Screening for mineral oil hydrocarbons in vegetable oils by silver ion–planar solid phase extraction

2021 ◽  
pp. 462732
Author(s):  
Melanie Wagner ◽  
Claudia Oellig
Keyword(s):  
Solid Phase Extraction ◽  
Vegetable Oils ◽  
Solid Phase ◽  
Mineral Oil ◽  
Silver Ion ◽  
Phase Extraction ◽  
Oil Hydrocarbons ◽  
Mineral Oil Hydrocarbons

scholarly journals ANÁLISE DE PESTICIDAS ORGANOCLORADOS EM ÓLEOS VEGETAIS POR CROMATOGRAFIA GASOSA DE ALTA RESOLUÇÃO (HRGC)

2018 ◽  
Vol 35 (3) ◽  
pp. 189
Author(s):  
Eudécio Bonfim dos Santos Dias ◽  
Eliane Da Costa Vilela ◽  
Fernando Mauro Lanças
Keyword(s):  
Solid Phase Extraction ◽  
Vegetable Oil ◽  
Vegetable Oils ◽  
Concentration Level ◽  
Solid Phase ◽  
Agricultural Products ◽  
Phase Extraction ◽  
Human Diet ◽  
Animal Fats ◽  
Chemical Products

Vegetable oil were introduced in human diet in the last decade to change the use of animal fats. The chemical products althrought utilized in correct manner can cause residues in food bring to healt there be a necessity of a constant monitoring of the concentration level the several agricultural products. The answer to this necessity has motivated the development of several of a methodology for simultaneous analysis of aldrin, dieldrin, endrin and endosulfanin vegetable oils by HRGC, using solid phase extraction (SPE) using silica and XAD-2. The recovery was 70-110%.

scholarly journals Determination of Aflatoxin B1 and B2 in Vegetable Oils Using Fe3O4/rGO Magnetic Solid Phase Extraction Coupled with High-Performance Liquid Chromatography Fluorescence with Post-Column Photochemical Derivatization

Toxins ◽  
2019 ◽  
Vol 11 (11) ◽  
pp. 621 ◽  
Author(s):  
Li Yu ◽  
Fei Ma ◽  
Liangxiao Zhang ◽  
Peiwu Li
Keyword(s):  
High Performance Liquid Chromatography ◽  
Solid Phase Extraction ◽  
Vegetable Oils ◽  
High Performance ◽  
Solid Phase ◽  
Magnetic Solid Phase Extraction ◽  
Phase Extraction ◽  
Magnetic Solid ◽  
Graphene Nanocomposite

In this study, magnetic graphene nanocomposite Fe3O4/rGO was synthesized by facile one-pot solvothermal method. The nanocomposite was successfully used as magnetic solid phase extraction (MSPE) adsorbents for the determination of aflatoxins in edible vegetable oils through the π–π stacking interactions. MSPE parameters including the amount of adsorbents, extraction and desorption time, washing conditions, and the type and volume of desorption solvent were optimized. Under optimal conditions, good linear relationships were achieved. Limits of detection of this method were as low as 0.02 µg/kg and 0.01 µg/kg for aflatoxin B1 and B2, respectively. Finally, the magnetic graphene nanocomposite was successfully applied to aflatoxin analysis in vegetable oils. The results indicated that the recoveries of the B-group aflatoxins ranged from 80.4% to 106.0%, whereas the relative standard deviations (RSDs) were less than 8.1%. Owing to the simplicity, rapidity and efficiency, Fe3O4/rGO magnetic solid phase extraction coupled with high-performance liquid chromatography fluorescence with post-column photochemical derivatization (Fe3O4/rGO MSPE-HPLC-PCD-FLD) is a promising analytical method for routine and accurate determination of aflatoxins in lipid matrices.

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