This paper presents the results of a study performed with an experimental domestic sewage treatment plant (240 m3.d-1 flow) consisting of expanded bed anaerobic reactor (EBAR) followed by dissolved air flotation (DAF) unit. For the flotation step, the anaerobic reactor effluent was previously coagulated with 50 mgFeCl3.l-1 and flocculated under different conditions (mean velocity gradient, Gf, and flocculation time, Tf). The Gf values were from 60 to 100 s-1 associated with 13 and 20 min Tf values. During the tests, the following operational conditions of the flotation unit were maintained: chemical addition (50 mgFeCl3.l-1), 18% recirculation rate associated with a pressure of 450 ± 10 kPa in the saturation chamber and overflow rate of 180 m3.mÐ2.d-1. Temperature ranged from 23.8¡C to 30.01/4C. Best results were achieved for Gf = 80 s-1 and Tf = 20 min. For these conditions, the DAF unit removal efficiencies were: 94.4% for chemical oxygen demand (with 53 mg.l-1 COD residual), 87% for phosphorus (with 0.80 mgP.l-1 residual), 96.7% for total suspended solids (with 9 mg.l-1 TSS residual) and 96.4% for turbidity (with 12.9 NTU residual), when the anaerobic reactor effluents have worst quality during the whole day.