An energy–momentum couple stress formula for variational-based macroscopic modelings of roving-matrix composites in dynamics

As part of a broad program on composite materials, the role of the interface on the micromechanics of deformation of metal-matrix composites is being studied. The approach is to correlate elastic behavior, micro and macroyielding, flow, and fracture behavior with associated structural detail (dislocation substructure, fracture characteristics) and stress-state. This provides an understanding of the mode of deformation from an atomistic viewpoint; a critical evaluation can then be made of existing models of composite behavior based on continuum mechanics. This paper covers the electron microscopy (transmission, fractography, scanning microscopy) of two distinct forms of composite material: conventional fiber-reinforced (aluminum-stainless steel) and directionally solidified eutectic alloys (aluminum-copper). In the former, the interface is in the form of a compound and/or solid solution whereas in directionally solidified alloys, the interface consists of a precise crystallographic boundary between the two constituents of the eutectic.

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TEM examination of 2014-SiC metal matrix composite

Proceedings, annual meeting, Electron Microscopy Society of America ◽

10.1017/s0424820100105692 ◽

1988 ◽

Vol 46 ◽

pp. 726-727

Author(s):

M. G. Burke ◽

M. N. Gungor ◽

P. K. Liaw

Keyword(s):

Metal Matrix Composite ◽

Metal Matrix Composites ◽

Matrix Composite ◽

Metal Matrix ◽

Tensile Deformation ◽

Microstructural Characterization ◽

Thin Foil ◽

Matrix Alloy ◽

Matrix Composites ◽

Ion Milling

Aluminum-based metal matrix composites offer unique combinations of high specific strength and high stiffness. The improvement in strength and stiffness is related to the particulate reinforcement and the particular matrix alloy chosen. In this way, the metal matrix composite can be tailored for specific materials applications. The microstructural characterization of metal matrix composites is thus important in the development of these materials. In this study, the structure of a p/m 2014-SiC particulate metal matrix composite has been examined after extrusion and tensile deformation.Thin-foil specimens of the 2014-20 vol.% SiCp metal matrix composite were prepared by dimpling to approximately 35 μm prior to ion-milling using a Gatan Dual Ion Mill equipped with a cold stage. These samples were then examined in a Philips 400T TEM/STEM operated at 120 kV. Two material conditions were evaluated: after extrusion (80:1); and after tensile deformation at 250°C.

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Preparation of Electron Transparent Metal-Matrix Composites

Proceedings, annual meeting, Electron Microscopy Society of America ◽

10.1017/s0424820100101414 ◽

1968 ◽

Vol 26 ◽

pp. 334-335 ◽

Cited By ~ 2

Author(s):

M. R. Pinnel ◽

A. Lawley

Keyword(s):

Stainless Steel ◽

Load Transfer ◽

Volume Fraction ◽

Steel Wire ◽

Initial Step ◽

Interfacial Region ◽

Matrix Composites ◽

Specific Test ◽

The Matrix ◽

The One

Numerous phenomenological descriptions of the mechanical behavior of composite materials have been developed. There is now an urgent need to study and interpret deformation behavior, load transfer, and strain distribution, in terms of micromechanisms at the atomic level. One approach is to characterize dislocation substructure resulting from specific test conditions by the various techniques of transmission electron microscopy. The present paper describes a technique for the preparation of electron transparent composites of aluminum-stainless steel, such that examination of the matrix-fiber (wire), or interfacial region is possible. Dislocation substructures are currently under examination following tensile, compressive, and creep loading. The technique complements and extends the one other study in this area by Hancock.The composite examined was hot-pressed (argon atmosphere) 99.99% aluminum reinforced with 15% volume fraction stainless steel wire (0.006″ dia.).Foils were prepared so that the stainless steel wires run longitudinally in the plane of the specimen i.e. the electron beam is perpendicular to the axes of the wires. The initial step involves cutting slices ∼0.040″ in thickness on a diamond slitting wheel.

