High polar organic–inorganic hybrid coating stir bar sorptive extraction combined with high performance liquid chromatography–inductively coupled plasma mass spectrometry for the speciation of seleno-amino acids and seleno-oligopeptides in biological samples

2012 ◽  
Vol 1256 ◽  
pp. 32-39 ◽  
Author(s):  
Xiangju Mao ◽  
Bin Hu ◽  
Man He ◽  
Beibei Chen
Author(s):  
Yung-Chun Chen ◽  
Shiuh-Jen Jiang

Liquid chromatography and dynamic reaction cell inductively coupled plasma mass spectrometry are used in tandem for the simultaneous speciation of arsenic and mercury in fish.


Author(s):  
J.S. Edmonds ◽  
Y. Shibata ◽  
R.I.T. Prince ◽  
K.A. Francesconi ◽  
M. Morita

Examination of extracts of tissues of a leatherback turtle, Dermochelys coriacea (L.) (Reptilia: Dermochelyidae) by high-performance liquid chromatography inductively coupled plasma-mass spectrometry has demonstrated the presence of arsenobetaine, arsenocholine and inorganic arsenate in heart muscle and liver, and arsenobetaine and inorganic arsenate in pectoral muscle. Although arsenobetaine was the major form in all tissues, inorganic arsenate and arsenocholine accounted for 50% and 15% respectively of arsenic in aqueous extracts of the liver.


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