Thermal debinding of powder injection molded parts: Observations and mechanisms

In the present work the influence of two different thermal debinding atmosphere, vacuum and air, on the properties of 5wt% Y2O3-doped aluminum nitride (AlN) ceramics was investigated. The AlN powder as a raw material was synthesized by self-propagating high-temperature synthesis (SHS) and compact was fabricated by employing powder injection molding technique. The polymer-wax binder consists of 60wt% paraffin wax (PW), 35wt% polypropylene (PP) and 5wt% stearic acid (SA). The binder was removed through debinding process in two steps, solvent debinding followed by thermal debinding. After the removal of binder, specimens were sintered at 1850˚С in nitrogen atmosphere at atmospheric pressure. The result reveals that debinding atmosphere has significant effect on the thermal conductivity and densification of AlN ceramics. The microstructure and secondary phase identification was determined by scanning electron microscopy and X-ray diffraction. The thermal conductivity and density of injection molded AlN ceramics are 177.3W·m-1·K-1 and 3.31g·cm-3 in the air and 200.8W·m-1·K-1 and 3.28g·cm-3 in the vacuum.

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Opportunities for producing dimensionally enhanced powder-injection-molded parts

Metal Powder Report ◽

10.1016/j.mprp.2017.06.071 ◽

2018 ◽

Vol 73 (2) ◽

pp. 68-71 ◽

Cited By ~ 1

Author(s):

Volker Piotter ◽

Alexander Klein ◽

Tobias Mueller ◽

Klaus Plewa

Keyword(s):

Powder Injection ◽

Molded Parts ◽

Injection Molded

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A Study on the Birefringence Measurement in Injection Molded Parts Using Two Different Laser Sources and R-G-B Separation of White Light

Key Engineering Materials ◽

10.4028/www.scientific.net/kem.326-328.187 ◽

2006 ◽

Vol 326-328 ◽

pp. 187-190

Author(s):

Jong Sun Kim ◽

Chul Jin Hwang ◽

Kyung Hwan Yoon

Keyword(s):

White Light ◽

Low Cost ◽

Main Idea ◽

Injection Molding Process ◽

Molding Process ◽

Laser Method ◽

High Productivity ◽

Molded Parts ◽

Injection Molded ◽

Plastic Parts

Recently, injection molded plastic optical products are widely used in many fields, because injection molding process has advantages of low cost and high productivity. However, there remains residual birefringence and residual stresses originated from flow history and differential cooling. The present study focused on developing a technique to measure the birefringence in transparent injection-molded optical plastic parts using two methods as follows: (i) the two colored laser method, (ii) the R-G-B separation method of white light. The main idea of both methods came from the fact that more information can be obtained from the distribution of retardation caused by different wavelengths. The comparison between two methods is demonstrated for the same sample of which retardation is up to 850 nm.

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Injection Molding and Near-Complete Densification of Monolithic and Al2O3 Fiber-Reinforced Ti2AlC MAX Phase Composites

Materials ◽

10.3390/ma14133632 ◽

2021 ◽

Vol 14 (13) ◽

pp. 3632

Author(s):

Sylvain Badie ◽

Rimy Gabriel ◽

Doris Sebold ◽

Robert Vaßen ◽

Olivier Guillon ◽

...

Keyword(s):

Injection Molding ◽

Graphite Powder ◽

Max Phase ◽

Powder Injection ◽

Fiber Reinforced ◽

Ceramic Fibers ◽

Plasma Sintering ◽

Molded Parts ◽

Al2o3 Fiber ◽

Induced Velocity

Near-net shape components composed of monolithic Ti2AlC and composites thereof, containing up to 20 vol.% Al2O3 fibers, were fabricated by powder injection molding. Fibers were homogeneously dispersed and preferentially oriented, due to flow constriction and shear-induced velocity gradients. After a two-stage debinding procedure, the injection-molded parts were sintered by pressureless sintering at 1250 °C and 1400 °C under argon, leading to relative densities of up to 70% and 92%, respectively. In order to achieve near-complete densification, field assisted sintering technology/spark plasma sintering in a graphite powder bed was used, yielding final relative densities of up to 98.6% and 97.2% for monolithic and composite parts, respectively. While the monolithic parts shrank isotropically, composite assemblies underwent anisotropic densification due to constrained sintering, on account of the ceramic fibers and their specific orientation. No significant increase, either in hardness or in toughness, upon the incorporation of Al2O3 fibers was observed. The 20 vol.% Al2O3 fiber-reinforced specimen accommodated deformation by producing neat and well-defined pyramidal indents at every load up to a 30 kgf (~294 N).

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