Determination of tropane alkaloids atropine and scopolamine by liquid chromatography–mass spectrometry in plant organs of Datura species

2012 ◽  
Vol 1232 ◽  
pp. 295-301 ◽  
Author(s):  
Silvia Jakabová ◽  
Lajos Vincze ◽  
Ágnes Farkas ◽  
Ferenc Kilár ◽  
Borbála Boros ◽  
...  
Keyword(s):  
Mass Spectrometry ◽  
Liquid Chromatography ◽  
Tropane Alkaloids ◽  
Liquid Chromatography Mass Spectrometry ◽  
Plant Organs ◽  
Chromatography Mass Spectrometry

Gas-Liquid Chromatography-Mass Spectrometry Investigation of Tropane Alkaloids in Hyoscyamus albus L. from Morocco

2012 ◽  
Vol 67 (9-10) ◽  
pp. 461-465 ◽  
Author(s):  
Ahmed El Bazaoui ◽  
My Ahmed Bellimam ◽  
Ibn Toumert Lançar ◽  
Abdelmajid Soulaymani
Keyword(s):  
Mass Spectrometry ◽  
Liquid Chromatography ◽  
Tropane Alkaloids ◽  
Gas Liquid Chromatography ◽  
Liquid Chromatography Mass Spectrometry ◽  
Plant Organs ◽  
Chromatography Mass Spectrometry ◽  
New Compounds ◽  
First Time ◽  
Hyoscyamus Albus

Thirty-four alkaloids were identified in the organs of Hyoscyamus albus L. by gas-liquid chromatography-mass spectrometry (GLC-MS). Eight new compounds for the roots, eleven for the stems, twelve for the leaves, nineteen for the flowers, and seven for the seeds were detected. The alkaloids 5-(2-oxopropyl)-hygrine (8) and phygrine (20) are new for this species and 3-(hydroxyacetoxy)tropane (9), 6,7-dehydro-3-phenylacetoxytropane (15), 3-(2’-phenylpropionyloxy) tropane (17), 6,7-dehydro-3-apotropoyloxytropane (18), 3-(3’-methoxytropoyloxy)tropane (23), and aponorscopolamine (25) are described for the first time for the genus Hyoscyamus. Hyoscyamine was the main alkaloid in the plant organs

scholarly journals Determination of regulatory ionophore coccidiostat residues in feedstuffs at carry-over levels by liquid chromatography-mass spectrometry

PLoS ONE ◽  
2017 ◽  
Vol 12 (8) ◽  
pp. e0182831 ◽  
Author(s):  
Loredana Annunziata ◽  
Pierina Visciano ◽  
Arianna Stramenga ◽  
Maria Novella Colagrande ◽  
Guido Campana ◽  
...  
Keyword(s):  
Mass Spectrometry ◽  
Liquid Chromatography ◽  
Liquid Chromatography Mass Spectrometry ◽  
Chromatography Mass Spectrometry ◽  
Carry Over
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