Integrated sol-gel and hydrothermal synthesis of V2O5–TiO2 nanocatalysts for enhanced catalytic removal of H2S

2021 ◽  
pp. 129791
Author(s):  
Hyun Soo Lee ◽  
Jae Hwan Yang ◽  
Hyun Ji Lee ◽  
Hyojin Lee ◽  
Sang-Chae Jeon
Materials ◽  
2021 ◽  
Vol 14 (14) ◽  
pp. 3876
Author(s):  
Jesús Valdés ◽  
Daniel Reséndiz ◽  
Ángeles Cuán ◽  
Rufino Nava ◽  
Bertha Aguilar ◽  
...  

The effect of microwave radiation on the hydrothermal synthesis of the double perovskite Sr2FeMoO6 has been studied based on a comparison of the particle size and structural characteristics of products from both methods. A temperature, pressure, and pH condition screening was performed, and the most representative results of these are herein presented and discussed. Radiation of microwaves in the hydrothermal synthesis method led to a decrease in crystallite size, which is an effect from the reaction temperature. The particle size ranged from 378 to 318 nm when pH was 4.5 and pressure was kept under 40 bars. According to X-ray diffraction (XRD) results coupled with the size-strain plot method, the product obtained by both synthesis methods (with and without microwave radiation) have similar crystal purity. The Scanning Electron Microscopy (SEM) and Energy Dispersive X-ray Spectroscopy (EDS) techniques showed that the morphology and the distribution of metal ions are uniform. The Curie temperature obtained by thermogravimetric analysis indicates that, in the presence of microwaves, the value was higher with respect to traditional synthesis from 335 K to 342.5 K. Consequently, microwave radiation enhances the diffusion and nucleation process of ionic precursors during the synthesis, which promotes a uniform heating in the reaction mixture leading to a reduction in the particle size, but keeping good crystallinity of the double perovskite. Precursor phases and the final purity of the Sr2FeMoO6 powder can be controlled via hydrothermal microwave heating on the first stages of the Sol-Gel method.


2016 ◽  
Vol 33 (4) ◽  
pp. 1192-1199 ◽  
Author(s):  
Behrang Izadkhah ◽  
Aligholi Niaei ◽  
Daryush Salari ◽  
Shahriar Hosseinpoor ◽  
Seyed Ali Hosseini ◽  
...  
Keyword(s):  
Sol Gel ◽  

2013 ◽  
Vol 690-693 ◽  
pp. 351-354 ◽  
Author(s):  
Hong Dan Xue ◽  
Fu Li Wang ◽  
Guo Li Li ◽  
Pu Liu ◽  
Yong Qing Bai ◽  
...  

Hydrotalcite-like compounds are a class of anionic lays or layed double hydroxiods (LDHs) which consists of alkalescence, anion-exchanges and memory effect. The synthetic methods of LDHs include coprecipitation, hydrothermal synthesis, mirowave radiation, ion exchange, sol-gel method, roasting reduction method, instant synthesis, etc.The molar ratio of raw materials, pH value,reaction temperature,reaction time and so on have a greater impact on the purity and crystallinity of the LDHs.


2006 ◽  
Vol 41 (7) ◽  
pp. 1330-1336 ◽  
Author(s):  
Lei Hou ◽  
Yu-Dong Hou ◽  
Xue-Mei Song ◽  
Man-Kang Zhu ◽  
Hao Wang ◽  
...  

2015 ◽  
Vol 263 ◽  
pp. 9-19 ◽  
Author(s):  
Jiancheng Wang ◽  
Zhaoliang Peng ◽  
Ying Chen ◽  
Weiren Bao ◽  
Liping Chang ◽  
...  

2009 ◽  
Vol 517 (6) ◽  
pp. 2023-2028 ◽  
Author(s):  
Aiping Jin ◽  
Wen Chen ◽  
Quanyao Zhu ◽  
Ying Yang ◽  
V.L. Volkov ◽  
...  

2021 ◽  
Vol 6 (2) ◽  
pp. 39-52
Author(s):  
Jaya Edianta ◽  
Nanang Fauzi ◽  
Marzuki Naibaho ◽  
Fitri Suryani Arsyad ◽  
Idha Royani

Betel leaf is a typical Indonesian herbal plant that propagates on other tree trunks. So far, betel leaf has only been used in biomedicine and traditional medicine, whereas the chemical compounds of betel leaf can be used to absorb electromagnetic waves. In this mini-review, we review several research results to discuss the potential effectiveness of betel leaf in barium hexaferrite as an absorber of electromagnetic radiation. We compiled this mini-review based on the literature review method that is discussed extensively and in-depth regarding the chemical composition of betel leaf, modification of the development of barium hexaferrite material with betel leaf media extract, characteristics of BaFe12O19 as absorption of electromagnetic waves, and the effectiveness of media extracts in BaFe12O19 as absorption of electromagnetic waves. Based on the results of the literature review, the modification of BaFe12O19 material synthesis can include microemulsion, solid-state, coprecipitation, sol-gel, and hydrothermal synthesis. So far, hydrothermal synthesis is a synthesis method of mixing betel leaf extract media and ferrite-based magnets that have been studied before. Betel leaf in ferrite-based magnetic materials has been studied not to damage the surface morphology and characteristics of the magnetic material. The results of the assessment also show the effectiveness of adding other elements or compounds such as Ni, Al2O3, and composites in ferrite-based magnetic materials that can absorb more than 90% of electromagnetic waves in the frequency range 2-18 GHz.


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