Microstructure and in vitro bioactivity of laser-cladded bioceramic coating on titanium alloy in a simulated body fluid

2010 ◽  
Vol 489 (1) ◽  
pp. 211-214 ◽  
Author(s):  
Min Zheng ◽  
Ding Fan ◽  
Xiu-kun Li ◽  
Jian-bin Zhang ◽  
Qi-bin Liu
2016 ◽  
Author(s):  
S. A. Syed Nuzul Fadzli ◽  
S. Roslinda ◽  
Firuz Zainuddin ◽  
Hamisah Ismail

Materials ◽  
2017 ◽  
Vol 11 (1) ◽  
pp. 26 ◽  
Author(s):  
Mohamed Hussein ◽  
Madhan Kumar ◽  
Robin Drew ◽  
Nasser Al-Aqeeli

2011 ◽  
Vol 471-472 ◽  
pp. 325-330 ◽  
Author(s):  
K. Venkateswarlu ◽  
N. Rameshbabu ◽  
Arumugam Chandra Bose ◽  
V. Muthupandi ◽  
S. Subramanian

Nanostructured titania/hydroxyapatite (HA) composite layer was developed on commercially pure titanium (Cp Ti) implant material by plasma electrolytic processing (PEP) technique in order to improve its bioactivity and corrosion resistance under physiological conditions. The phases present in the developed composite layer were studied by X-ray diffraction (XRD) technique. The surface morphology and thickness of the composite layers were observed by scanning electron microscopy (SEM). The corrosion characteristics of the developed layer were studied by potentiodynamic polarization scan under simulated body fluid (7.4 pH Hanks solution) and simulated osteoclast (4.5 pH) conditions. The in-vitro bioactivity of the composite layers was studied by using Kokubu’s simulated body fluid (SBF) solution. The X-ray diffractograms reveal the presence of anatase TiO2 and HA phases in the developed layer. The SEM results confirm the pore-free morphology of the implant material surface and the thickness of the developed composite layer was observed to be 110 ± 5 µm for 12 min of PEP. The potentiodynamic polarization study shows an improved corrosion resistance and the in-vitro bioactivity test results indicate enhanced apatite forming ability of PEP treated Cp Ti surfaces compared to that of the untreated Cp Ti, under simulated body fluid conditions.


2011 ◽  
Vol 493-494 ◽  
pp. 582-587 ◽  
Author(s):  
Marziyeh Abbasi-Shahni ◽  
Saeed Hesaraki ◽  
Ali Asghar Behnam-Ghader ◽  
Masoud Hafezi-Ardakani

In this study, nanocomposites based on of β-tri calcium phosphate (β-TCP) and 2.5-10 wt% merwinite nanoparticles were prepared and sintered at 1100-1300°c.The mechanical properties were investigated by measuring compressive strength and fracture toughness. Structural properties were evaluated by XRD, TEM and SEM analysis, and the in vitro bioactivity was studied by soaking the samples in simulated body fluid (SBF). The mechanical strength of the sintered samples wereincreased, by increasing the amount of merwinite phase up to 5 wt%, whereas it decreased when the samples were sintered at 1100 and 1200°c. Nanostructured calcium phosphate layer was formed on the surfaces of the nanocomposites within 1 day immersion in simulated body fluid. Because of appropriate mechanical properties the composite is suggested to be used as substitute for hard tissue.


2015 ◽  
Vol 105 (1) ◽  
pp. 193-203 ◽  
Author(s):  
I.V. Sukhorukova ◽  
A.N. Sheveyko ◽  
Ph. V. Kiryukhantsev‐Korneev ◽  
E.A. Levashov ◽  
D.V. Shtansky

2006 ◽  
Vol 510-511 ◽  
pp. 13-16
Author(s):  
Xiao Bing Zhao ◽  
Xuan Yong Liu ◽  
Chuan Xian Ding

TiO2 coatings on titanium alloy substrates were prepared by atmospheric plasma spraying using commercial nano-powders. Then, as-sprayed coatings were treated using 10% hydrofluoric acid (HF) at room temperature for 30 seconds. As-sprayed and HF-treated titania coatings were soaked in simulated body fluid to investigate the formation of apatite on their surface. Field-emission scanning electron microscopy was used to observe the surface morphologies, and the phase composition of the as-sprayed coating and apatite were analyzed by X-ray diffraction and energy-dispersive X-ray spectrometry. As-sprayed titania coating is composed of rutile, anatase, and a small quantity of Ti3O5. It exhibited excellent adhesion between the TiO2 coatings and titanium alloy substrates, and the bonding strength was about 38 MPa. After in vitro experiment, a new substance containing calcium and phosphate was formed on the surface of HF-treated TiO2 coatings after being soaked in SBF, while the new substance was not formed on the surface of as-sprayed TiO2 coatings. The results indicated that the bioactivity can be induced to the surface of plasma sprayed TiO2 coatings by hydrofluoric acid treatment.


2014 ◽  
Vol 2 (31) ◽  
pp. 5068-5076 ◽  
Author(s):  
Dana Rohanová ◽  
Aldo Roberto Boccaccini ◽  
Diana Horkavcová ◽  
Pavlína Bozděchová ◽  
Petr Bezdička ◽  
...  

For decades the bioactivity of materials has been tested in laboratories by means of in vitro tests under standard ISO 23317 in a Tris-buffered simulated body fluid solution (SBF).


RSC Advances ◽  
2019 ◽  
Vol 9 (22) ◽  
pp. 12232-12246 ◽  
Author(s):  
Zakaria Tabia ◽  
Khalil El Mabrouk ◽  
Meriame Bricha ◽  
Khalid Nouneh

The effects of the magnesium doping of binary glass (Si–Ca) on particle texture, on the biomineralization process in simulated body fluid (SBF) as well as on drug loading and release were examined.


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