scholarly journals Microstructure and Residual Stress Evolution of Laser Powder Bed Fused Inconel 718 under Heat Treatments

2020 ◽  
Author(s):  
Giulio Marchese ◽  
Eleonora Atzeni ◽  
Alessandro Salmi ◽  
Sara Biamino
Keyword(s):  
Residual Stresses ◽  
Inconel 718 ◽  
Heat Treatments ◽  
Powder Bed Fusion ◽  
Stress Evolution ◽  
Laser Powder Bed Fusion ◽  
Powder Bed ◽  
Melt Pool ◽  
Sintering Mechanisms ◽  
Dendritic Structures

AbstractThe current work aimed to study the influence of various heat treatments on the microstructure, hardness, and residual stresses of Inconel 718 processed by laser powder bed fusion process. The reduction in residual stresses is crucial to avoid the deformation of the component during its removal from the building platform. Among the different heat treatments, 800 °C kept almost unaltered the original microstructure, reducing the residual stresses. Heat treatments at 900, 980, and 1065 °C gradually triggered the melt pool and dendritic structures dissolution, drastically reducing the residual stresses. Heat treatments at 900 and 980 °C involved the formation of δ phases, whereas 1065 °C generated carbides. These heat treatments were also performed on components with narrow internal channels revealing that heat treatments up to 900 °C did not trigger sintering mechanisms allowing to remove the powder from the inner channels.

scholarly journals Optimization of the Post-Process Heat Treatment of Inconel 718 Superalloy Fabricated by Laser Powder Bed Fusion Process

Metals ◽  
2021 ◽  
Vol 11 (1) ◽  
pp. 144
Author(s):  
Eslam M. Fayed ◽  
Mohammad Saadati ◽  
Davood Shahriari ◽  
Vladimir Brailovski ◽  
Mohammad Jahazi ◽  
...  
Keyword(s):  
Inconel 718 ◽  
Mechanical Performance ◽  
Solution Treatment ◽  
Heat Treatments ◽  
Powder Bed Fusion ◽  
Laser Powder Bed Fusion ◽  
Homogenization Treatment ◽  
Powder Bed ◽  
Post Process ◽  
High Fraction

In the present study, multi-objective optimization is employed to develop the optimum heat treatments that can achieve both high-mechanical performance and non-distinctive crystallographic texture of 3D printed Inconel 718 (IN718) fabricated by laser powder bed fusion (LPBF). Heat treatments including homogenization at different soaking times (2, 2.5, 3, 3.5 and 4 h) at 1080 °C, followed by a 1 h solution treatment at 980 °C and the standard aging have been employed. 2.5 h is found to be the homogenization treatment threshold after which there is a depletion of hardening precipitate constituents (Nb and Ti) from the γ-matrix. However, a significant number of columnar grains with a high fraction (37.8%) of low-angle grain boundaries (LAGBs) have still been retained after the 2.5 h homogenization treatment. After a 4 h homogenization treatment, a fully recrystallized IN718 with a high fraction of annealing twins (87.1%) is obtained. 2.5 and 4 h homogenization treatments result in tensile properties exceeding those of the wrought IN718 at both RT and 650 °C. However, considering the texture requirements, it is found that the 4 h homogenization treatment offers the optimum treatment, which can be used to produce IN718 components offering a balanced combination of high mechanical properties and adequate microstructural isotropy.

scholarly journals In Situ Alloying of a Modified Inconel 625 via Laser Powder Bed Fusion: Microstructure and Mechanical Properties

Metals ◽  
2021 ◽  
Vol 11 (6) ◽  
pp. 988
Author(s):  
Giulio Marchese ◽  
Margherita Beretta ◽  
Alberta Aversa ◽  
Sara Biamino
Keyword(s):  
Mechanical Properties ◽  
Base Alloy ◽  
Heat Treatments ◽  
Inconel 625 ◽  
Powder Bed Fusion ◽  
Laser Powder Bed Fusion ◽  
Powder Bed ◽  
Melt Pool ◽  
Composition Modification

This study investigates the in situ alloying of a Ni-based superalloy processed by means of laser powder bed fusion (LPBF). For this purpose, Inconel 625 powder is mixed with 1 wt.% of Ti6Al4V powder. The modified alloy is characterized by densification levels similar to the base alloy, with relative density superior to 99.8%. The material exhibits Ti-rich segregations along the melt pool contours. Moreover, Ti tends to be entrapped in the interdendritic areas during solidification in the as-built state. After heat treatments, the modified Inconel 625 version presents greater hardness and tensile strengths than the base alloy in the same heat-treated conditions. For the solution annealed state, this is mainly attributed to the elimination of the segregations into the interdendritic structures, thus triggering solute strengthening. Finally, for the aged state, the further increment of mechanical properties can be attributed to a more intense formation of phases than the base alloy, due to elevated precipitation strengthening ability under heat treatments. It is interesting to note how slight chemical composition modification can directly develop new alloys by the LPBF process.

scholarly journals Pandora’s Box–Influence of Contour Parameters on Roughness and Subsurface Residual Stresses in Laser Powder Bed Fusion of Ti-6Al-4V

Materials ◽  
2020 ◽  
Vol 13 (15) ◽  
pp. 3348
Author(s):  
Katia Artzt ◽  
Tatiana Mishurova ◽  
Peter-Philipp Bauer ◽  
Joachim Gussone ◽  
Pere Barriobero-Vila ◽  
...  
Keyword(s):  
Surface Roughness ◽  
Residual Stresses ◽  
Surface Quality ◽  
Powder Bed Fusion ◽  
Fuel Injector ◽  
Laser Powder Bed Fusion ◽  
Powder Bed ◽  
Melt Pool ◽  
Contour Lines ◽  
High Laser