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Deformation at interfaces of Ti-6Al-4V/SiC fiber composites

Proceedings, annual meeting, Electron Microscopy Society of America ◽

10.1017/s0424820100121193 ◽

1992 ◽

Vol 50 (1) ◽

pp. 158-159

Author(s):

Warren J. Moberly ◽

Daniel B. Miracle ◽

S. Krishnamurthy

Keyword(s):

Thermal Stresses ◽

Load Transfer ◽

Coefficient Of Thermal Expansion ◽

Hot Isostatic Pressing ◽

Matrix Composites ◽

Ongoing Research ◽

Aerospace Applications ◽

Sic Fiber ◽

The Matrix ◽

Intermetallic Matrix Composites

Titanium-aluminum alloy metal matrix composites (MMC) and Ti-Al intermetallic matrix composites (IMC), reinforced with continuous SCS6 SiC fibers are leading candidates for high temperature aerospace applications such as the National Aerospace Plane (NASP). The nature of deformation at fiber / matrix interfaces is characterized in this ongoing research. One major concern is the mismatch in coefficient of thermal expansion (CTE) between the Ti-based matrix and the SiC fiber. This can lead to thermal stresses upon cooling down from the temperature incurred during hot isostatic pressing (HIP), which are sufficient to cause yielding in the matrix, and/or lead to fatigue from the thermal cycling that will be incurred during application, A second concern is the load transfer, from fiber to matrix, that is required if/when fiber fracture occurs. In both cases the stresses in the matrix are most severe at the interlace.

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A TEM investigation of silicon nitride whiskers

Proceedings, annual meeting, Electron Microscopy Society of America ◽

10.1017/s0424820100125737 ◽

1987 ◽

Vol 45 ◽

pp. 160-161

Author(s):

Tapan Roy

Keyword(s):

Silicon Nitride ◽

High Resolution ◽

Ceramic Matrix Composites ◽

High Resolution Electron Microscopy ◽

Molten Silicon ◽

Matrix Composites ◽

Ceramic Fibers ◽

Resolution Electron ◽

Point To Point ◽

Technological University

Ceramic fibers are being used to improve the mechanical properties of metal matrix and ceramic matrix composites. This paper reports a study of the structural and other microstructural characteristics of silicon nitride whiskers using both conventional TEM and high resolution electron microscopy.The whiskers were grown by T. E. Scott of Michigan Technological University, by passing nitrogen over molten silicon in the presence of a catalyst. The whiskers were ultrasonically dispersed in chloroform and picked up on holey carbon grids. The diameter of some whiskers (<70nm) was small enough to allow direct observation without thinning. Conventional TEM was performed on a Philips EM400T while high resolution imaging was done on a JEOL 200CX microscope with a point to point resolution of 0.23nm.

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Microstructural characterization of plasma-processed Ti-Al metal matrix composites

Proceedings, annual meeting, Electron Microscopy Society of America ◽

10.1017/s0424820100154731 ◽

1989 ◽

Vol 47 ◽

pp. 552-553

Author(s):

M. G. Burke ◽

M. N. Gungor ◽

M. A. Burke

Keyword(s):

High Temperature ◽

Titanium Aluminide ◽

Plasma Processing ◽

Microstructural Characterization ◽

High Temperature Strength ◽

Matrix Composites ◽

Intermetallic Matrix ◽

Long Time ◽

Strength And Stiffness ◽

Intermetallic Matrix Composites

Intermetallic matrix composites are candidates for ultrahigh temperature service when light weight and high temperature strength and stiffness are required. Recent efforts to produce intermetallic matrix composites have focused on the titanium aluminide (TiAl) system with various ceramic reinforcements. In order to optimize the composition and processing of these composites it is necessary to evaluate the range of structures that can be produced in these materials and to identify the characteristics of the optimum structures. Normally, TiAl materials are difficult to process and, thus, examination of a suitable range of structures would not be feasible. However, plasma processing offers a novel method for producing composites from difficult to process component materials. By melting one or more of the component materials in a plasma and controlling deposition onto a cooled substrate, a range of structures can be produced and the method is highly suited to examining experimental composite systems. Moreover, because plasma processing involves rapid melting and very rapid cooling can be induced in the deposited composite, it is expected that processing method can avoid some of the problems, such as interfacial degradation, that are associated with the relatively long time, high temperature exposures that are induced by conventional processing methods.

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