Effect of intergranular phase segregation on magnetic properties of NdFeB magnet

2014 ◽  
Vol 10 (1) ◽  
pp. 153-157 ◽  
Author(s):  
Gülten Sadullahoğlu ◽  
Baki Altuncevahir ◽  
A. Okan Addemir
2006 ◽  
Vol 299 (1) ◽  
pp. 195-204 ◽  
Author(s):  
J. Li ◽  
Y. Liu ◽  
S.J. Gao ◽  
M. Li ◽  
Y.Q. Wang ◽  
...  

2009 ◽  
Vol 54 (18) ◽  
pp. 3206-3210
Author(s):  
Min Liu ◽  
RuWei Gao ◽  
GuangBing Han ◽  
Wu Yang

Materials ◽  
2020 ◽  
Vol 13 (15) ◽  
pp. 3319
Author(s):  
M. Parans Paranthaman ◽  
Volkan Yildirim ◽  
Tej Nath Lamichhane ◽  
Benjamin A. Begley ◽  
Brian K. Post ◽  
...  

Extrusion based additive manufacturing of polymer composite magnets can increase the solid loading volume fraction with greater mechanical force through the printing nozzle as compared to traditional injection molding process. About 63 vol% of isotropic NdFeB magnet powders were compounded with 37 vol% of polyphenylene sulfide and bonded permanent magnets were fabricated while using Big Area Additive Manufacturing without any degradation in magnetic properties. The polyphenylene sulfide bonded magnets have a tensile stress of 20 MPa, almost double than that of nylon bonded permanent magnets. Additively manufactured and surface-protective-resin coated bonded magnets meet the industrial stability criterion of up to 175 °C with a flux-loss of 2.35% over 1000 h. They also exhibit better corrosion resistance behavior when exposed to acidic (pH = 1.35) solution for 24 h and also annealed at 80 °C over 100 h (at 95% relative humidity) over without coated magnets. Thus, polyphenylene sulfide bonded, additively manufactured, protective resin coated bonded permanent magnets provide better thermal, mechanical, and magnetic properties.


2020 ◽  
Vol 31 (22) ◽  
pp. 20431-20443
Author(s):  
Lennart Leich ◽  
Arne Röttger ◽  
Rene Kuchenbecker ◽  
Werner Theisen

AbstractThis study investigates the compaction of nanocrystalline NdFeB magnet powder by electro-discharge sintering (EDS). On this account, process parameters, microstructure, and the associated magnetic properties of the EDS-densified nanocrystalline NdFeB specimens were investigated by varying the discharge energy EEDS and compression load pEDS. Although optimized process parameters could be evaluated, three different microstructures (fully densified zone, insufficiently densified zone, and melted zone) are present in the EDS-compacted specimens. Thereby, volume fractions of these formed three different microstructures determine the resulting mechanical and magnetic properties of the specimens. For all specimens, the intrinsic coercivity Hc,J deteriorates with increasing discharge energy, as the generated Joule heat leads to microstructural changes (grain growth, dissolution of magnetic phases), which reduces the magnetic properties. The compression load has less influence on the coercivity Hc,J, as it only affects the initial resistance of the pre-compacted powder loose. The residual induction Br deteriorates with increasing the discharge energy due to microstructural changes. An increase in the compression load pEDS results in an increase in the specimens’ density and thus promotes the residual induction Br.


2007 ◽  
Vol 15 (11) ◽  
pp. 1483-1488 ◽  
Author(s):  
Wenjian Mo ◽  
Lanting Zhang ◽  
Aidang Shan ◽  
Lijun Cao ◽  
Jiansheng Wu ◽  
...  

1993 ◽  
Vol 07 (01n03) ◽  
pp. 725-728
Author(s):  
P. SCHREY ◽  
M. VELICESCU

Powder metallurgical additions of Bi enhance the temperature stability of (Nd, Dy)-Fe-B permanent magnets. Bi is not solved in the hardmagnetic RE2Fe14B phase, thus does not influence the intrinsic magnetic properties, Only the microstructure of the sintered magnets is changed. Addition of a few wt.% of Bi leads to the formation of a new ternary intergranular phase with the composition Nd6Fe13Bi. This phase substitutes partially the intergranular Nd-rich phase providing the magnetic insulation of hardmagnetic grains. An enhancement of HCJ by about 40% was reached at 150 ºC for a Nd15.5Dy1.5Fe74AlB8 magnet containing 2.5 wt.% Bi compared to the Bi-free material.


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