jon A Lebo ◽  
Jim L Zajicek ◽  
Thomas W May ◽  
Lawrence M Smith

Abstract A large-scale method, using custom-made apparatus, is described for making potassium hydroxide-modified silica gel. Batches as large as 2.3 kg can be made in 16 man-hours. A smaller-scale version of the method, requiring no specialized apparatus, is also described. The method can be used to integrate this adsorbent into many sampleenrichment procedures.

RSC Advances ◽  
2017 ◽  
Vol 7 (35) ◽  
pp. 21721-21732 ◽  
Author(s):  
Bin Liao ◽  
Zhenguo An ◽  
Jingjie Zhang

Micron-sized double shell composite hollow particles with excellent electromagnetic behavior are prepared using a highly efficient and large scale method.


1969 ◽  
Vol 22 (03) ◽  
pp. 577-583 ◽  
Author(s):  
M.M.P Paulssen ◽  
A.C.M.G.B Wouterlood ◽  
H.L.M.A Scheffers

SummaryFactor VIII can be isolated from plasma proteins, including fibrinogen by chromatography on agarose. The best results were obtained with Sepharose 6B. Large scale preparation is also possible when cryoprecipitate is separated by chromatography. In most fractions containing factor VIII a turbidity is observed which may be due to the presence of chylomicrons.The purified factor VIII was active in vivo as well as in vitro.


2000 ◽  
Vol 116 (1) ◽  
pp. 56-61
Author(s):  
Tatsuo YAMAGUCHI ◽  
Toshiaki NAKAI ◽  
Kunihiko TAKEDA

1992 ◽  
Vol 70 (6) ◽  
pp. 448-454 ◽  
Author(s):  
Ewa Świeżewska ◽  
T. Chojnacki ◽  
W. J. Jankowski ◽  
K. Singh ◽  
J. Olsson

The long chain polyprenols composed of 30 and more isoprene units from leaves of plants belonging to the genera Potentilla and Rosa have been described. They occur in the form of fatty acid esters. The composition of polyprenol mixture was species dependent and its content reached ca. 0.5% wet weight. Large scale preparation of individual polyprenols from a natural polyprenol mixture was performed using time-extended liquid chromatography on the hydrophobic gel Lipidex-5000.Key words: long chain polyprenols, Rosaceae.


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