Initial stages of Nb3Sn phase formation in Nb-bronze matrix composite wires investigated by means of electron microscopy

Rare Metals ◽  
2020 ◽  
Author(s):  
Shu-Rui Li ◽  
Bin Hu ◽  
Hui-Jie Ren ◽  
Lei Wang ◽  
Xing-Ming Wang
2015 ◽  
Vol 69 (8) ◽  
Author(s):  
Jolanta Kochana ◽  
Katarzyna Hnida ◽  
Grzegorz Sulka ◽  
Paweł Knihnicki ◽  
Joanna Kozak ◽  
...  

AbstractPolypyrrole nanowires (PPyNWs) were fabricated and examined as a structural component of amperometric biosensor matrix. An enzyme, tyrosinase (TYR), was immobilized onto PPyNWs using glutaraldehyde (GA). Matrix composite morphology was investigated using scanning electron microscopy. Electrochemical behavior of the prepared PPyNWs/GA/TYR biosensor towards catechol was studied and the assessment of its analytical characteristics was carried out taking into account linear range, sensitivity, repeatability, reproducibility and operational stability.


2019 ◽  
Vol 26 (1) ◽  
pp. 18-28
Author(s):  
Yingwei Fan ◽  
Xiaorong Zhou

AbstractThe kinetics and mechanisms of interface reactions in a unidirectional continuous SiC fiber-reinforced Ti-17 matrix composite were investigated using transmission electron microscopy and scanning electron microscopy. It was found that a reaction zone (RZ) consisting of two-layered TiC-type carbide forms at the fiber/matrix interface during fabrication of the composite. After isothermal exposure at elevated temperatures, the two-layered TiC-type carbide is inherited, and a new TiC-type carbide layer forms within the RZ after exposure at temperatures lower than 900°C, while a new Ti3C2-type carbide layer forms after exposure at 900°C. It was also observed that the growth of RZ is a diffusion-controlled and temperature-dependent process, obeying the Fick's law-based parabolic relationship and the Arrhenius equation. Two material constants, the temperature-independent rate constant k0 and activation energy Q, are determined as 31.5 × 10−4µm/s1/2 and 49.9 kJ/mol, respectively.


2012 ◽  
Vol 706-709 ◽  
pp. 687-692
Author(s):  
Li Ming Peng ◽  
Bin Hu ◽  
Wen Jiang Ding

Metal matrix composites reinforced with discontinuous reinforcement (short fiber, whisker or particle) are attractive for applications requiring higher stiffness and strength than traditional alloys. Unlike continuously reinforced composites, where the properties are mainly influenced by fibers, the properties of the discontinuously reinforced composites seem to be influenced more by matrix properties. Most of the discontinuously reinforced composites are based on age-hardenable light alloys, so that aging treatments can be applied to develop the optimum properties of the composites. The aging behavior of discontinuously reinforced composites has been a subject of great interest both from scientific and technological view points. Recently developed NZ30K (Mg-3wt.%Nd-0.5wt.%Zn-0.5wt.%Zr) alloys exhibit higher specific strength at both room and elevated temperatures, better strength and creep resistance than the existing commercial magnesium alloys. Accordingly, this alloy can be considered as a candidate material for potential automobile applications, such as engine blocks and pistons, which experience high service temperature. Its use could save considerable mass weight in powertrain systems. However, low elastic modulus and wear resistance of magnesium alloys limit their widespread applications. Metal matrix composites have been proposed as the feasible and economical solution. The aim of this study is to investigate the effect of alumina fibers on the aging hardening kinetics and age-hardening efficiency of squeeze cast NZ30K/Saffil/15p magnesium matrix composite. The aging behavior has been examined using Vickers, combined with microstructure observation developed during heat treatment by optical microscopy, scanning electron microscopy (SEM) and transmission electron microscopy (TEM).


2011 ◽  
Vol 172-174 ◽  
pp. 517-522 ◽  
Author(s):  
Paolo Galimberti ◽  
Sabine Lay ◽  
Annie Antoni-Zdziobek

The precipitation behaviour of the Fe20Co18W (wt%) alloy was studied by transmission electron microscopy during aging treatments at 800°C. The decomposition of the matrix produces the C14 phase. At the beginning of the heat treatment, the observation at the atom scale indicates that the structure of the precipitates does not coincide exactly with the Laves phase. Using the orientation relationship between the Fe based matrix and the precipitates it is shown that simple atomic shifts can lead to the transformation from the bcc matrix to the C14 Laves phase.


Sign in / Sign up

Export Citation Format

Share Document