Nanocrystalline diamond sheets as protective coatings for fiber-optic measurement head

Carbon ◽  
2020 ◽  
Vol 156 ◽  
pp. 104-109 ◽  
Author(s):  
Monika Kosowska ◽  
Daria Majchrowicz ◽  
Mateusz Ficek ◽  
Paweł Wierzba ◽  
Yafit Fleger ◽  
...  
Materials ◽  
2019 ◽  
Vol 12 (13) ◽  
pp. 2124 ◽  
Author(s):  
Monika Kosowska ◽  
Daria Majchrowicz ◽  
Kamatchi J. Sankaran ◽  
Mateusz Ficek ◽  
Ken Haenen ◽  
...  

This paper reports the application of doped nanocrystalline diamond (NCD) films—nitrogen-doped NCD and boron-doped NCD—as reflective surfaces in an interferometric sensor of refractive index dedicated to the measurements of liquids. The sensor is constructed as a Fabry–Pérot interferometer, working in the reflective mode. The diamond films were deposited on silicon substrates by a microwave plasma enhanced chemical vapor deposition system. The measurements of refractive indices of liquids were carried out in the range of 1.3 to 1.6. The results of initial investigations show that doped NCD films can be successfully used in fiber-optic sensors of refractive index providing linear work characteristics. Their application can prolong the lifespan of the measurement head and open the way to measure biomedical samples and aggressive chemicals.


Measurement ◽  
2021 ◽  
pp. 110495
Author(s):  
Małgorzata Szczerska ◽  
Monika Kosowska ◽  
Paulina Listewnik ◽  
Michał Rycewicz ◽  
Mikhael Bechelany ◽  
...  

2002 ◽  
Vol 16 (06n07) ◽  
pp. 1013-1017 ◽  
Author(s):  
JINGQI LI ◽  
DEYAN HE ◽  
WANTU GUO ◽  
JIHUA ZHANG ◽  
YINING SUN ◽  
...  

Nanocrystalline diamond thin films have been grown on both sides of Si wafer by microwave plasma-enhanced chemical vapor deposition using a mixture of CH4 and H2 as source gas. It was shown that infrared transmission of Si has been greatly enhanced and the maximum transmittance reaches 85%. By optimizing the film thickness, we can obtain the maximum increment in the desired infrared wavelength range. Sand spraying test showed that, while the bare Si substrate exhibited obvious surface damage, no damage could be observed on the diamond surface after the sand spraying. The results confirm that the nanocrystalline diamond films coated on Si can not only increase the infrared transmission but also act as a protective coating.


2002 ◽  
Vol 91 (12) ◽  
pp. 10068 ◽  
Author(s):  
W. B. Yang ◽  
F. X. Lü ◽  
Z. X. Cao

Author(s):  
J. M. Cowley ◽  
R. Glaisher ◽  
J. A. Lin ◽  
H.-J. Ou

Some of the most important applications of STEM depend on the variety of imaging and diffraction made possible by the versatility of the detector system and the serial nature, of the image acquisition. A special detector system, previously described, has been added to our STEM instrument to allow us to take full advantage of this versatility. In this, the diffraction pattern in the detector plane may be formed on either of two phosphor screens, one with P47 (very fast) phosphor and the other with P20 (high efficiency) phosphor. The light from the phosphor is conveyed through a fiber-optic rod to an image intensifier and TV system and may be photographed, recorded on videotape, or stored digitally on a frame store. The P47 screen has a hole through it to allow electrons to enter a Gatan EELS spectrometer. Recently a modified SEM detector has been added so that high resolution (10Å) imaging with secondary electrons may be used in conjunction with other modes.


2019 ◽  
Vol 107 (3) ◽  
pp. 305
Author(s):  
Mengmei Geng ◽  
Yuting Long ◽  
Tongqing Liu ◽  
Zijuan Du ◽  
Hong Li ◽  
...  

Surface-enhanced Raman Scattering (SERS) fiber probe provides abundant interaction area between light and materials, permits detection within limited space and is especially useful for remote or in situ detection. A silver decorated SERS fiber optic probe was prepared by hydrothermal method. This method manages to accomplish the growth of silver nanoparticles and its adherence on fiber optic tip within one step, simplifying the synthetic procedure. The effects of reaction time on phase composition, surface plasmon resonance property and morphology were investigated by X-ray diffraction analysis (XRD), ultraviolet-visible absorption spectrum (UV-VIS absorption spectrum) and scanning electron microscope (SEM). The results showed that when reaction time is prolonged from 4–8 hours at 180 °C, crystals size and size distribution of silver nanoparticles increase. Furthermore, the morphology, crystal size and distribution density of silver nanoparticles evolve along with reaction time. A growth mechanism based on two factors, equilibrium between nucleation and growth, and the existence of PVP, is hypothesized. The SERS fiber probe can detect rhodamin 6G (R6G) at the concentration of 10−6 M. This SERS fiber probe exhibits promising potential in organic dye and pesticide residue detection.


2020 ◽  
pp. 15-23
Author(s):  
V. M. Grechishnikov ◽  
E. G. Komarov

The design and operation principle of a multi-sensor Converter of binary mechanical signals into electrical signals based on a partitioned fiber-optic digital-to-analog Converter with a parallel structure is considered. The digital-to-analog Converter is made from a set of simple and technological (three to five digit) fiber-optic digital-to-analog sections. The advantages of the optical scheme of the proposed. Converter in terms of metrological and energy characteristics in comparison with single multi-bit converters are justified. It is shown that by increasing the number of digital-analog sections, it is possible to repeatedly increase the information capacity of a multi-sensor Converter without tightening the requirements for its manufacturing technology and element base. A mathematical model of the proposed Converter is developed that reflects the features of its operation in the mode of sequential time conversion of the input code vectors of individual fiber-optic sections into electrical analogues and the formation of the resulting output code vector.


Metrologiya ◽  
2020 ◽  
pp. 38-51
Author(s):  
V. N. Astapov ◽  
I. N. Kozlova

This article presents the rationale and methodology for developing an intrinsically safe device, namely, a hydrostatic fiber optic sensor with a position-sensitive detector for monitoring the level of oil products in large-capacity tanks at oil depots and during pumping in a raw material warehouses. This device suitable for continuous monitoring of the liquid level, based on the measurement of a hydrostatic column of liquid with automatic offset of changes in the density of the liquid. Offset is carried out by means of a displacer (a fully submerged float), inside which a housing with a position-sensitive detector (PSD) is integrated. Theoretical validation of the bellows suspension usage for a displacer is given. During filling a container with a liquid whose level is measured, liquid bellows, the movement of which is recorded by an optical triangulation sensor using the reflected infrared ray incident on the bottom of the bellows. The principle of the triangulation sensor operation is based on the geometric properties of the triangles. The pulses of infrared radiation come through a fiber optic cable. In order to measure the movement of the surface (the bottom of the bellows) by measuring the movement of the reflected beam, a position-sensitive detector is used, which is located in a remote controller. In this device for the intrinsic safety problem solution, optical inputs of a fiber optic flat cable are located in the active zone of the sensor, which is connected to the optical inputs of a position-sensitive detector, operated on the principles of photoelectric effect. The light spot moving along the sensitive zone and converted by the detector into a one-dimensional signal proportional to the distance to the object. hydrostatically applies pressure over the entire effective area of the measuring


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