Microstructure, tensile properties and thermal stability of AlMgSiScZr alloy printed by laser powder bed fusion

2021 ◽  
Vol 69 ◽  
pp. 200-211
Author(s):  
Jiang Bi ◽  
Zhenglong Lei ◽  
Yanbin Chen ◽  
Xi Chen ◽  
Ze Tian ◽  
...  
2020 ◽  
pp. 129074
Author(s):  
P.K. Shurkin ◽  
N.V. Letyagin ◽  
A.I. Yakushkova ◽  
M.E. Samoshina ◽  
D. Yu. Ozherelkov ◽  
...  

Metals ◽  
2018 ◽  
Vol 8 (8) ◽  
pp. 643 ◽  
Author(s):  
Pavel Krakhmalev ◽  
Gunnel Fredriksson ◽  
Krister Svensson ◽  
Igor Yadroitsev ◽  
Ina Yadroitsava ◽  
...  

This article overviews the scientific results of the microstructural features observed in 316 L stainless steel manufactured by the laser powder bed fusion (LPBF) method obtained by the authors, and discusses the results with respect to the recently published literature. Microscopic features of the LPBF microstructure, i.e., epitaxial nucleation, cellular structure, microsegregation, porosity, competitive colony growth, and solidification texture, were experimentally studied by scanning and transmission electron microscopy, diffraction methods, and atom probe tomography. The influence of laser power and laser scanning speed on the microstructure was discussed in the perspective of governing the microstructure by controlling the process parameters. It was shown that the three-dimensional (3D) zig-zag solidification texture observed in the LPBF 316 L was related to the laser scanning strategy. The thermal stability of the microstructure was investigated under isothermal annealing conditions. It was shown that the cells formed at solidification started to disappear at about 800 °C, and that this process leads to a substantial decrease in hardness. Colony boundaries, nevertheless, were quite stable, and no significant grain growth was observed after heat treatment at 1050 °C. The observed experimental results are discussed with respect to the fundamental knowledge of the solidification processes, and compared with the existing literature data.


Metals ◽  
2021 ◽  
Vol 12 (1) ◽  
pp. 57
Author(s):  
Bharat Mehta ◽  
Arvid Svanberg ◽  
Lars Nyborg

This study shows a rapid and systematic approach towards identifying full density and peak hardness for an Al-Mg-Sc-Zr alloy commonly known as Scalmalloy®. The alloy is tailored for the laser powder bed fusion process and has been shown to be printable with >99.8% relative density. The microstructure suggests Al grain refinement in melt pool boundaries, associated with formation of primary Al3(Sc,Zr) particles during solidification. Peak hardening response was identified by heat treatment tests at 573,598 and 623 K between 0 and 10 h. A peak hardness of 172 HV0.3 at 598 K for 4 h was identified. The mechanical properties were also tested with yield and ultimate strengths of 287 MPa and 364 MPa in as-printed and 468 MPa and 517 MPa in peak hardened conditions, respectively, which is consistent with the literature. Such an approach is considered apt when qualifying new materials in industrial laser powder bed fusion systems. The second part of the study discusses the thermal stability of such alloys post-peak-hardening. One set of samples was peak hardened at the conditions identified before and underwent secondary ageing at three different temperatures of 423,473 and 523 K between 0 and 120 h to understand thermal stability and benchmark against conventional Al alloys. The secondary heat treatments performed at lower temperatures revealed lower deterioration of hardness over ageing times as compared to the datasheets for conventional Al alloys and Scalmalloy®, thus suggesting that longer ageing times are needed.


Materials ◽  
2021 ◽  
Vol 14 (15) ◽  
pp. 4280
Author(s):  
Magnus Neikter ◽  
Emil Edin ◽  
Sebastian Proper ◽  
Phavan Bhaskar ◽  
Gopi Krishna Nekkalapudi ◽  
...  

Alloy 21-6-9 is an austenitic stainless steel with high strength, thermal stability at high temperatures, and retained toughness at cryogenic temperatures. This type of steel has been used for aerospace applications for decades, using traditional manufacturing processes. However, limited research has been conducted on this alloy manufactured using laser powder-bed fusion (LPBF). Therefore, in this work, a design of experiment (DOE) was performed to obtain optimized process parameters with regard to low porosity. Once the optimized parameters were established, horizontal and vertical blanks were built to investigate the mechanical properties and potential anisotropic behavior. As this alloy is exposed to elevated temperatures in industrial applications, the effect of elevated temperatures (room temperature and 750 °C) on the tensile properties was investigated. In this work, it was shown that alloy 21-6-9 could be built successfully using LPBF, with good properties and a density of 99.7%, having an ultimate tensile strength of 825 MPa, with an elongation of 41%, and without any significant anisotropic behavior.


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