Developing micro-Raman spectroscopy for char structure characterization in the scale of micro- and bulk: A case study of Zhundong coal pyrolysis

Study of modern artistic materials using combined spectroscopic and chromatographic techniques. Case study: painting with the signature “Picasso”

Analytical Methods ◽

10.1039/c4ay02365j ◽

2015 ◽

Vol 7 (4) ◽

pp. 1499-1508 ◽

Cited By ~ 11

Author(s):

Maria Rosa López-Ramírez ◽

Natalia Navas ◽

Luis R. Rodríguez-Simón ◽

Juan C. Otero ◽

Eloisa Manzano

Keyword(s):

Raman Spectroscopy ◽

Analytical Techniques ◽

Chromatographic Techniques ◽

Micro Raman Spectroscopy

A painting bearing the signature “Picasso” was investigated and its components were characterised using micro-Raman spectroscopy combined with other analytical techniques such as SEM/EDX, ATR-FTIR and GC-MS).

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Micro-Raman Spectroscopy Evaluation of the Local Mechanical Stress in Shallow Trench Isolation CMOS Structures: Correlation with Defect Generation and Diode Leakage

10.31399/asm.cp.istfa1998p0011 ◽

1998 ◽

Author(s):

I. De Wolf ◽

G. Groeseneken ◽

H.E. Maes ◽

M. Bolt ◽

K. Barla ◽

...

Keyword(s):

Raman Spectroscopy ◽

Mechanical Stress ◽

Defect Formation ◽

Active Area ◽

Wet Oxidation ◽

Leakage Currents ◽

Shallow Trench Isolation ◽

Micro Raman Spectroscopy ◽

Silicon Devices ◽

Trench Isolation

Abstract It is shown, using micro-Raman spectroscopy, that Shallow Trench Isolation introduces high stresses in the active area of silicon devices when wet oxidation steps are used. These stresses result in defect formation in the active area, leading to high diode leakage currents. The stress levels are highest near the outer edges of line structures and at square structures. They also increase with decreasing active area dimensions.

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MICRO RAMAN SPECTROSCOPY OF FLUID INCLUSIONS IN CHERTS: EXTENDING LIFE DETECTION STRATEGIES TO GEOCHRONOLOGY

10.1130/abs/2016am-287294 ◽

2016 ◽

Author(s):

Dina M. Bower ◽

◽

Andrew Steele ◽

Pamela G. Conrad ◽

Marc Fries

Keyword(s):

Raman Spectroscopy ◽

Fluid Inclusions ◽

Micro Raman Spectroscopy ◽

Life Detection ◽

Detection Strategies

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Micro-Raman spectroscopy of Shang oracle bone inscriptions

Journal of Archaeological Science Reports ◽

10.1016/j.jasrep.2021.102910 ◽

2021 ◽

Vol 37 ◽

pp. 102910

Author(s):

Jhih-Huei Liu ◽

Weiying Ke ◽

Ming-chorng Hwang ◽

Kuang Yu Chen

Keyword(s):

Raman Spectroscopy ◽

Micro Raman Spectroscopy

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Use of WetSEM® capsules for convenient multimodal scanning electron microscopy, energy dispersive X-ray analysis, and micro Raman spectroscopy characterisation of technetium oxides

Journal of Radioanalytical and Nuclear Chemistry ◽

10.1007/s10967-021-07737-5 ◽

2021 ◽

Author(s):

D. J. Bailey ◽

M. C. Stennett ◽

J. Heo ◽

N. C. Hyatt

Keyword(s):

Raman Spectroscopy ◽

Low Cost ◽

Powder Materials ◽

Spectroscopy Analysis ◽

X Ray ◽

Micro Raman Spectroscopy ◽

Hazard And Risk ◽

Sem Imaging ◽

General User ◽

532 Nm

AbstractSEM–EDX and Raman spectroscopy analysis of radioactive compounds is often restricted to dedicated instrumentation, within radiological working areas, to manage the hazard and risk of contamination. Here, we demonstrate application of WetSEM® capsules for containment of technetium powder materials, enabling routine multimodal characterisation with general user instrumentation, outside of a controlled radiological working area. The electron transparent membrane of WetSEM® capsules enables SEM imaging of submicron non-conducting technetium powders and acquisition of Tc Lα X-ray emission, using a low cost desktop SEM–EDX system, as well as acquisition of good quality μ-Raman spectra using a 532 nm laser.

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Influence of Different Conditioning Treatments on The Bond Integrity of Root Dentin to rGO Infiltrated Dentin Adhesive. SEM, EDX, FTIR and MicroRaman Study

Polymers ◽

10.3390/polym13101555 ◽

2021 ◽

Vol 13 (10) ◽

pp. 1555

Author(s):

Firas Alqarawi ◽

Mazen Alkahtany ◽

Khalid Almadi ◽

Afnan Gassem ◽

Faris Alshahrani ◽

...