The contour scan strategies in laser powder bed fusion (LPBF) of Ti-6Al-4V were studied at the coupon level. These scan strategies determined the surface qualities and subsurface residual stresses. The correlations to these properties were identified for an optimization of the LPBF processing. The surface roughness and the residual stresses in build direction were linked: combining high laser power and high scan velocities with at least two contour lines substantially reduced the surface roughness, expressed by the arithmetic mean height, from values as high as 30 µm to 13 µm, while the residual stresses rose from ~340 to about 800 MPa. At this stress level, manufactured rocket fuel injector components evidenced macroscopic cracking. A scan strategy completing the contour region at 100 W and 1050 mm/s is recommended as a compromise between residual stresses (625 MPa) and surface quality (14.2 µm). The LPBF builds were monitored with an in-line twin-photodiode-based melt pool monitoring (MPM) system, which revealed a correlation between the intensity quotient I2/I1, the surface roughness, and the residual stresses. Thus, this MPM system can provide a predictive estimate of the surface quality of the samples and resulting residual stresses in the material generated during LPBF.

scholarly journals Multi-Scale Modeling of Residual Stresses Evolution in Laser Powder Bed Fusion of Inconel 625

2021 ◽  
Vol 6 (1) ◽  
pp. 2
Author(s):  
Mohamed Balbaa ◽  
Mohamed Elbestawi
Keyword(s):  
Residual Stresses ◽  
Cooling Rate ◽  
Process Parameters ◽  
Laser Exposure ◽  
Powder Bed Fusion ◽  
Laser Powder Bed Fusion ◽  
Linear Temperature ◽  
Powder Bed ◽  
Multi Scale ◽  
Melt Pool

Laser powder bed fusion exhibits many advantages for manufacturing complex geometries from hard to machine alloys such as IN625. However, a major drawback is the formation of high tensile residual stresses, and the complex relationship between the process parameters and the residual stresses has not been fully investigated. The current study presents multi-scale models to examine the variation of process parameters on melt pool dimensions, cyclic temperature evolutions, cooling rate, and cyclic stress generation and how they affect the stress end state. In addition, the effect of the same energy density, which is often overlooked, on the generated residual stresses is investigated. Multi-level validation is performed based on melt pool dimensions, temperature measurements with a two-color pyrometer, and finally, in-depth residual stress measurement. The results show that scan speed has the strongest effect on residual stresses, followed by laser power and hatch spacing. The results are explained in light of the non-linear temperature evolution, temperature gradient, and cooling rate during laser exposure, cooling time, and the rate during recoating time.

scholarly journals Knowledge of process-structure-property relationships to engineer better heat treatments for laser powder bed fusion additive manufactured Inconel 718

2020 ◽  
Vol 31 ◽  
pp. 100977 ◽  
Author(s):  
Thomas G. Gallmeyer ◽  
Senthamilaruvi Moorthy ◽  
Branden B. Kappes ◽  
Michael J. Mills ◽  
Behnam Amin-Ahmadi ◽  
...  
Keyword(s):  
Inconel 718 ◽  
Heat Treatments ◽  
Powder Bed Fusion ◽  
Structure Property ◽  
Laser Powder Bed Fusion ◽  
Powder Bed ◽  
Structure Property Relationships ◽  
Process Structure

scholarly journals Comparison of Phase Characteristics and Residual Stresses in Ti-6Al-4V Alloy Manufactured by Laser Powder Bed Fusion (L-PBF) and Electron Beam Powder Bed Fusion (EB-PBF) Techniques

Crystals ◽  
2021 ◽  
Vol 11 (7) ◽  
pp. 796
Author(s):  
Aya Takase ◽  
Takuya Ishimoto ◽  
Naotaka Morita ◽  
Naoko Ikeo ◽  
Takayoshi Nakano
Keyword(s):  
Electron Beam ◽  
Residual Stresses ◽  
Cooling Rate ◽  
Process Parameters ◽  
Phase Evolution ◽  
Powder Bed Fusion ◽  
Laser Powder Bed Fusion ◽  
Solidification Temperature ◽  
Powder Bed ◽  
Β Phase

Ti-6Al-4V alloy fabricated by laser powder bed fusion (L-PBF) and electron beam powder bed fusion (EB-PBF) techniques have been studied for applications ranging from medicine to aviation. The fabrication technique is often selected based on the part size and fabrication speed, while less attention is paid to the differences in the physicochemical properties. Especially, the relationship between the evolution of α, α’, and β phases in as-grown parts and the fabrication techniques is unclear. This work systematically and quantitatively investigates how L-PBF and EB-PBF and their process parameters affect the phase evolution of Ti-6Al-4V and residual stresses in the final parts. This is the first report demonstrating the correlations among measured parameters, indicating the lattice strain reduces, and c/a increases, shifting from an α’ to α+β or α structure as the crystallite size of the α or α’ phase increases. The experimental results combined with heat-transfer simulation indicate the cooling rate near the β transus temperature dictates the resulting phase characteristics, whereas the residual stress depends on the cooling rate immediately below the solidification temperature. This study provides new insights into the previously unknown differences in the α, α’, and β phase evolution between L-PBF and EB-PBF and their process parameters.

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