Keyword(s):

Raman Spectroscopy ◽

Bond Strength ◽

Strength Test ◽

Control Group ◽

Micro Raman Spectroscopy ◽

Fiber Posts ◽

Root Canal Disinfection ◽

Reduced Graphene ◽

Root Dentin ◽

Push Out

The present study aimed to synthesize and equate the mechanical properties and dentin interaction of two adhesives; experimental adhesive (EA) and 5 wt.% reduced graphene oxide rGO) containing adhesive. Scanning electron microscopy (SEM)-Energy-dispersive X-ray spectroscopy (EDX), Micro-Raman spectroscopy, push-out bond strength test, and Fourier Transform Infrared (FTIR) spectroscopy were employed to study nano-bond strength, degree of conversion (DC), and adhesive-dentin interaction. The EA was prepared, and rGO particles were added to produce two adhesive groups, EA-rGO-0% (control) and rGO-5%. The canals of sixty roots were shaped and prepared, and fiber posts were cemented. The specimens were further alienated into groups based on the root canal disinfection technique, including 2.5% sodium hypochlorite (NaOCl), Photodynamic therapy (PDT), and ER-CR-YSGG laser (ECYL). The rGO nanoparticles were flake-shaped, and EDX confirmed the presence of carbon (C). Micro-Raman spectroscopy revealed distinct peaks for graphene. Push-out bond strength test demonstrated highest values for the EA-rGO-0% group after NaOCl and PDT conditioning whereas, rGO-5% showed higher values after ECYL conditioning. EA-rGO-0% presented greater DC than rGO-5% adhesive. The rGO-5% adhesive demonstrated comparable push-out bond strength and rheological properties to the controls. The rGO-5% demonstrated acceptable DC (although lower than control group), appropriate dentin interaction, and resin tag establishment.

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New minerals tsangpoite Ca5(PO4)2(SiO4) and matyhite Ca9(Ca0.5□0.5)Fe(PO4)7 from the D'Orbigny angrite

Mineralogical Magazine ◽

10.1180/mgm.2018.125 ◽

2018 ◽

Vol 83 (02) ◽

pp. 293-313 ◽

Cited By ~ 1

Author(s):

Shyh-Lung Hwang ◽

Pouyan Shen ◽

Hao-Tsu Chu ◽

Tzen-Fu Yui ◽

Maria-Euginia Varela ◽

...

Keyword(s):

Electron Microscopy ◽

Raman Spectroscopy ◽

Electron Diffraction ◽

Grain Boundary ◽

Electron Probe ◽

Formation Mechanisms ◽

Formula Unit ◽

Micro Raman Spectroscopy ◽

The Common ◽

Oxygen Atoms

AbstractTsangpoite, ideally Ca5(PO4)2(SiO4), the hexagonal polymorph of silicocarnotite, and matyhite, ideally Ca9(Ca0.5□0.5)Fe(PO4)7, the Fe-analogue of Ca-merrillite, were identified from the D'Orbigny angrite meteorite by electron probe microanalysis, electron microscopy and micro-Raman spectroscopy. On the basis of electron diffraction, the symmetry of tsangpoite was shown to be hexagonal,P63/morP63, witha= 9.489(4) Å,c= 6.991(6) Å,V= 545.1(6) Å3andZ= 2 for 12 oxygen atoms per formula unit, and that of matyhite was shown to be trigonal,R3c, witha= 10.456 (7) Å,c= 37.408(34) Å,V= 3541.6 (4.8) Å3andZ= 6 for 28 oxygen atoms per formula unit. On the basis of their constant association with the grain-boundary assemblage: Fe sulfide + ulvöspinel + Al–Ti-bearing hedenbergite + fayalite–kirschsteinite intergrowth, the formation of tsangpoite and matyhite, along with kuratite (the Fe-analogue of rhönite), can be readily rationalised as crystallisation from residue magmas at the final stage of the D'Orbigny meteorite formation. Alternatively, the close petrographic relations between tsangpoite/matyhite and the resorbed Fe sulfide rimmed by fayalite + kirschsteinite symplectite, such as the nucleation of tsangpoite in association with magnetite ± other phases within Fe sulfide and the common outward growth of needle-like tsangpoite or plate-like matyhite from the fayalite–kirschsteinite symplectic rim of Fe sulfide into hedenbergite, infer that these new minerals and the grain-boundary assemblage might represent metasomatic products resulting from reactions between an intruding metasomatic agent and the porous olivine–plagioclase plate + fayalite-kirschsteinite overgrowth + augite + Fe sulfide aggregates. Still further thermochemical and kinetics evidence is required to clarify the exact formation mechanisms/conditions of the euhedral tsangpoite, matyhite and kuratite at the grain boundary of the D'Orbigny angrite.

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